Analysis of the sulfuric acid hydrolysis of wood pulp for cellulose nanocrystal production: A central composite design study

Industrial Crops and Products

Volumn 93, Issue , 2016, Pages 76-87

  Dong, Shuping ^a   Bortner, Michael J ^a,b   Roman, Maren ^a  

^a VIRGINIA POLYTECHNIC INSTITUTE AND STATE UNIVERSITY   (United States)

^b State University   (United States)

Author keywords

Acid hydrolysis; Cellulose nanocrystals; Central composite design; Sulfate group density; Yield

Indexed keywords

CELLULOSE; CELLULOSE DERIVATIVES; DESIGN; NANOCRYSTALS; PULP MATERIALS; REGRESSION ANALYSIS; SULFUR COMPOUNDS; SULFURIC ACID; WOOD;

ACID HYDROLYSIS; CELLULOSE NANO-CRYSTALS; CENTRAL COMPOSITE DESIGNS; SULFATE GROUPS; YIELD;

HYDROLYSIS;

CELLULOSE; COMPOSITE; CRYSTAL; DESIGN METHOD; EXPERIMENTAL DESIGN; HYDROLYSIS; NANOPARTICLE; PULP AND PAPER INDUSTRY; SULFATE GROUP; SULFURIC ACID; WOOD; YIELD;

EID: 84958581527     PISSN: 09266690     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.indcrop.2016.01.048     Document Type: Article

References (26)

1. Araki, J., Wada, M., Kuga, S., Okano, T., Flow properties of microcrystalline cellulose suspension prepared by acid treatment of native cellulose. Colloids Surf. A 142 (1998), 75–82.
2. Battista, O.A., Coppick, S., Howsmon, J.A., Morehead, F.F., Sisson, W.A., Level-off degree of polymerization—relation to polyphase structure of cellulose fibres. Ind. Eng. Chem. 48 (1956), 333–335.
3. Bondeson, D., Mathew, A., Oksman, K., Optimization of the isolation of nanocrystals from microcrystalline cellulose by acid hydrolysis. Cellulose 13 (2006), 171–180.
4. Chen, L., Wang, Q., Hirth, K., Baez, C., Agarwal, U.P., Zhu, J.Y., Tailoring the yield and characteristics of wood cellulose nanocrystals (CNC) using concentrated acid hydrolysis. Cellulose 22 (2015), 1753–1762.
5. Cowie, J., Bilek, E.M., Wegner, T.H., Shatkin, J., Market projections of cellulose nanomaterial-enabled products—part 2 Volume estimates. TAPPI J. 13 (2014), 57–69.
6. Dong, X.M., Revol, J.F., Gray, D.G., Effect of microcrystalline preparation conditions on the formation of colloid crystals of cellulose. Cellulose 1998:5 (1998), 19–32.
7. Fan, J.S., Li, Y.H., Maximizing the yield of nanocrystalline cellulose from cotton pulp fiber. Carbohydr. Polym. 88 (2012), 1184–1188.
8. Giovannitti-Jensen, A., Myers, R.H., Graphical assessment of the prediction capability of response surface designs. Technometrics 31 (1989), 159–171.
9. Hamad, W.Y., Hu, T.Q., Structure-process-yield interrelations in nanocrystalline cellulose extraction. Can. J. Chem. Eng. 88 (2010), 392–402.
10. Lu, Z.X., Fan, L.W., Zheng, H.Y., Lu, Q.L., Liao, Y.Q., Huang, B.A., Preparation: characterization and optimization of nanocellulose whiskers by simultaneously ultrasonic wave and microwave assisted. Bioresour. Technol. 46 (2013), 82–88.
11. Marchessault, R.H., Morehead, F.F., Koch, M.J., Some hydrodynamic properties of neutral suspensions of cellulose crystallites as related to size and shape. J. Colloid Sci. 16 (1961), 327–344.
12. Mukherjee, S.M., Woods, H.J., X-ray and electron microscope studies of the degradation of cellulose by sulphuric acid. Biochim. Biophys. Acta 10 (1953), 499–511.
13. Nickerson, R.F., Habrle, J.A., Cellulose intercrystalline structure. Ind. Eng. Chem. 39 (1947), 1507–1512.
14. Rawlings, J.O., Pantula, S.G., Dickey, D.A., Applied Regression Analysis. A Research Tool. 2nd ed., 1998, Springer, New York.
15. Rånby, B.G., III. Fibrous macromolecular systems. Cellulose and muscle. The colloidal properties of cellulose micelles. Discussions Faraday Soc. 11 (1951), 158–164.
16. Revol, J.-F., Bradford, H., Giasson, J., Marchessault, R.H., Gray, D.G., Helicoidal self-ordering of cellulose microfibrils in aqueous suspension. Int. J. Biol. Macromol. 14 (1992), 170–172.
17. Revol, J.-F., Godbout, L., Dong, X.M., Gray, D.G., Chanzy, H., Maret, G., Chiral nematic suspensions of cellulose crystallites; phase separation and magnetic field orientation. Liq. Cryst. 16 (1994), 127–134.
18. Revol, J.-F., Godbout, L., Gray, D.G., Solid self-assembled films of cellulose with chiral nematic order and optically variable properties. J. Pulp Pap. Sci. 24 (1998), 146–149.
19. Ridge, E., Kudenko, D., Sequential experiment designs for screening and tuning parameters of stochastic heuristics. In Proceedings of the Workshop on Empirical Methods for the Analysis of Algorithms, Reykjavik, Iceland, September 9, 2006, 27–34.
20. Shatkin, J., Wegner, T.H., Bilek, E.M., Cowie, C., Market projections of cellulose nanomaterial-enabled products—part 1 applications. TAPPI J. 13 (2014), 9–16.
21. Tang, L.-R., Huang, B., Ou, W., Chen, X.R., Chen, Y.D., Manufacture of cellulose nanocrystals by cation exchange resin-catalyzed hydrolysis of cellulose. Bioresour. Technol. 102 (2011), 10973–10977.
22. Vining, G., Technical advice design of experiments, response surface methodology, and sequential experimentation. Qual. Eng. 23 (2011), 217–220.
23. Wang, H.Z., Qian, C., Roman, M., Effects of pH and salt concentration on the formation and properties of chitosan–cellulose nanocrystal polyelectrolyte–macroion complexes. Biomacromolecules 12 (2011), 3708–3714.
24. Wang, Q.Q., Zhu, J.Y., Reiner, R.S., Verrill, S.P., Baxa, U., McNeil, S.E., Approaching zero cellulose loss in cellulose nanocrystal (CNC) production: recovery and characterization of cellulosic solid residues (CSR) and CNC. Cellulose 19 (2012), 2033–2047.
25. Wang, Q.Q., Zhao, X.B., Zhu, J.Y., Kinetics of strong acid hydrolysis of a bleached kraft pulp for producing cellulose nanocrystals (CNCs). Ind. Eng. Chem. Res. 53 (2014), 11007–11014.
26. Zou, P.P., Zhang, P., Gao, D., Xia, Q.N., Process’ optimization of nanocrystalline cellulose and its properties. Appl. Mech. Mater. 200 (2012), 373–376.