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2 evolution. The mixture was heated gradually to 200 °C where it was kept for 5 h before being successfully brought to 800 °C. It was kept at 800 °C for 8 h. A red glassy ingot was obtained by cooling at a rate of 40 °C/h to room temperature; method
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85099670707
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-4 Torr) in a 13 mm (OD) carbon coated fused-silica tube and heated (80 °C/h) to 800 °C. It was kept there for 24 h, followed by cooling to room temperature at 40 °C/h; method
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6 based on EDS analyses. The product is a red ingot
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2S (1 mmol, 0.2205 g), S (5 mmol, 0.1620 g), Sn (1 mmol, 0.1187 g), and Sb (2 mmol, 0.2435 g) in accordance to the conditions and heating profile for the synthesis compound 1; method
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85042978006
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