Experimental design for extraction of bio-oils from flax seeds under supercritical ethanol conditions

Clean Technologies and Environmental Policy

Volumn 18, Issue 2, 2016, Pages 461-471

  Tekin, Kubilay ^a   Akalin, Mehmet K ^a   Karagöz, Selhan ^a  

^a KARABUK UNIVERSITY   (Turkey)

Author keywords

Bio oil; Experimental design; Flax seeds; Supercritical ethanol extraction

Indexed keywords

BIOCONVERSION; BIOMASS; DESIGN OF EXPERIMENTS; ETHANOL; EXTRACTION; FATTY ACIDS; FLAX; LINEN; PLANTS (BOTANY); STATISTICS;

BIO OIL; BIOMASS CONCENTRATIONS; CENTRAL COMPOSITE DESIGNS; COEFFICIENT OF DETERMINATION; EXTRACTION TEMPERATURES; OXYGENATED HYDROCARBON; RELATIVE CONCENTRATION; SUPERCRITICAL ETHANOL;

OILSEEDS;

EID: 84958121455     PISSN: 1618954X     EISSN: 16189558     Source Type: Journal    
DOI: 10.1007/s10098-015-1021-y     Document Type: Article

References (32)

1. Akalin MK, Karagoz S, Akyuz M (2013) Supercritical ethanol extraction of bio-oils from German beech wood: Design of experiments. Ind Crop Prod 49:720-729
2. Akalln MK, Akyüz M, Karagöz S (2015) Supercritical fluid extraction of bio-oils from hawthorn stones: A Box-Behnken design for the extraction parameters. Energy Technol 3:40-47
3. Alper K, Tekin K, Karagoz S (2014) Pyrolysis of agricultural residues for bio-oil production. Clean Technol Environ Policy 17:211-223
4. Bezerra MA, Santelli RE, Oliveira EP, Villar LS, Escaleira LA (2008) Response surface methodology (RSM) as a tool for optimization in analytical chemistry. Talanta 76:965-977
5. Borugadda VB, Goud VV (2012) Biodiesel production from renewable feedstocks: Status and opportunities. Renew Sustain Energy Rev 16:4763-4784
6. Brand S, Susanti RF, Kim SK, Lee H, Kim J, Sang B-I (2013) Supercritical ethanol as an enhanced medium for lignocellulosic biomass liquefaction: Influence of physical process parameters. Energy 59:173-182
7. Brown JN, Brown RC (2012) Process optimization of an auger pyrolyzer with heat carrier using response surface methodology. Bioresour Technol 103:405-414
8. Halim SFA, Kamaruddin AH, Fernando WJN (2009) Continuous biosynthesis of biodiesel from waste cooking palm oil in a packed bed reactor: Optimization using response surface methodology (RSM) and mass transfer studies. Bioresour Technol 100:710-716
9. Ivanov DS, Čolović RR, Lević JD, Sredanović SA (2012) Optimization of supercritical fluid extraction of linseed oil using RSM. Eur J Lipid Sci Technol 114:807-815
10. Khayet M, Zahrim AY, Hilal N (2011) Modelling and optimization of coagulation of highly concentrated industrial grade leather dye by response surface methodology. Chem Eng J 167:77-83
11. Kim J-Y, Oh S, Hwang H, Cho T, Choi I-G, Choi JW (2013) Effects of various reaction parameters on solvolytical depolymerization of lignin in sub- And supercritical ethanol. Chemosphere 93:1755-1764
12. Leardi R (2009) Experimental design in chemistry: A tutorial. Anal Chim Acta 652:161-172
13. Lestander TA, Samuelsson R (2010) Prediction of resin and fatty acid content of biorefinery feedstock by on-line near-infrared (NIR) spectroscopy. Energy Fuels 24:5148-5152
14. Liu H-M, Liu Y-L (2014) Characterization of milled solid residue from cypress liquefaction in sub- And super ethanol. Bioresour Technol 151:424-427
15. Liu Z, Zhang F-S (2008) Effects of various solvents on the liquefaction of biomass to produce fuels and chemical feedstocks. Energy Convers Manag 49:3498-3504
16. Lu J, Boughner EC, Liotta CL, Eckert CA (2002) Nearcritical and supercritical ethanol as a benign solvent: Polarity and hydrogen-bonding. Fluid Phase Equilib 198:37-49
17. Miller JE, Evans L, Littlewolf A, Trudell DE (1999) Batch microreactor studies of lignin and lignin model compound depolymerization by bases in alcohol solvents. Fuel 78:1363-1366
18. Morris DH (2007) Flax - A health and nutrition primer, 4th edn. Flax Council of Canada, Chapter 1, pp 9-21
19. Nikoo M, Saeidi S, Lohi A (2015) A comparative thermodynamic analysis and experimental studies on hydrogen synthesis by supercritical water gasification of glucose. Clean Technol Environ Policy. doi: 10.1007/s10098-015-0965-2
20. Prasad L, Salvi BL, Kumar V (2015) Thermal degradation and gasification characteristics of Tung shells as an open top downdraft wood gasifier feedstock. Clean Technol Environ Policy 17:1699-1706. doi: 10.1007/s10098-014-0891-8
21. Ramos MJ, Fernández CM, Casas A, Rodríguez L, Pérez Á (2009) Influence of fatty acid composition of raw materials on biodiesel properties. Bioresour Technol 100:261-268
22. Reddy HK, Muppaneni T, Patil PD, Ponnusamy S, Cooke P, Schaub T, Deng S (2014) Direct conversion of wet algae to crude biodiesel under supercritical ethanol conditions. Fuel 115:720-726
23. Santos DT, Albarelli JQ, Rostagno MA, Ensinas AV, Marechal F, Meireles MAA (2014) New proposal for production of bioactive compounds by supercritical technology integrated to a sugarcane biorefinery. Clean Technol Environ Policy 16:1455-1468
24. Sharif KM, Rahman MM, Azmir J, Mohamed A, Jahurul MHA, Sahena F, Zaidul ISM (2014) Experimental design of supercritical fluid extraction - A review. J Food Eng 124:105-116
25. Tekin K (2015) Hydrothermal conversion of russian olive seeds into crude bio-oil using a CaO catalyst derived from waste mussel shells. Energy Fuels 29:4382-4392. doi: 10.1021/acs.energyfuels.5b00724
26. Tekin K, Karagoz S, Bektaş S (2013) Hydrothermal conversion of woody biomass with disodium octaborate tetrahydrate and boric acid. Ind Crops Prod 49:334-340
27. Tekin K, Karagoz S, Bektas S (2014) A review of hydrothermal biomass processing. Renew Sustain Energy Rev 40:673-687
28. Tekin K, Akalin MK, Karagöz S (2015) The effects of water tolerant Lewis acids on the hydrothermal liquefaction of lignocellulosic biomass. J Energy Inst. doi: 10.1016/j.joei.2015.06.003
29. Toor SS, Rosendahl L, Rudolf A (2011) Hydrothermal liquefaction of biomass: A review of subcritical water technologies. Energy 36:2328-2342
30. Wang Y, Wang H, Lin H, Zheng Y, Zhao J, Pelletier A, Li K (2013) Effects of solvents and catalysts in liquefaction of pinewood sawdust for the production of bio-oils. Biomass Bioenerg 59:158-167
31. White PJ (2007) Chapter 10 fatty acids in oilseeds (vegetable oils). In: Chow CK (ed) Fatty acids in foods and their health implications, 3rd edn. CRC Press, New York, pp 227-252
32. Yoshida T, Tsubaki S, TeramotoY Azuma J (2010) Optimization of microwave-assisted extraction of carbohydrates from industrial waste of corn starch production using response surface methodology. Bioresour Technol 101:7820-7826