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Volumn 1, Issue 7, 2014, Pages 821-824

A convenient, economical and scalable multi-gram synthesis of 1-vinylcyclopropyl 4-methylbenzenesulfonate

Author keywords

[No Author keywords available]

Indexed keywords

ALKYLIDENECYCLOPROPANES; CARBOCYCLIZATION; CYCLOISOMERIZATION REACTIONS; HIGHER-ORDER;

EID: 84926511552     PISSN: 20524110     EISSN: 20524129     Source Type: Journal    
DOI: 10.1039/c4qo00089g     Document Type: Article
Times cited : (3)

References (27)
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  • 12
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    • (2011) Science of Synthesis , vol.3 , pp. 145-242
    • Aubert, C.1    Malacria, M.2    Ollivier, C.3
  • 16
    • 84930195351 scopus 로고    scopus 로고
    • in, ed J. G. De Vries, G. A. Molander and A. Evans, Thieme, Stuttgart, Germany, and pertinent references cited therein
    • I. D. G. Watson and F. D. Toste, in Science of Synthesis, ed, J. G. De Vries, G. A. Molander, and, P. A. Evans, Thieme, Stuttgart, Germany, 2011, vol. 3, pp. 243-307 and pertinent references cited therein
    • (2011) Science of Synthesis , vol.3 , pp. 243-307
    • Watson, I.D.G.1    Toste, F.D.2
  • 17
    • 84857755116 scopus 로고    scopus 로고
    • For seminal work on the preparation of ACPs using palladium-catalyzed Tsuji-Trost alkylations, see
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    • (2012) J. Am. Chem. Soc. , vol.134 , pp. 3635
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  • 21
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    • For the synthesis of using Method A, see ref. 9c and pertinent references cited therein For the synthesis of 1 using Method B, see
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    • (1999) Synlett , vol.1 , pp. 1539
    • Ollivier, J.1    Girard, N.2    Salaün, J.3
  • 22
    • 0001229218 scopus 로고    scopus 로고
    • -1 and does not account for the quantity purchased or reagent purity Although (1-ethoxycyclopropoxy)trimethylsilane 8 can be prepared from 10; this approach adds an additional step and does not circumvent the aforementioned challenges. 15
    • S. Bräse S. Schömenauer G. McGaffin A. Stolle A. de Meijere Chem.-Eur J. 1996 2 545
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