In-cell clean-up pressurized liquid extraction and gas chromatography-tandem mass spectrometry determination of hydrophobic persistent and emerging organic pollutants in coastal sediments

Journal of Chromatography A

Volumn 1429, Issue , 2016, Pages 107-118

  Pintado Herrera, Marina G ^a   González Mazo, Eduardo ^a   Lara Martín, Pablo A ^a  

^a UNIVERSITY OF CÁDIZ   (Spain)

Author keywords

Emerging contaminants; Gas chromatography; Mass spectrometry; Persistent organic pollutants; Pressurized liquid extraction; Sediment

Indexed keywords

ALUMINA; AROMATIC HYDROCARBONS; CHROMATOGRAPHY; DICHLOROMETHANE; DRUG PRODUCTS; FLAME RETARDANTS; GAS CHROMATOGRAPHY; HYDROPHOBIC CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; LIQUIDS; MARINE POLLUTION; MASS SPECTROMETRY; ORGANIC POLLUTANTS; POLLUTION; POLYCHLORINATED BIPHENYLS; POLYCYCLIC AROMATIC HYDROCARBONS; SEDIMENTS; SPECTROMETRY; SUBMARINE GEOLOGY;

EMERGING CONTAMINANT; GAS CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; ORGANOPHOSPHORUS FLAME RETARDANTS; PERSISTENT ORGANIC POLLUTANT (POP); POLYCHLORINATED BIPHENYL (PCBS); POLYCYCLIC AROMATIC HYDROCARBONS (PAHS); PRESSURIZED LIQUID EXTRACTION; SIMULTANEOUS DETERMINATIONS;

EXTRACTION;

1,1 DICHLORO 2,2 BIS(4 CHLOROPHENYL)ETHANE; ALDRIN; ALUMINUM OXIDE; ANTHRACENE; ATRAZINE; BIOCIDE; DELTAMETHRIN; DICHLOROMETHANE; DIELDRIN; DIETHYLTOLUAMIDE; ENDOCRINE DISRUPTOR; ESTRONE; ETHION; FRAGRANCE; GALAXOLIDE; HEPTACHLOR; METHYLTRICLOSAN; MUSK AMBRETTE; MUSK KETONE; MUSK MOSKENE; MUSK TIBETENE; MUSK XYLENE; NONYLPHENOL; ORGANIC CARBON; ORGANOPHOSPHORUS COMPOUND; PESTICIDE; POLYCHLORINATED BIPHENYL; POLYCYCLIC AROMATIC HYDROCARBON; TRICLOSAN; UNINDEXED DRUG; BENZOPHENONE DERIVATIVE; FLAME RETARDANT; ORGANIC COMPOUND; ORTHO-HYDROXYBENZOPHENONE; WATER POLLUTANT;

ARTICLE; CLAY; DERIVATIZATION; EMERGING ORGANIC POLLUTANT; EXTRACTION; GAS CHROMATOGRAPHY; HYDROPHOBICITY; LIMIT OF DETECTION; PERSISTENT ORGANIC POLLUTANT; POLLUTANT; PRESSURIZED LIQUID EXTRACTION; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; PRODUCT RECOVERY; QUANTITATIVE ANALYSIS; SAND; SEASHORE; SEDIMENT; SPAIN; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS; ANALYSIS; CHEMISTRY; ENVIRONMENTAL MONITORING; MASS FRAGMENTOGRAPHY; PROCEDURES; WATER POLLUTANT;

BENZOPHENONES; ENDOCRINE DISRUPTORS; ENVIRONMENTAL MONITORING; FLAME RETARDANTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GEOLOGIC SEDIMENTS; ORGANIC CHEMICALS; PESTICIDES; POLYCHLORINATED BIPHENYLS; POLYCYCLIC HYDROCARBONS, AROMATIC; SPAIN; TANDEM MASS SPECTROMETRY; WATER POLLUTANTS, CHEMICAL;

EID: 84953212184     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2015.12.040     Document Type: Article

References (50)

1. Guzzella L., Poma G., De Paolis A., Roscioli C., Viviano G. Organic persistent toxic substances in soils, waters and sediments along an altitudinal gradient at Mt. Sagar matha, Himalayas, Nepal. Environ. Pollut. 2011, 159:2552-2564.
2. Zhou H., Huang X., Gao M., Wang X., Wen X. Distribution and elimination of polycyclic musks in three sewage treatment plants of Beijing, China. J. Environ. Sci. 2009, 21:561-567.
3. Beretta M., Britto V., Tavares T.M., Teixeira da Silva S.M., Pletsch A.L. Occurrence of pharmaceutical and personal care products (PPCPs) in marine sediments in the Todos os Santos Bay and the north coast of Salvador, Bahia, Brazil. J. Soils Sediments 2014, 14:1278-1286.
4. Castro-Jimenez J., Berrojalbiz N., Pizarro M., Dachs J. Organophosphate Ester (OPE) flame retardants and plasticizers in the open Mediterranean and Black Seas atmosphere. Environ. Sci. Technol. 2014, 48:3203-3209.
5. Heim S., Hucke A., Schwarzbauer J., Littke R., Mangini A. Geochronology of anthropogenic contaminants in a dated sediment core of the Rhine River (Germany): emission sources and risk assessment. Acta Hydroch. Hydrob. 2006, 34:34-52.
6. Alvarez D.A., Rosen M.R., Perkins S.D., Cranor W.L., Schroeder V.L., Jones-Lepp T.L. Bottom sediment as a source of organic contaminants in Lake Mead, Nevada, USA. Chemosphere 2012, 88:605-611.
7. Choi M., Kim Y.-J., Lee I.-S., Choi H.-G. Development of a one-step integrated pressurized liquid extraction and cleanup method for determining polycyclic aromatic hydrocarbons in marine sediments. J. Chromatogr. A 2014, 1340:8-14.
8. Traverso-Soto J.M., Lara-Martin P.A., Leon V.M., Gonzalez-Mazo E. Analysis of alcohol polyethoxylates and polyethylene glycols in marine sediments. Talanta 2013, 110:171-179.
9. Net S., El-Osmani R., Prygiel E., Rabodonirina S., Dumoulin D., Ouddane B. Overview of persistent organic pollution (PAHs, Me-PAHs and PCBs) in freshwater sediments from Northern France. J. Geochem. Explor. 2015, 148:181-188.
10. Concha-Graña E., Fernández-González V., Grueiro-Noche G., Muniategui-Lorenzo S., López-Mahía P., Fernández-Fernández E., Prada-Rodríguez D. Development of an environmental friendly method for the analysis of organochlorine pesticides in sediments. Chemosphere 2010, 79:698-705.
11. Pintado-Herrera M.G., Gonzalez-Mazo E., Lara-Martin P.A. Environmentally friendly analysis of emerging contaminants by pressurized hot water extraction-stir bar sorptive extraction-derivatization and gas chromatography-mass spectrometry. Anal. Bioanal. Chem. 2013, 405:401-411.
12. Lara-Martín P.A., Gómez-Parra A., González-Mazo E. Simultaneous extraction and determination of anionic surfactants in waters and sediments. J. Chromatogr. A 2006, 1114:205-210.
13. Sapozhnikova Y., Liebert D., Wirth E., Fulton M. Polycyclic musk fragrances in sediments and shrimp tissues. Polycycl. Aromat. Compd. 2010, 30:298-308.
14. Ghosh K.J. Selective pressurized liquid extraction of three classes of halogenated contaminants in fish. J. Chromatogr. A 2011, 1218:7242-7247.
15. Vallecillos L., Borrull F., Pocurull E. Determination of musk fragrances in sewage sludge by pressurized liquid extraction coupled to automated ionic liquid-based headspace single-drop microextraction followed by GC-MS/MS. J. Sep. Sci. 2012, 35:2735-2742.
16. Pintado-Herrera M.G., Gonzalez-Mazo E., Lara-Martin P.A. Determining the distribution of triclosan and methyl triclosan in estuarine settings. Chemosphere 2014, 95:478-485.
17. Rodil R., Moeder M. Development of a simultaneous pressurised-liquid extraction and clean-up procedure for the determination of UV filters in sediments. Anal. Chim. Acta 2008, 612:152-159.
18. Negreira N., Rodríguez I., Rubí E., Cela R. Optimization of pressurized liquid extraction and purification conditions for gas chromatography-mass spectrometry determination of UV filters in sludge. J. Chromatogr. A 2010, 1218:211-217.
19. Abdallah M.A., Drage D., Harrad S. A one-step extraction/clean-up method for determination of PCBs, PBDEs and HBCDs in environmental solid matrices. Environ. Sci. Process. Impacts 2013, 15:2279-2287.
20. Gomez M.J., Herrera S., Sole D., Garcia-Calvo E., Fernandez-Alba A.R. Automatic searching and evaluation of priority and emerging contaminants in wastewater and river water by stir bar sorptive extraction followed by comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry. Anal. Chem. 2011, 83:2638-2647.
21. Albero B., Sánchez-Brunete E., Pérez R.A., Tadeo J.L. Determination of selected organic contaminants in soil by pressurized liquid extraction and gas chromatography tandem mass spectrometry with in situ derivatization. J. Chromatogr. A 2012, 1248:9-17.
22. Guo J.H., Li Z.N., Sandy A.L., Li A. Method development for simultaneous analyses of multiple legacy and emerging organic chemicals in sediments. J. Chromatogr. A 2014, 1370:1-8.
23. El Rayis O.A. Re-assessment of the titration method for determination of organic carbon in recent sediments. Rapp. Commun. Int. Mer. Medit. 1985, 45-47.
24. Certificate of analysis, Standard Reference Material 1941: Organics in marine sediment, National Institute of Standard s and Technology (NIST). Gaithersburg MD 20899, (2012).
25. Chu S., Metcalfe C.D. Simultaneous determination of triclocarban and triclosan in municipal biosolids by liquid chromatography tandem mass spectrometry. J. Chromatogr. A 2007, 1164:212-218.
26. Zhang Z., Rhind S.M., Kerr C., Osprey M., Kyle C.E. Selective pressurized liquid extraction of estrogenic compounds in soil and analysis by gas chromatography-mass spectrometry. Anal. Chim. Acta 2011, 685:29-35.
27. Recent Advances in Sample Preparation for Accelerated Solvent Extraction- Thermo Scientific Poster Note, PN70546.
28. Fromme H., Otto T., Pilz K. Polycyclic musk fragrances in different environmental compartments in Berlin (Germany). Water. Res. 2001, 35:121-128.
29. Sulfur Cleanup-Method 3660B, Environmental Protection Agency. (EPA).
30. Eguvbe P.M., Iwegbue C.M.A., Ogala J.E., Nwajei G.E., Egboh S.H.O. Distribution of polycyclic aromatic hydrocarbons (PAHs) in sediment cores of selected creeks in Delta State, Nigeria. Environ. Forensics 2014, 15:121-133.
31. Liu Y.S., Ying G.G., Shareef A., Kookana R.S. Simultaneous determination of benzotriazoles and ultraviolet filters in ground water, effluent and biosolid samples using gas chromatography-tandem mass spectrometry. J. Chromatogr. A 2011, 1218:5328-5335.
32. Hawthorne S.B., Yang Y., Miller D.J. Extraction of organic pollutants from environmental solids with sub- and supercritical water. Anal. Chem. 1994, 66:2912-2920.
33. Burkhardt M.R., Zaugg S.D., Burbank T.L., Olson M.C., Iverson J.L. Pressurized liquid extraction using water/isopropanol coupled with solid-phase extraction cleanup for semivolatile organic compounds, polycyclic aromatic hydrocarbons (PAH), and alkylated PAH homolog groups in sediment. Anal. Chim. Acta 2005, 549:104-116.
34. Peck A.M., Linebaugh E.K., Hornbuckle K.C. Synthetic musk fragrances in Lake Erie and Lake Ontario sediment cores. Environ. Sci. Technol. 2006, 40:5629-5635.
35. Van Emon J.M., Chuang J.C., Bronshtein A., Altstein M. Determination of polychlorinated biphenyls in soil and sediment by selective pressurized liquid extraction with immunochemical detection. Sci. Total Environ. 2013, 463:326-333.
36. Essumang D.K., Kowalski K., Sogaard E.G. Levels, distribution and source characterization of polycyclic aromatic hydrocarbons (PAHs) in topsoils and roadside soils in Esbjerg, Denmark. Bull. Environ. Contam. Toxicol. 2011, 86:438-443.
37. Che J.S., Yu R.P., Song Q.J., Wang L.P., Wu S.F. Determination of synthetic musks in the sediment of the Taihu lake by using accelerated solvent extraction (ASE) and GC/MS. Int. J. Environ. An. Ch. 2011, 91:387-399.
38. Göbel A., Thomsen A., McArdell C.S., Alder A.C., Giger W., Theib N., Löffler D., Ternes T.A. Extraction and determination of sulfonamides, macrolides, and trimethoprim in sewage sludge. J. Chromatogr. A 2005, 1085:179-189.
39. corporation D. Accelerated solvent extraction online selectively removal disruptors. Tech. Note 2015, TN210.
40. Sumner N.R., Guitart C., Fuentes G., Readman J.W. Inputs and distributions of synthetic musk fragrances in an estuarine and coastal environment; a case study. Environ. Pollut. 2010, 158:215-222.
41. Ana Perez R., Albero B., Sanchez-Brunete C., Luis Tadeo J. Determination of chlorinated toluenes in soils using gas chromatography tandem mass spectrometry. Int. J. Environ. Anal. Chem. 2012, 92:1666-1678.
42. Camino-Sánchez F.J., Zafra-Gómez A., Pérez-Trujillo J.P., Conde-González J.E., Marques J.C., Vílchez J.L. Validation of a GC-MS/MS method for simultaneous determination of 86 persistent organic pollutants in marine sediments by pressurized liquid extraction followed by stir bar sorptive extraction. Chemosphere 2011, 84:869-881.
43. Casado-Martinez M.C., Forja J.M., DelValls T.A. A multivariate assessment of sediment contamination in dredged materials from Spanish ports. J. Hazard. Mater. 2009, 163:1353-1359.
44. Lara-Martin P.A., Gomez-Parra A., Petrovic M., Barcelo D., Gonzalez-Mazo E. Distribution of organic pollutants in coastal sediments of Cadiz Bay (SW Spain). Cienc. Mar. 2005, 31:203-212.
45. Camacho-Munoz D., Martin J., Santos J.L., Aparicio I., Alonso E. Distribution and risk assessment of pharmaceutical compounds in river sediments from Donana Park (Spain). Water Air Soil Pollut. 2013, 224.
46. Lara-Martín P.A., Petrovic M., Gómez-Parra A., Barceló D., González-Mazo E. Presence of surfactants and their degradation intermediates in sediment cores and grabs from the Cadiz Bay area. Environ. Pollut. 2006, 144:483-491.
47. Cantarero S., Camino-Sanchez F.J., Zafra-Gomez A., Ballesteros O., Navalon A., Vilchez J.L., Verge C., Reis M.S., Saraiva P.M. Evaluation of the presence of major anionic surfactants in marine sediments. Mar. Pollut. Bull. 2012, 64:587-594.
48. Lu B., Feng Y., Gao P., Zhang Z., Lin N. Distribution and fate of synthetic musks in the Songhua River, Northeastern China: influence of environmental variables. Environ. Sci. Pollut. Res. Int. 2015, 22:9090-9099.
49. Mu L., Wen J. Spatial distribution characteristics of polycyclic musks as a chemical marker in river water and sediment compared with other typical pollutants. Water Sci. Technol. 2013, 67:1173-1180.
50. Kameda Y., Kimura K., Miyazaki M. Occurrence and profiles of organic sun-blocking agents in surface waters and sediments in Japanese rivers and lakes. Environ. Pollut. 2011, 159:1570-1576.