Improving Electrodeposition of Mg through an Open Circuit Potential Hold

Journal of Physical Chemistry C

Volumn 119, Issue 41, 2015, Pages 23366-23372

  Esbenshade, Jennifer L ^a   Barile, Christopher J ^a   Fister, Timothy T ^b   Bassett, Kimberly L ^a   Fenter, Paul ^b   Nuzzo, Ralph G ^a   Gewirth, Andrew A ^a  

^a UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

^b ARGONNE NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DEPOSITION; DEPOSITS; ELECTRODEPOSITION; X RAY DIFFRACTION; X RAY PHOTOELECTRON SPECTROSCOPY;

ELECTROCHEMICAL METHODS; ELECTRODE SURFACES; ENHANCEMENT LAYERS; IN-SITU X-RAY DIFFRACTION; OPEN CIRCUIT POTENTIAL; OVER POTENTIAL; POLYCRYSTALLINE; STRIPPING KINETICS;

ELECTRODES;

EID: 84944411451     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/acs.jpcc.5b07825     Document Type: Article

References (38)

1. Saha, P.; Datta, M. K.; Velikokhatnyi, O. I.; Manivannan, A.; Alman, D.; Kumta, P. N. Rechargeable magnesium battery: Current status and key challenges for the future Prog. Mater. Sci. 2014, 66, 1-86 10.1016/j.pmatsci.2014.04.001
2. Aurbach, D.; Lu, Z.; Schechter, A.; Gofer, Y.; Gizbar, H.; Turgeman, R.; Cohen, Y.; Moshkovich, M.; Levi, E. Prototype systems for rechargeable magnesium batteries Nature 2000, 407, 724-727 10.1038/35037553
3. Muldoon, J.; Bucur, C. B.; Gregory, T. Quest for nonaqueous multivalent secondary batteries: magnesium and beyond Chem. Rev. 2014, 114, 11683-11720 10.1021/cr500049y
4. Witte, F. The history of biodegradable magnesium implants: A review Acta Biomater. 2010, 6, 1680-1692 10.1016/j.actbio.2010.02.028
5. Besenhard, J. O.; Winter, M. Advances in battery technology: Rechargeable magnesium batteries and novel negative-electrode materials for lithium ion batteries ChemPhysChem 2002, 3, 155 10.1002/1439-7641(20020215)3:2<155::AID-CPHC155>3.0.CO;2-S
6. Muldoon, J.; Bucur, C. B.; Oliver, A. G.; Sugimoto, T.; Matsui, M.; Kim, H. S.; Allred, G. D.; Zajicek, J.; Kotani, Y. Electrolyte roadblocks to a magnesium rechargeable battery Energy Environ. Sci. 2012, 5, 5941-5950 10.1039/c2ee03029b
7. Amir, N.; Vestfrid, Y.; Chusid, O.; Gofer, Y.; Aurbach, D. Progress in nonaqueous magnesium electrochemistry J. Power Sources 2007, 174, 1234-1240 10.1016/j.jpowsour.2007.06.206
8. Levi, E.; Gofer, Y.; Aurbach, D. On the way to techargeable mg batteries: The challenge of new cathode materials Chem. Mater. 2010, 22, 860-868 10.1021/cm9016497
9. Shterenberg, I.; Salama, M.; Gofer, Y.; Levi, E.; Aurbach, D. The challenge of developing rechargeable magnesium batteries MRS Bull. 2014, 39, 453-460 10.1557/mrs.2014.61
10. Aurbach, D.; Gofer, Y.; Lu, Z.; Schechter, A.; Chusid, O.; Gizbar, H.; Cohen, Y.; Ashkenazi, V.; Moshkovich, M.; Turgeman, R. A short review on the comparison between Li battery systems and rechargeable magnesium battery technology J. Power Sources 2001, 97, 28-32 10.1016/S0378-7753(01)00585-7
11. Vardar, G.; Sleightholme, A. E. S.; Naruse, J.; Hiramatsu, H.; Siegel, D. J.; Monroe, C. W. Electrochemistry of magnesium electrolytes in ionic liquids for secondary batteries ACS Appl. Mater. Interfaces 2014, 6, 18033-18039 10.1021/am5049064
12. Gregory, T. D.; Hoffman, R. J.; Winterton, R. C. Nonaqueous electrochemistry of magnesium- applications to energy storage J. Electrochem. Soc. 1990, 137 (3) 775-780 10.1149/1.2086553
13. Aurbach, D.; Moshkovich, M.; Schechter, A.; Turgeman, R. Magnesium deposition and dissolution processes in ethereal grignard salt solutions using simultaneous EQCM-EIS and in situ FTIR spectroscopy Electrochem. Solid-State Lett. 2000, 3, 31-34 10.1149/1.1390949
14. Barile, C. J.; Spatney, R.; Zavadil, K. R.; Gewirth, A. A. Investigating the reversibility of in situ generated magnesium organohaloalurninates for magnesium deposition and dissolution J. Phys. Chem. C 2014, 118, 10694-10699 10.1021/jp503506c
15. Mizrahi, O.; Amir, N.; Pollak, E.; Chusid, O.; Marks, V.; Gottlieb, H.; Larush, L.; Zinigrad, E.; Aurbach, D. Electrolyte solutions with a wide electrochemical window for recharge magnesium batteries J. Electrochem. Soc. 2008, 155, A103-A109 10.1149/1.2806175
16. Yoo, H. D.; Shterenberg, I.; Gofer, Y.; Gershinsky, G.; Pour, N.; Aurbach, D. Mg rechargeable batteries: an on-going challenge Energy Environ. Sci. 2013, 6, 2265-2279 10.1039/c3ee40871j
17. Doe, R. E.; Han, R.; Hwang, J.; Gmitter, A. J.; Shterenberg, I.; Yoo, H. D.; Pour, N.; Aurbach, D. Novel, electrolyte solutions comprising fully inorganic salts with high anodic stability for rechargeable magnesium batteries Chem. Commun. 2014, 50, 243-245 10.1039/C3CC47896C
18. Barile, C. J.; Barile, E. C.; Zavadil, K. R.; Nuzzo, R. G.; Gewirth, A. A. Electrolytic conditioning of a magnesium aluminum chloride complex for reversible magnesium deposition J. Phys. Chem. C 2014, 118, 27623-27630 10.1021/jp506951b
19. Barile, C. J.; Nuzzo, R. G.; Gewirth, A. A. Exploring salt and solvent effects in chloride-based electrolytes for magnesium electrodeposition and dissolution J. Phys. Chem. C 2015, 119, 13524-13534 10.1021/acs.jpcc.5b03508
20. Liao, C.; Guo, B. K.; Jiang, D. E.; Custelcean, R.; Mahurin, S. M.; Sun, X. G.; Dai, S. Highly soluble alkoxide magnesium salts for rechargeable magnesium batteries J. Mater. Chem. A 2014, 2, 581-584 10.1039/C3TA13691D
21. Kim, I. T.; Yamabuki, K.; Morita, M.; Tsutsumi, H.; Yoshimoto, N. Effects of alkoxide addition on the electrochemical deposition and dissolution in triglyme-based solution dissolving magnesium bis(trifluoromethanesulfonyl)amide J. Power Sources 2015, 278, 340-343 10.1016/j.jpowsour.2014.12.089
22. Ha, S. Y.; Lee, Y. W.; Woo, S. W.; Koo, B.; Kim, J. S.; Cho, J.; Lee, K. T.; Choi, N. S. Magnesium(II) Bis(trifluoromethane sulfonyl) imide-based electrolytes with wide electrochemical windows for rechargeable magnesium batteries ACS Appl. Mater. Interfaces 2014, 6, 4063-4073 10.1021/am405619v
23. Pan, B. F.; Zhang, J. J.; Huang, J. H.; Vaughey, J. T.; Zhang, L.; Han, S. D.; Burrell, A. K.; Zhang, Z. C.; Liao, C. A Lewis acid-free and phenolate-based magnesium electrolyte for rechargeable magnesium batteries Chem. Commun. 2015, 51, 6214-6217 10.1039/C5CC01225B
24. Tutusaus, O.; Mohtadi, R.; Arthur, T. S.; Mizuno, F.; Nelson, E. G.; Sevryugina, Y. V. An efficient halogen-free electrolyte for use in rechargeable magnesium batteries Angew. Chem., Int. Ed. 2015, 127, 8011-8015 10.1002/ange.201412202
25. Viestfrid, Y.; Levi, M. D.; Gofer, Y.; Aurbach, D. Microelectrode studies of reversible Mg deposition in THF solutions containing complexes of alkylaluminum chlorides and dialkylmagnesium J. Electroanal. Chem. 2005, 576, 183-195 10.1016/j.jelechem.2004.09.034
26. Schlesinger, M.; Paunovic, M. Modern electroplating; http://site.ebrary.com/id/10510261 (accessed May 29, 2015).
27. Shao, W.; Pattanaik, G.; Zangari, G. Influence of chloride anions on the mechanism of copper electrodeposition from acidic sulfate electrolytes J. Electrochem. Soc. 2007, 154, D201-D207 10.1149/1.2434682
28. Rappoport, Z.; Marek, I. The Chemistry of Organomagnesium Compounds; J. Wiley: Chichester, UK, 2008.
29. Zhang, R.; Arthur, T. S.; Ling, C.; Mizuno, F. Manganese dioxides as rechargeable magnesium battery cathode; synthetic approach to understand magnesiation process J. Power Sources 2015, 282, 630-638 10.1016/j.jpowsour.2015.02.067
30. Arthur, T. S.; Glans, P. A.; Matsui, M.; Zhang, R. G.; Ma, B. W.; Guo, J. H. Mg deposition observed by in situ electrochemical Mg K-edge X-ray absorption spectroscopy Electrochem. Commun. 2012, 24, 43-46 10.1016/j.elecom.2012.08.018
31. Benmayza, A.; Ramanathan, M.; Arthur, T. S.; Matsui, M.; Mizuno, F.; Guo, J. H.; Glans, P. A.; Prakash, J. Effect of electrolytic properties of a magnesium organohaloaluminate electrolyte on magnesium deposition J. Phys. Chem. C 2013, 117, 26881-26888 10.1021/jp4077068
32. Gofer, Y.; Pour, N.; Aurbach, D. Electrolytic solutions for rechargeable magnesium batteries Lithium Batteries: Advanced Technologies and Applications 2013, 327-347 10.1002/9781118615515.ch15
33. Fister, T. T.; Esbenshade, J.; Chen, X.; Long, B. R.; Shi, B.; Schleputz, C. M.; Gewirth, A. A.; Bedzyk, M. J.; Fenter, P. Lithium intercalation behavior in multilayer silicon electrodes Adv. Energy Mater. 2014, 10.1002/aenm.201301494
34. Raynor, G.; Rothery, W. H. A technique for the X-ray powder photography of reactive metals and alloys, with special reference to the lattice spacing of magnesium at high temperatures J. Inst. Met. 1939, 65, 379
35. Watts, J. F.; Wolstenholme, J. An Introduction to Surface Analysis by XPS and AES; Wiley: New York, 2003.
36. Kongstein, O. E.; Haarberg, G. M.; Thonstad, J. Current efficiency and kinetics of cobalt electrodeposition in acid chloride solutions. Part II: The influence of chloride and sulphate concentrations J. Appl. Electrochem. 2007, 37, 675-680 10.1007/s10800-007-9298-0
37. Hill, C. L.; Vander Sande, J. B.; Whitesides, G. M. Mechanism of formation of Grignard reagents. Corrosion of metallic magnesium by alkyl halides in ethers J. Org. Chem. 1980, 45, 1020-1028 10.1021/jo01294a021
38. Wetzel, D. J.; Malone, M. A.; Haasch, R. T.; Meng, Y.; Vieker, H.; Hahn, N. T.; Golzhauser, A.; Zuo, J.-M.; Zavadil, K. R.; Gewirth, A. A. Passivation dynamics in the anisotropic deposition and stripping of bulk magnesium electrodes during electrochemical cycling ACS Appl. Mater. Interfaces 2015, 7, 18406 10.1021/acsami.5b04487