Pesticide analysis at ppt concentration levels: coupling nano-liquid chromatography with dielectric barrier discharge ionization-mass spectrometry

Analytical and Bioanalytical Chemistry

Volumn 408, Issue 13, 2016, Pages 3425-3434

  Mirabelli, Mario F ^a   Wolf, Jan Christoph ^a,b   Zenobi, Renato ^a  

^a ETH ZURICH   (Switzerland)

^b Plasmion UG   (Germany)

Author keywords

Active capillary plasma ionization; Ambient ionization; DBDI; Nano liquid chromatography; Pesticides; QuEChERS

Indexed keywords

CHEMICAL CONTAMINATION; DIELECTRIC DEVICES; DIELECTRIC MATERIALS; ELECTRIC DISCHARGES; FLOW CONTROL; IONIZATION OF LIQUIDS; LIQUIDS; MASS SPECTROMETRY; PESTICIDES;

AMBIENT IONIZATIONS; CAPILLARY PLASMA; DBDI; NANO LIQUID CHROMATOGRAPHY; QUECHERS;

LIQUID CHROMATOGRAPHY;

PESTICIDE;

ELECTROSPRAY MASS SPECTROMETRY; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY; NANOTECHNOLOGY; PROCEDURES; TANDEM MASS SPECTROMETRY;

CHROMATOGRAPHY, LIQUID; LIMIT OF DETECTION; NANOTECHNOLOGY; PESTICIDES; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

EID: 84959128714     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-016-9419-x     Document Type: Article

References (19)

1. Alder L, Greulich K, Kempe G, Vieth B. Residue analysis of 500 high priority pesticides: better by GC-MS or LC-MS/MS? Mass Spectrom Rev. 2006;25(6):838–65.
2. Karlsson KE, Novotny M. Separation efficiency of slurry-packed liquid chromatography microcolumns with very small inner diameters. Anal Chem. 1988;60(17):1662–5.
3. Hernández-Borges J, Aturki Z, Rocco A, Fanali S. Recent applications in nanoliquid chromatography. J Sep Sci. 2007;30(11):1589–610.
4. Mills M, Maltas J, Lough WJ. Assessment of injection volume limits when using on-column focusing with microbore liquid chromatography. J Chromatogr A. 1997;759(1):1–11.
5. Buonasera K, D’Orazio G, Fanali S, Dugo P, Mondello L. Separation of organophosphorus pesticides by using nano-liquid chromatography. J Chromatogr A. 2009;1216(18):3970–6.
6. Cappiello A, Famiglini G, Palma P, Mangani F. Trace level determination of organophosphorus pesticides in water with the new direct-electron ionization LC/MS interface. Anal Chem. 2002;74(14):3547–54.
7. Cappiello A, Famiglini G, Mangani F, Palma P, Siviero A. Nano-high-performance liquid chromatography–electron ionization mass spectrometry approach for environmental analysis. Anal Chim Acta. 2003;493(2):125–36.
8. Zhu KY, Leung KW, Ting AKL, Wong ZCF, Ng WYY, Choi RCY, et al. Microfluidic chip based nano liquid chromatography coupled to tandem mass spectrometry for the determination of abused drugs and metabolites in human hair. Anal Bioanal Chem. 2012;402(9):2805–15.
9. Asensio-Ramos M, D’Orazio G, Hernandez-Borges J, Rocco A, Fanali S. Multi-walled carbon nanotubes-dispersive solid-phase extraction combined with nano-liquid chromatography for the analysis of pesticides in water samples. Anal Bioanal Chem. 2011;400(4):1113–23.
10. Smoluch M, Mielczarek P, Silberring J. Plasma‐based ambient ionization mass spectrometry in bioanalytical sciences. Mass Spectrom Rev. 2015. doi:10.1002/mas.21460.
11. Wiley JS, García-Reyes JF, Harper JD, Charipar NA, Ouyang Z, Cooks RG. Screening of agrochemicals in foodstuffs using low-temperature plasma (LTP) ambient ionization mass spectrometry. Analyst. 2010;135(5):971–9.
12. Albert A, Kramer A, Scheeren S, Engelhard C. Rapid and quantitative analysis of pesticides in fruits by QuEChERS pretreatment and low-temperature plasma desorption/ionization orbitrap mass spectrometry. Anal Methods. 2014;6(15):5463–71.
13. Tang F, Chen J, Wang X, Zhang S, Zhang X. Development of dielectric-barrier-discharge ionization. Anal Bioanal Chem. 2015;407(9):2345–64.
14. Gilbert-López B, Geltenpoth H, Meyer C, Michels A, Hayen H, Molina-Díaz A, et al. Performance of dielectric barrier discharge ionization mass spectrometry for pesticide testing: a comparison with atmospheric pressure chemical ionization and electrospray ionization. Rapid Commun Mass Spectrom. 2013;27(3):419–29.
15. Hayen H, Michels A, Franzke J. Dielectric barrier discharge ionization for liquid chromatography/mass spectrometry. Anal Chem. 2009;81(24):10239–45.
16. Gilbert-López B, García-Reyes JF, Meyer C, Michels A, Franzke J, Molina-Díaz A, et al. Simultaneous testing of multiclass organic contaminants in food and environment by liquid chromatography/dielectric barrier discharge ionization-mass spectrometry. Analyst. 2012;137(22):5403–10.
17. Nudnova MM, Zhu L, Zenobi R. Active capillary plasma source for ambient mass spectrometry. Rapid Commun Mass Spectrom. 2012;26(12):1447–52.
18. Wolf J, Schaer M, Siegenthaler P, Zenobi R. Direct quantification of chemical warfare agents and related compounds at low ppt levels: comparing active capillary dielectric barrier discharge plasma ionization and secondary electrospray ionization mass spectrometry. Anal Chem. 2014;87(1):723–9.
19. Makarov A, Scigelova M. Coupling liquid chromatography to Orbitrap mass spectrometry. J Chromatogr A. 2010;1217(25):3938–45.