Nanoporous Intergrowths: How Crystal Growth Dictates Phase Composition and Hierarchical Structure in the CHA/AEI System

Chemistry of Materials

Volumn 27, Issue 12, 2015, Pages 4205-4215

  Smith, Rachel L ^a   Sawiński, Wojciech A ^b   Lind, Anna ^c   Wragg, David S ^b   Cavka, Jasmina H ^c   Arstad, Bjørnar ^c   Fjellvag, Helmer ^b   Attfield, Martin P ^a   Akporiaye, Duncan ^c   Anderson, Michael W ^a  

^a UNIVERSITY OF MANCHESTER   (United Kingdom)

^b UNIVERSITY OF OSLO   (Norway)

^c SINTEF MATERIALS AND CHEMISTRY   (Norway)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMIC FORCE MICROSCOPY; CRYSTAL GROWTH; CRYSTAL STRUCTURE; DISLOCATIONS (CRYSTALS); GROWTH (MATERIALS); PHASE COMPOSITION; POROUS MATERIALS; SCREW DISLOCATIONS; X RAY DIFFRACTION ANALYSIS;

COMPETING MECHANISMS; CRYSTAL GROWTH MECHANISM; HIERARCHICAL STRUCTURES; INTERGROWTH STRUCTURE; LAYER STACKING SEQUENCE; NANO-POROUS MATERIALS; SPECIFIC PROPERTIES; STRUCTURE/PROPERTY RELATIONSHIPS;

CRYSTAL ATOMIC STRUCTURE;

EID: 84934995159     PISSN: 08974756     EISSN: 15205002     Source Type: Journal    
DOI: 10.1021/cm504284x     Document Type: Article

References (55)

1. Chen, J. Q.; Bozzano, A.; Glover, B.; Fuglerud, T.; Kvisle, S. Recent advancements in ethylene and propylene production using the UOP/Hydro MTO process Catal. Today 2005, 106, 103-107
2. Vora, B. V.; Marker, T. L.; Barger, P. T.; Nilsen, H. R.; Kvisle, S.; Fuglerud, T. Economic route for natural gas conversion to ethylene and propylene Stud. Surf. Sci. Catal. 1997, 107, 87-98
3. Chen, D.; Moljord, K.; Holmen, A. A methanol to olefins review: Diffusion, coke formation and deactivation on SAPO type catalysts Microporous Mesoporous Mater. 2012, 164, 239-250
4. Djieugoue, M.-A.; Prakash, A. M.; Kevan, L. Catalytic Study of Methanol-to-Olefins Conversion in Four Small-Pore Silicoaluminophosphate Molecular Sieves: Influence of the Structural Type, Nickel Incorporation, Nickel Location, and Nickel Concentration J. Phys. Chem. B 2000, 104, 6452-6461
5. Aguayo, A. T.; Gayubo, A. G.; Vivanco, R.; Olazar, M.; Bilbao, J. Role of acidity and microporous structure in alternative catalysts for the transformation of methanol into olefins Appl. Catal., A 2005, 283, 197-207
6. Wendlebo, R.; Akporiaye, D. E.; Anderson, A.; Dahl, M. I.; Mostad, H. B.; Fuglerud, T.; Kvisle, S. Microporous crystalline silico-alumino-phosphate composition, catalytic material comprising said composition and use of these for production of olefins from methanol. U.S. Patent 6,334,994, Jan 1, 2002.
7. Sinkler, W.; Broach, R. W.; Erdman, N.; Reynolds, T. M.; Chen, J. Q.; Wilson, S. T.; Barger, P. T. Enhancement of molecular sieve performance. U.S. Patent 7,547,812, June 16, 2009.
8. Mertens, M. M. Synthesis and use of aei structure-type molecular sieves. WO 2009/117186, Feb 6, 2009.
9. Lok, B. M.; Messina, C. A.; Patton, R. L.; Gajek, R. T.; Cannan, T. R.; Flanigen, E. M. Silicoaluminophosphate molecular sieves: another new class of microporous crystalline inorganic solids J. Am. Chem. Soc. 1984, 106, 6092-6093
10. Chen, J. S.; Thomas, J. M.; Wright, P. A.; Townsend, R. P. Silicoaluminophosphate number eighteen (SAPO-18): a new microporous solid acid catalyst Catal. Lett. 1994, 28, 241-248
11. Treacy, M. M. J.; Newsam, J. M.; Deem, M. W. A General Recursion Method for Calculating Diffracted Intensities from Crystals Containing Planar Faults Proc. R. Soc. London A 1991, 433, 499-520
12. Leoni, M.; Gualtieri, A. F.; Roveri, N. Simultaneous refinement of structure and microstructure of layered materials J. Appl. Crystallogr. 2004, 37, 166-173
13. Janssen, M. J. G.; Fung, S. C.; Verberckmoes, A.; Mertens, M. M.; Mortier, W. J. Silicoaluminophosphate molecular sieve. WO 02/070407, Feb 4, 2002.
14. Mertens, M. M.; Verberckmoes, A.; Janssen, M. J.; Chang, Y. F.; Martens, L. R. M.; Vaughn, S. N.; Clem, K. R.; Mortier, W. J. Crystalline intergrowth material of silicoaluminophosphate having two intergrown phases. U.S. Patent 7,914,760, March 29, 2011.
15. Lillerud, K. P.; Akporiaye, D. Systematic Relationships Between the Structures of CHA, AEI and KFI Stud. Surf. Sci. Catal. 1994, 84, 543-550
16. Terasaki, O.; Ohsuna, T.; Alfredsson, V.; Bovin, J.-O.; Watanabe, D.; Carr, S. W.; Anderson, M. W. Observation of spatially correlated intergrowths of faujasitic polytypes and the pure end members by high-resolution electron microscopy Chem. Mater. 1993, 5, 452-458
17. Hanif, N.; Anderson, M. W.; Alfredsson, V.; Terasaki, O. The effect of stirring on the synthesis of intergrowths of zeolite Y polymorphs Phys. Chem. Chem. Phys. 2000, 2, 3349-3357
18. awiński, W. A.; Wragg, D. S.; Akporiaye, D.; Fjellvag, H. Intergrowth structure modelling in silicoaluminophosphate SAPO-18/34 family Microporous Mesoporous Mater. 2014, 195, 311-318
19. Anderson, M. W.; Pachis, K. S.; Prébin, F.; Carr, S. W.; Terasaki, O.; Ohsuna, T.; Alfreddson, V. Intergrowths of cubic and hexagonal polytypes of faujasitic zeolites J. Chem. Soc., Chem. Commun. 1991, 1660-1664
20. Binning, G.; Quate, C. F.; Gerber, Ch. Atomic Force Microscope Phys. Rev. Lett. 1986, 56, 930-933
21. John, N. S.; Stevens, S. M.; Terasaki, O.; Anderson, M. W. Evolution of Surface Morphology with Introduction of Stacking Faults in Zeolites Chem. Eur. J. 2010, 16, 2220-2230
22. González, G.; Stracke, W.; Lopez, Z.; Keller, U.; Ricker, A.; Reichelt, R. Characterization of Defects and Surface Structures in Microporous Materials by HRTEM, HRSEM, and AFM Microsc. Microanal. 2004, 10, 224-235
23. Vomscheid, R.; Briend, M.; Peltre, M. J.; Man, P. P.; Barthomeuf, D. The Role of the Template in Directing the Si Distribution in SAPO Zeolites J. Phys. Chem. 1994, 98, 9614-9618
24. Zibrowius, B.; Löffler, E.; Hunger, M. Multinuclear MAS n.m.r. and i.r. spectroscopic study of silicon incorporation into SAPO-5, SAPO-31, and SAPO-34 molecular sieves Zeolites 1992, 12, 167-174
25. Tan, J.; Liu, Z.; Bao, X.; Liu, X.; Han, X.; He, C.; Zhai, R. Crystallization and Si incorporation mechanisms of SAPO-34 Microporous Mesoporous Mater. 2002, 53, 97-108
26. Xu, L.; Du, A.; Wei, Y.; Wang, Y.; Yu, Z.; He, Y.; Zhang, X.; Liu, Z. Synthesis of SAPO-34 with only Si (4Al) species: Effect of Si contents on Si incorporation mechanism and Si coordination environment of SAPO-34 Microporous Mesoporous Mater. 2008, 115, 332-337
27. Martens, J. A.; Xiong, Y. L.; Feijen, J. P.; Grobet, P. J.; Jacobs, P. A. Phase discrimination with 29Si MAS NMR in EMT/FAU zeolite intergrowths J. Phys. Chem. 1993, 97, 5132-5135
28. Feijen, E. J. P.; Reynders, R. A.; Geerts, H.; Martens, J. A.; Grobet, P. J.; Jacobs, P. A. Use of 13C CP NMR spectroscopy for the quantification of FAU/EMT zeolite intergrowths synthesized with 15-crown-5 and 18-crown-6 ethers J. Phys. Chem. 1995, 99, 1837-1839
29. Proffen, T.; Neder, R. B. DISCUS: a program for diffuse scattering and defect-structure simulation Appl. Crystallogr. 1997, 30, 171-175
30. Neder, R. B.; Proffen, T. Diffuse Scattering and Defect Structure Simulations; Oxford University Press: Oxford, 2008.
31. Price, K.; Storn, R. M.; Lampinen, J. A. Differential Evolution: A Practical Approach to Global Optimization; Springer: Amsterdam, The Netherlands, 2005.
32. He, H.; Klinowski, J. Solid-state NMR studies of the aluminophosphate molecular sieve AlPO4-18 J. Phys. Chem. 1993, 97, 10385-10388
33. Fan, D.; Tian, P.; Xu, S.; Xia, Q.; Su, X.; Zhang, L.; Zhang, Y.; He, Y.; Liu, Z. A novel solvothermal approach to synthesize SAPO molecular sieves using organic amines as the solvent and template J. Mater. Chem. 2012, 22, 6568-6574
34. Evans, D. J.; Leigh, G. J.; Macdonald, C. Carbon-13 and related NMR chemical shifts in alkylammonium and alkylphosphonium salts J. Magn. Reson. Chem. 1990, 28, 711-714
35. Wendelbo, R.; Akporiaye, D.; Andersen, A.; Dahl, I. M.; Mostad, H. B. Synthesis, characterization and catalytic testing of SAPO-18, MgAPO-18, and ZnAPO-18 in the MTO reaction Appl. Catal., A 1996, 142, L197-L207
36. Meza, L. I.; Anderson, M. W.; Agger, J. R. Differentiating fundamental structural units during the dissolution of zeolite A Chem. Commun. 2007, 2473-2475
37. Brent, R.; Anderson, M. W. Fundamental crystal growth mechanism in zeolite L revealed by atomic force microscopy Angew. Chem., Int. Ed. 2008, 47, 5327-5330
38. Meza, L. I.; Anderson, M. W.; Slater, B.; Agger, J. R. In situ atomic force microscopy of zeolite A dissolution Phys. Chem. Chem. Phys. 2008, 10, 5066-5076
39. Brent, R.; Cubillas, P.; Stevens, S. M.; Jelfs, K. E.; Umemura, A.; Gebbie, J. T.; Slater, B.; Terasaki, O.; Holden, M.; Anderson, M. W. Unstitching the Nanoscopic Mystery of Zeolite Crystal Formation J. Am. Chem. Soc. 2010, 132, 13858-13868
40. Holden, M.; Cubillas, P.; Anderson, M. W. In situ crystal growth of nanoporous zincophosphate observed by atomic force microscopy Chem. Commun. 2010, 46, 1047-1049
41. Cubillas, P.; Holden, M.; Anderson, M. W. Crystal Growth Studies on Microporous Zincophosphate-Faujasite Using Atomic Force Microscopy Cryst. Growth Des. 2011, 11, 3163-3171
42. Holden, M.; Cubillas, P.; Attfield, M. P.; Gebbie, J. T.; Anderson, M. W. Growth Mechanism of Microporous Zincophosphate Sodalite Revealed by In Situ Atomic Force Microscopy J. Am. Chem. Soc. 2012, 134, 13066-13073
43. Shöâeè, M.; Anderson, M. W.; Attfield, M. P. Crystal Growth of the Nanoporous Metal-Organic Framework HKUST-1 Revealed by In Situ Atomic Force Microscopy Angew. Chem., Int. Ed. 2008, 47, 8525-8528
44. John, N. S.; Scherb, C.; Shöâeè, M.; Anderson, M. W.; Attfield, M. P.; Bein, T. Single layer growth of sub-micron metal-organic framework crystals observed by in situ atomic force microscopy Chem. Commun. 2009, 6294-6296
45. Moh, P. Y.; Cubillas, P.; Anderson, M. W.; Attfield, M. P. Revelation of the Molecular Assembly of the Nanoporous Metal Organic Framework ZIF-8 J. Am. Chem. Soc. 2011, 113, 13304-13307
46. Cubillas, P.; Anderson, M. W.; Attfield, M. P. Crystal Growth Mechanisms and Morphological Control of the Prototypical Metal-Organic Framework MOF-5 Revealed by Atomic Force Microscopy Chem. Eur. J. 2012, 18, 15406-15415
47. Cubillas, P.; Anderson, M. W.; Attfield, M. P. Materials Discovery and Crystal Growth of Zeolite A Type Zeolitic-Imidazolate Frameworks Revealed by Atomic Force Microscopy Chem. Eur. J. 2013, 19, 8236-8243
48. Moh, P. Y.; Brenda, M.; Anderson, M. W.; Attfield, M. P. Crystallisation of solvothermally synthesised ZIF-8 investigated at the bulk, single crystal and surface level CrystEngComm 2013, 15, 9672-9678
49. Cubillas, P.; Anderson, M. W.; Attfield, M. P. Influence of Isomorphous Substituting Cobalt Ions on the Crystal Growth of the MOF-5 Framework Determined by Atomic Force Microscopy of Growing Core-Shell Crystals Cryst. Growth Des. 2013, 13, 4526-4532
50. Cubillas, P.; Etherington, K.; Anderson, M. W.; Attfield, M. P. Crystal growth of MOF-5 using secondary building units studied by in situ atomic force microscopy CrystEngComm 2014, 16, 9834-9841
51. Lupulescu, A. I.; Rimer, J. D. In Situ Imaging of Silicalite-1 Surface Growth Reveals the Mechanism of Crystallization Science 2014, 344, 729-732
52. Davis, T. M.; Drews, T. O.; Ramanan, H.; He, C.; Dong, J.; Schnablegger, H.; Katsoulakis, M. A.; Kokkoli, E.; McCormick, A. V.; Penn, R. L.; Tsapatsis, M. Mechanistic principles of nanoparticle evolution to zeolite crystals Nat. Mater. 2006, 5, 400-408
53. Kumar, S.; Davis, T. M.; Ramanan, H.; Penn, R. L.; Tsapatsis, M. Aggregative Growth of Silicalite-1 J. Phys. Chem. B 2007, 111, 3398-3403
54. Harada, S.; Alexander; Seki, K.; Yamamoto, Y.; Zhu, C.; Yamamoto, Y.; Arai, S.; Yamasaki, J.; Tanakam, N.; Uijhara, T. Polytype Transformation by Replication of Stacking Faults Formed by Two-Dimensional Nucleation on Spiral Steps during SiC Solution Growth Cryst. Growth Des. 2012, 12, 3209-3214
55. Hassan, J.; Bergman, J. P.; Henry, A.; Janzén, E. On-axis homoepitaxial growth on Si-face 4H-SiC substrates J. Cryst. Growth. 2008, 310, 4424-4429