Pd nanoparticle formation in ionic liquid thin films monitored by in situ vibrational spectroscopy

Langmuir

Volumn 31, Issue 44, 2015, Pages 12126-12139

  Mehl, Sascha ^a   Toghan, Arafat ^a,b   Bauer, Tanja ^a   Brummel, Olaf ^a   Taccardi, Nicola ^a   Wasserscheid, Peter ^a   Libuda, Jörg ^a  

^a UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

^b SOUTH VALLEY UNIVERSITY   (Egypt)

Author keywords

[No Author keywords available]

Indexed keywords

ABSORPTION SPECTROSCOPY; AGGLOMERATION; C (PROGRAMMING LANGUAGE); COBALT DEPOSITS; DEPOSITION; DYES; FILM PREPARATION; IONIC LIQUIDS; METAL NANOPARTICLES; METALS; MULTILAYER FILMS; NANOPARTICLES; PARTICLE SIZE; PHYSICAL VAPOR DEPOSITION; SYNTHESIS (CHEMICAL); THICK FILMS; THIN FILMS; VAPOR DEPOSITION;

DEPOSITION PARAMETERS; IONIC LIQUID (ILS); IR REFLECTION ABSORPTION SPECTROSCOPY; LOW PARTIAL PRESSURES; MELTING TRANSITIONS; NANOMETER-THICK FILMS; PREPARATION METHOD; TEMPERATURE PROGRAMMED;

PALLADIUM;

EID: 84946945198     PISSN: 07437463     EISSN: 15205827     Source Type: Journal    
DOI: 10.1021/acs.langmuir.5b03386     Document Type: Article

References (54)

1. Wasserscheid, P.; Welton, T. Ionic Liquids in Synthesis; Wiley-VCH: New York, 2007.
2. Wasserscheid, P.; Stark, A. Handbook of Green Chemistry-Green Solvents, Vol. 6, Ionic Liquids; Wiley-VCH: New York, 2013.
3. Torimoto, T.; Okazaki, K.; Kiyama, T.; Hirahara, K.; Tanaka, N.; Kuwabata, S. Sputter deposition onto ionic liquids: Simple and clean synthesis of highly dispersed ultrafine metal nanoparticles Appl. Phys. Lett. 2006, 89 (24) 243117 10.1063/1.2404975
4. Mertens, S. F. L.; Vollmer, C.; Held, A.; Aguirre, M. H.; Walter, M.; Janiak, C.; Wandlowski, T. ″Ligand-Free″ Cluster Quantized Charging in an Ionic Liquid Angew. Chem., Int. Ed. 2011, 50 (41) 9735-9738 10.1002/anie.201104381
5. Vollmer, C.; Janiak, C. Naked metal nanoparticles from metal carbonyls in ionic liquids: Easy synthesis and stabilization Coord. Chem. Rev. 2011, 255 (17-18) 2039-2057 10.1016/j.ccr.2011.03.005
6. Scholten, J. D.; Leal, B. C.; Dupont, J. Transition Metal Nanoparticle Catalysis in Ionic Liquids ACS Catal. 2012, 2 (1) 184-200 10.1021/cs200525e
7. Dupont, J.; Scholten, J. D. On the structural and surface properties of transition-metal nanoparticles in ionic liquids Chem. Soc. Rev. 2010, 39 (5) 1780-1804 10.1039/b822551f
8. Dupont, J.; Meneghetti, M. R. On the stabilisation and surface properties of soluble transition-metal nanoparticles in non-functionalised imidazolium-based ionic liquids Curr. Opin. Colloid Interface Sci. 2013, 18 (1) 54-60 10.1016/j.cocis.2012.12.001
9. Hirano, M.; Enokida, K.; Okazaki, K.; Kuwabata, S.; Yoshida, H.; Torimoto, T. Composition-dependent electrocatalytic activity of AuPd alloy nanoparticles prepared via simultaneous sputter deposition into an ionic liquid Phys. Chem. Chem. Phys. 2013, 15 (19) 7286-7294 10.1039/c3cp50816a
10. Ghasemi, S.; Setayesh, S. R.; Habibi-Yangjeh, A.; Hormozi-Nezhad, M. R.; Gholami, M. R. Assembly of CeO2-TiO2 nanoparticles prepared in room temperature ionic liquid on graphene nanosheets for photocatalytic degradation of pollutants J. Hazard. Mater. 2012, 199, 170-178 10.1016/j.jhazmat.2011.10.080
11. Goharshadi, E. K.; Samiee, S.; Nancarrow, P. Fabrication of cerium oxide nanoparticles: Characterization and optical properties J. Colloid Interface Sci. 2011, 356 (2) 473-480 10.1016/j.jcis.2011.01.063
12. Kaper, H.; Endres, F.; Djerdj, I.; Antonietti, M.; Smarsly, B. M.; Maier, J.; Hu, Y. S. Direct low-temperature synthesis of rutile nanostructures in ionic liquids Small 2007, 3 (10) 1753-1763 10.1002/smll.200700138
13. Li, Z. X.; Li, L. L.; Yuan, Q.; Feng, W.; Xu, J.; Sun, L. D.; Song, W. G.; Yan, C. H. Sustainable and Facile Route to Nearly Monodisperse Spherical Aggregates of CeO(2) Nanocrystals with Ionic Liquids and Their Catalytic Activities for CO Oxidation J. Phys. Chem. C 2008, 112 (47) 18405-18411 10.1021/jp807348n
14. Schliehe, C.; Yuan, J.; Glatzel, S.; Siemensmeyer, K.; Kiefer, K.; Giordano, C. Iron Nitride and Carbide: from Crystalline Nanoparticles to Stable Aqueous Dispersions Chem. Mater. 2012, 24 (14) 2716-2721 10.1021/cm3007342
15. Jiang, Y.; Zhu, Y.-J. J. Phys. Chem. B 2005, 109, 4361 10.1021/jp044350+
16. Khare, V.; Kraupner, A.; Mantion, A.; Jelicic, A.; Thunemann, A. F.; Giordano, C.; Taubert, A. Stable Iron Carbide Nanoparticle Dispersions in [Emim][SCN] and [Emim][N(CN)(2)] Ionic Liquids Langmuir 2010, 26 (13) 10600-10605 10.1021/la100775m
17. Parnham, E. R.; Morris, R. E. Ionothermal synthesis of zeolites, metal-organic frameworks, and inorganic-organic hybrids Acc. Chem. Res. 2007, 40 (10) 1005-1013 10.1021/ar700025k
18. Richter, K.; Birkner, A.; Mudring, A. V. Stabilizer-Free Metal Nanoparticles and Metal Metal Oxide Nanocomposites with Long-Term Stability Prepared by Physical Vapor Deposition into Ionic Liquids Angew. Chem., Int. Ed. 2010, 49 (13) 2431-2435 10.1002/anie.200901562
19. Steinruck, H. P. Surface science goes liquid ! Surf. Sci. 2010, 604 (5-6) 481-484 10.1016/j.susc.2009.12.033
20. Steinruck, H. P.; Libuda, J.; Wasserscheid, P.; Cremer, T.; Kolbeck, C.; Laurin, M.; Maier, F.; Sobota, M.; Schulz, P. S.; Stark, M. Surface Science and Model Catalysis with Ionic Liquid-Modified Materials Adv. Mater. 2011, 23 (22-23) 2571-2587 10.1002/adma.201100211
21. Uhl, B.; Buchner, F.; Gabler, S.; Bozorgchenani, M.; Behm, R. J. Adsorption and reaction of sub-monolayer films of an ionic liquid on Cu(111) Chem. Commun. 2014, 50 (62) 8601-8604 10.1039/C4CC03203A
22. Uhl, B.; Cremer, T.; Roos, M.; Maier, F.; Steinruck, H. P.; Behm, J. At the ionic liquid|metal interface: structure formation and temperature dependent behavior of an ionic liquid adlayer on Au(111) Phys. Chem. Chem. Phys. 2013, 15 (40) 17295-17302 10.1039/c3cp52184b
23. Carstens, T.; Gustus, R.; Hofft, O.; Borisenko, N.; Endres, F.; Li, H.; Wood, R. J.; Page, A. J.; Atkin, R. Combined STM, AFM, and DFT Study of the Highly Ordered Pyrolytic Graphite/1-Octyl-3-methyl-imidazolium Bis(trifluoromethylsulfonyl)imide Interface J. Phys. Chem. C 2014, 118 (20) 10833-10843 10.1021/jp501260t
24. Carstens, T.; Hayes, R.; El Abedin, S. Z.; Corr, B.; Webber, G. B.; Borisenko, N.; Atkin, R.; Endres, F. In situ STM, AFM and DTS study of the interface 1-hexyl-3-methylimidazolium tris(pentafluoroethyl)trifluorophosphate/Au(111) Electrochim. Acta 2012, 82, 48-59 10.1016/j.electacta.2012.01.111
25. Borisenko, N.; El Abedin, S. Z.; Endres, F. In situ STM investigation of gold reconstruction and of silicon electrodeposition on Au(111) in the room temperature ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide J. Phys. Chem. B 2006, 110 (12) 6250-6256 10.1021/jp057337d
26. Maier, F.; Gottfried, J. M.; Rossa, J.; Gerhard, D.; Schulz, P. S.; Schwieger, W.; Wasserscheid, P.; Steinruck, H. P. Surface enrichment and depletion effects of ions dissolved in an ionic liquid: an X-ray photoelectron spectroscopy study Angew. Chem., Int. Ed. 2006, 45 (46) 7778-7780 10.1002/anie.200602756
27. Sobota, M.; Nikiforidis, I.; Hieringer, W.; Paape, N.; Happel, M.; Steinruck, H. P.; Gorling, A.; Wasserscheid, P.; Laurin, M.; Libuda, J. Toward Ionic-Liquid-Based Model Catalysis: Growth, Orientation, Conformation, and Interaction Mechanism of the [Tf2N](-) Anion in [BMIM][Tf2N] Thin Films on a Well-Ordered Alumina Surface Langmuir 2010, 26 (10) 7199-7207 10.1021/la904319h
28. Sobota, M.; Schmid, M.; Happel, M.; Amende, M.; Maier, F.; Steinruck, H. P.; Paape, N.; Wasserscheid, P.; Laurin, M.; Gottfried, J. M.; Libuda, J. Ionic liquid based model catalysis: interaction of [BMIM][Tf2N] with Pd nanoparticles supported on an ordered alumina film Phys. Chem. Chem. Phys. 2010, 12 (35) 10610-10621 10.1039/c003753b
29. Cremer, T.; Stark, M.; Deyko, A.; Steinruck, H. P.; Maier, F. Liquid/Solid Interface of Ultrathin Ionic Liquid Films: [C(1)C(1)lm][Tf2N] and [C(8)C(1)Im][Tf2N) on Au(111) Langmuir 2011, 27 (7) 3662-3671 10.1021/la105007c
30. Cremer, T.; Wibmer, L.; Calderon, S. K.; Deyko, A.; Maier, F.; Steinruck, H. P. Interfaces of ionic liquids and transition metal surfaces-adsorption, growth, and thermal reactions of ultrathin [C(1)C(1)Im][Tf2N] films on metallic and oxidised Ni(111) surfaces Phys. Chem. Chem. Phys. 2012, 14 (15) 5153-5163 10.1039/c2cp40278e
31. Schernich, S.; Kostyshyn, D.; Wagner, V.; Taccardi, N.; Laurin, M.; Wasserscheid, P.; Libuda, J. Interactions Between the Room-Temperature Ionic Liquid [C(2)C(1)Im][OTf] and Pd(111), Well-Ordered Al2O3, and Supported Pd Model Catalysts from IR Spectroscopy J. Phys. Chem. C 2014, 118 (6) 3188-3193 10.1021/jp5006692
32. Schernich, S.; Laurin, M.; Lykhach, Y.; Steinruck, H. P.; Tsud, N.; Skala, T.; Prince, K. C.; Taccardi, N.; Matolin, V.; Wasserscheid, P.; Libuda, J. Functionalization of Oxide Surfaces through Reaction with 1,3-Dialkylimidazolium Ionic Liquids J. Phys. Chem. Lett. 2013, 4 (1) 30-35 10.1021/jz301856a
33. Schernich, S.; Wagner, V.; Taccardi, N.; Wasserscheid, P.; Laurin, M.; Libuda, J. Interface Controls Spontaneous Crystallization in Thin Films of the Ionic Liquid [C(2)C(1)Im][OTf] on Atomically Clean Pd(111) Langmuir 2014, 30 (23) 6846-6851 10.1021/la500842c
34. Smith, E. F.; Rutten, F. J. M.; Villar-Garcia, I. J.; Briggs, D.; Licence, P. Ionic liquids in vacuo: Analysis of liquid surfaces using ultra-high-vacuum techniques Langmuir 2006, 22 (22) 9386-9392 10.1021/la061248q
35. Smith, E. F.; Villar Garcia, I. J.; Briggs, D.; Licence, P. Ionic liquids in vacuo; solution-phase X-ray photoelectron spectroscopy Chem. Commun. 2005, 45, 5633-5635 10.1039/b512311a
36. Zhang, G. P.; Zhou, H. H.; An, C. L.; Liu, D.; Huang, Z. Y.; Kuang, Y. F. Bimetallic palladium-gold nanoparticles synthesized in ionic liquid microemulsion Colloid Polym. Sci. 2012, 290 (14) 1435-1441 10.1007/s00396-012-2670-6
37. Zhang, G. P.; Zhou, H. H.; Hu, J. Q.; Liu, M.; Kuang, Y. F. Pd nanoparticles catalyzed ligand-free Heck reaction in ionic liquid microemulsion Green Chem. 2009, 11 (9) 1428-1432 10.1039/b822521d
38. Wender, H.; Migowski, P.; Feil, A. F.; Teixeira, S. R.; Dupont, J. Sputtering deposition of nanoparticles onto liquid substrates: Recent advances and future trends Coord. Chem. Rev. 2013, 257 (17-18) 2468-2483 10.1016/j.ccr.2013.01.013
39. Mehl, S.; Bauer, T.; Brummel, O.; Wasserscheid, P.; Libuda, J. Unpublished, 2015.
40. Akai, N.; Kawai, A.; Shibuya, K. Ion-Pair Structure of Vaporized Ionic Liquid Studied by Matrix-Isolation FTIR Spectroscopy with DFT Calculations: A Case of 1-Ethyl-3-methylimidazolium Trifluoromethanesulfonate J. Phys. Chem. A 2010, 114 (48) 12662-12666 10.1021/jp108209q
41. Gejji, S. P.; Hermansson, K.; Lindgren, J. Abinitio Vibrational Frequencies of the Triflate Ion, (Cf3so3)- J. Phys. Chem. 1993, 97 (15) 3712-3715 10.1021/j100117a014
42. Souda, R. Phase Transition of 1-Ethyl-3-Methylimidazolium Bis(trifluoromethylsulfonyl)imide Thin Films on Highly Oriented Pyrolytic Graphite J. Phys. Chem. B 2009, 113 (39) 12973-12977 10.1021/jp9049439
43. Choudhury, A. R.; Winterton, N.; Steiner, A.; Cooper, A. I.; Johnson, K. A. In situ crystallization of ionic liquids with melting points below-25 degrees C CrystEngComm 2006, 8 (10) 742-745 10.1039/b609598d
44. Hoffmann, F. M. Surf. Sci. Rep. 1983, 3, 107 10.1016/0167-5729(83)90001-8
45. Frank, M.; Baumer, M.; Kuhnemuth, R.; Freund, H. J. Metal atoms and particles on oxide supports: Probing structure and charge by infrared spectroscopy J. Phys. Chem. B 2001, 105 (36) 8569-8576 10.1021/jp010724c
46. Bertarione, S.; Scarano, D.; Zecchina, A.; Johanek, V.; Hoffmann, J.; Schauermann, S.; Frank, M. M.; Libuda, J.; Rupprechter, G.; Freund, H. J. Surface reactivity of Pd nanoparticles supported on polycrystalline substrates as compared to thin film model catalysts: Infrared study of CO adsorption J. Phys. Chem. B 2004, 108 (11) 3603-3613 10.1021/jp036718t
47. Bradshaw, A. M.; Hoffmann, F. M. Surf. Sci. 1978, 72, 513 10.1016/0039-6028(78)90367-9
48. Yudanov, I. V.; Sahnoun, R.; Neyman, K. M.; Rosch, N.; Hoffmann, J.; Schauermann, S.; Johanek, V.; Unterhalt, H.; Rupprechter, G.; Libuda, J.; Freund, H. J. CO adsorption on Pd nanoparticles: Density functional and vibrational spectroscopy studies J. Phys. Chem. B 2003, 107 (1) 255-264 10.1021/jp022052b
49. Szanyi, J.; Kuhn, W. K.; Goodman, D. W. Co Adsorption on Pd(111) and Pd(100)-Low and High-Pressure Correlations J. Vac. Sci. Technol., A 1993, 11 (4) 1969-1974 10.1116/1.578532
50. Kuhn, W. K.; Szanyi, J.; Goodman, D. W. Co Adsorption on Pd(111)-the Effects of Temperature and Pressure Surf. Sci. 1992, 274 (3) L611-L618 10.1016/0039-6028(92)90834-S
51. Koel, B. E.; Sellidj, A.; Paffett, M. T. Ultrathin Films of Pd on Au(111)-Evidence for Surface Alloy Formation Phys. Rev. B: Condens. Matter Mater. Phys. 1992, 46 (12) 7846-7856 10.1103/PhysRevB.46.7846
52. Hollins, P. The Influence of Surface-Defects on the Infrared-Spectra of Adsorbed Species Surf. Sci. Rep. 1992, 16 (2) 51-94 10.1016/0167-5729(92)90008-Y
53. Ma, Y. S.; Diemant, T.; Bansmann, J.; Behm, R. J. The interaction of CO with PdAg/Pd(111) surface alloys-A case study of ensemble effects on a bimetallic surface Phys. Chem. Chem. Phys. 2011, 13 (22) 10741-10754 10.1039/c1cp00009h
54. Pancotti, A.; Nascente, P. A. P.; de Siervo, A.; Landers, R.; Carazzolle, M. F.; Tallarico, D. A.; Kleiman, G. G. Characterization of Ultra-Thin Films of Pd Deposited on Au(111) Top. Catal. 2011, 54 (1-4) 70-76 10.1007/s11244-011-9649-2