Assessment of two extraction methods to determine pesticides in soils, sediments and sludges. Application to the Túria River Basin

Journal of Chromatography A

Volumn 1378, Issue , 2015, Pages 19-31

  Masiá, Ana ^a   Vásquez, Karina ^a   Campo, Julián ^a   Picó, Yolanda ^a  

^a UNIVERSITY OF VALENCIA   (Spain)

Author keywords

Liquid chromatography; Mass spectrometry; Pesticides; Sediments; Sludges; Soil

Indexed keywords

LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; MATRIX ALGEBRA; PESTICIDES; PHASE SEPARATION; RECOVERY; SEDIMENTS; SEWAGE SLUDGE; SOILS; WATERSHEDS;

DISPERSIVE SOLID PHASE EXTRACTION; EXTRACTION EFFICIENCIES; EXTRACTION METHOD; PRESSURIZED LIQUID EXTRACTION; REPRODUCIBILITIES; SIMULTANEOUS DETERMINATIONS; SLUDGES; STANDARD CALIBRATION;

EXTRACTION;

ACETOCHLOR; ALACHLOR; CARBOFURAN; CHLORPYRIFOS; DIMPYLATE; ENILCONAZOLE; HEXYTHIAZOX; ISOPROTURON; ORGANIC SOLVENT; PESTICIDE; PYRIPROXYFEN; TERBUMETON; TERBUTYLAZINE; TIABENDAZOLE; UNCLASSIFIED DRUG; SEWAGE; SOIL;

ARTICLE; CALIBRATION; CONTROLLED STUDY; EXTRACTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MEASUREMENT REPEATABILITY; PRESSURE; PRESSURIZED LIQUID EXTRACTION; QUICK EASY CHEAP EFFECTIVE RUGGED AND SAFE EXTRACTION; REPRODUCIBILITY; RIVER BASIN; SAMPLE SIZE; SEDIMENT; SLUDGE; SOIL; SOLID PHASE EXTRACTION; SPAIN; TANDEM MASS SPECTROMETRY; TEMPERATURE; CHEMISTRY; ENVIRONMENTAL MONITORING; PROCEDURES; RIVER; SEWAGE; STANDARDS;

ENVIRONMENTAL MONITORING; GEOLOGIC SEDIMENTS; PESTICIDES; REPRODUCIBILITY OF RESULTS; RIVERS; SEWAGE; SOIL; SOLID PHASE EXTRACTION;

EID: 84920706276     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2014.11.079     Document Type: Article

References (49)

1. Blasco C., Font G., Pico Y. Comparison of microextraction procedures to determine pesticides in oranges by liquid chromatography-mass spectrometry. J. Chromatogr. A 2002, 970:201-212.
2. Pindado Jimenez O., Perez Pastor R.M. Estimation of measurement uncertainty of pesticides, polychlorinated biphenyls and polyaromatic hydrocarbons in sediments by using gas chromatography-mass spectrometry. Anal. Chim. Acta 2012, 724:20-29.
3. Carvalho P.N., Rodrigues P.N., Alves F., Evangelista R., Basto M.C., Vasconcelos M. An expeditious method for the determination of organochlorine pesticides residues in estuarine sediments using microwave assisted pre-extraction and automated headspace solid-phase microextraction coupled to gas chromatography-mass spectrometry. Talanta 2008, 76:1124-1129.
4. Salvado V., Alcaide A., Carandell N., Hidalgo M. Evaluation of extraction procedures of organochlorine pesticides from natural waters and sediments. Int. J. Environ. Anal. Chem. 2001, 81:243-256.
5. Kvicalova M., Doubravova P., Jobanek R., Jokesova M., Ocenaskova V., Suessenbekova H., et al. Application of different extraction methods for the determination of selected pesticide residues in sediments. Bull. Environ. Contam. Toxicol. 2012, 89:21-26.
6. Vega Moreno D., Sosa Ferrera Z., Santana Rodiguez J.J. Microwave assisted micellar extraction coupled with solid phase microextraction for the determination of organochlorine pesticides in soil samples. Anal. Chim. Acta 2006, 571:51-57.
7. Herbert P., Morais S., Paiga P., Alves A., Santos L. Development and validation of a novel method for the analysis of chlorinated pesticides in soils using microwave-assisted extraction-headspace solid phase microextraction and gas chromatography-tandem mass spectrometry. Anal. Bioanal. Chem. 2006, 384:810-816.
8. Guo L., Lee H.K. Microwave assisted extraction combined with solvent bar microextraction for one-step solvent-minimized extraction, cleanup and preconcentration of polycyclic aromatic hydrocarbons in soil samples. J. Chromatogr. A 2013, 1286:9-15.
9. Martinez K., Barcelo D. Determination of antifouling pesticides and their degradation products in marine sediments by means of ultrasonic extraction and HPLC-APCI-MS. Fresenius J. Anal. Chem. 2001, 370:940-945.
10. Han M., Gan Z., Liang S., An L., Zhao X. Automated sample clean-up and fraction of organochlorine pesticides in sediments using the SPE-GPC-VAP System. Bull. Environ. Contam. Toxicol. 2012, 88:858-862.
11. Vagi M., Petsas A., Kostopoulou M., Karamanoli M., Lekkas T. Determination of organochlorine pesticides in marine sediments samples using ultrasonic solvent extraction followed by GC/ECD. Desalination 2007, 210:146-156.
12. Directive 2008/105/EC of the European Parliament and of the council of 16 December 2008 on environmental quality standards in the field of water policy, amending and subsequently repealing Council Directives 82/176/EEC, 83/513/EEC, 84/156/EEC, 84/491/EEC, 86/280/EEC and amending Directive 2000/60/EC of the European Parliament and of the Council. Off. J. Eur. Union 2008, 348:84-97.
13. Gerstl Z., Kliger L. Fractionation of the organic-matter in soils and sediments and their contribution to the sorption of pesticides. J. Environ. Sci. Health B 1990, 25:729-741.
14. Wang Q., Yin J., Pan H., Xu F., Yang Y. A novel method based on combining ultrasonic-assisted dispersive solid-phase extraction and low-density solvent dispersive liquid-liquid microextraction (UA-DSPE-LDS-DLLME) for the determination of organophosphorus pesticides in soil. Anal. Methods 2014, 6:7335-7342.
15. Kalogridi E.C., Christophoridis C., Bizani E., Drimaropoulou G., Fytianos K. Part II: temporal and spatial distribution of multiclass pesticide residues in lake sediments of northern Greece: application of an optimized MAE-LC-MS/MS pretreatment and analytical method. Environ. Sci. Pollut. Res. Int. 2014, 21:7252-7262.
16. Masia A., Campo J., Vazquez-Roig P., Blasco C., Pico Y. Screening of currently used pesticides in water, sediments and biota of the Guadalquivir River Basin (Spain). J. Hazard. Mater. 2013, 263:95-104.
17. Berlioz-Barbier A., Vauchez A., Wiest L., Baudot R., Vulliet E., Cren-Olive C. Multi-residue analysis of emerging pollutants in sediment using QuEChERS-based extraction followed by LC-MS/MS analysis. Anal. Bioanal. Chem. 2014, 406:1259-1266.
18. Pinto M.I., Vale C., Sontag G., Noronha J.P. Effects of ultrasonic irradiation and direct heating on extraction of priority pesticides from marine sediments. Int. J. Environ. Anal. Chem. 2013, 93:1638-1659.
19. Koeck-Schulmeyer M., Olmos M., Lopez de Alda M., Barcelo D. Development of a multiresidue method for analysis of pesticides in sediments based on isotope dilution and liquid chromatography-electrospray-tandem mass spectrometry. J. Chromatogr. A 2013, 1305:176-187.
20. Regueiro J., Matamoros V., Thibaut R., Porte C., Bayona J.M. Use of effect-directed analysis for the identification of organic toxicants in surface flow constructed wetland sediments. Chemosphere 2013, 91:1165-1175.
21. Chiaia-Hernandez A.C., Krauss M., Hollender J. Screening of lake sediments for emerging contaminants by liquid chromatography atmospheric pressure photoionization and electrospray ionization coupled to high resolution mass spectrometry. Environ. Sci. Technol. 2013, 47:976-986.
22. Harrison R., Bull I., Michaelides K. A method for the simultaneous extraction of seven pesticides from soil and sediment. Anal. Methods 2013, 5:2053-2058.
23. Lazartigues A., Fratta C., Baudot R., Wiest L., Feidt C., Thomas M., et al. Multiresidue method for the determination of 13 pesticides in three environmental matrices: water, sediments and fish muscle. Talanta 2011, 85:1500-1507.
24. Wu J., Lin Y., Lu J., Wilson C. Copper clean-up procedure for ultrasonic extraction and analysis of pyrethroid and phenylpyrazole pesticides in sediments by gas chromatography-electron capture detection. Sci. Total Environ. 2011, 409:3482-3491.
25. Camino-Sanchez F., Zafra-Gomez A., Perez-Trujillo J., Conde-Gonzalez J., Marques J., Luis Vilchez J. Validation of a GC-MS/MS method for simultaneous determination of 86 persistent organic pollutants in marine sediments by pressurized liquid extraction followed by stir bar sorptive extraction. Chemosphere 2011, 84:869-881.
26. Naeeni M.H., Yamini Y., Rezaee M. Combination of supercritical fluid extraction with dispersive liquid-liquid microextraction for extraction of organophosphorus pesticides from soil and marine sediment samples. J. Supercrit. Fluids 2011, 57:219-226.
27. Brondi S., de Macedo A., Vicente G., Nogueira A. Evaluation of the QuEChERS method and gas chromatography-mass spectrometry for the analysis pesticide residues in water and sediment. Bull. Environ. Contam. Toxicol. 2011, 86:18-22.
28. Hassan J., Farahani A., Shamsipur M., Damerchili F. Rapid and simple low density miniaturized homogeneous liquid-liquid extraction and gas chromatography/mass spectrometric determination of pesticide residues in sediment. J. Hazard. Mater. 2010, 184:869-871.
29. Li H., Wei Y., You J., Lydy M.J. Analysis of sediment-associated insecticides using ultrasound assisted microwave extraction and gas chromatography-mass spectrometry. Talanta 2010, 83:171-177.
30. Wang D., You J., Lydy M.J. Sediment matrix effects in analysis of pyrethroid insecticides using gas chromatography-mass spectrometry. Arch. Environ. Contam. Toxicol. 2010, 59:382-392.
31. Darwano H., Duy S.V., Sauve S. A new protocol for the analysis of pharmaceuticals, pesticides, and hormones in sediments and suspended particulate matter from rivers and municipal wastewaters. Arch. Environ. Contam. Toxicol. 2014, 66:582-593.
32. You J., Wang D., Lydy M.J. Determination of pyrethroid insecticides in sediment by gas chromatography-ion trap tandem mass spectrometry. Talanta 2010, 81:136-141.
33. Bol'shakov D.S., Amelin V.G., Tret'yakov A.V. Determination of polar pesticides in soil by micellar electrokinetic chromatography using QuEChERS sample preparation. J. Anal. Chem. 2014, 69:89-97.
34. Chai L.-K., Elie F., Jinang C. Determination of 24 pesticides residues in mineral and peat soils by modified QuEChERS method and gas chromatography. Int. J. Environ. Anal. Chem. 2014, 94:519-530.
35. Pose-Juan E., Herrero-Hernandez E., Alvarez-Martin A., Sanchez-Martin M.J., Sonia Rodriguez-Cruz M. Development of a procedure for the multiresidue analysis of pesticides in vineyard soils and its application to real samples. J. Sep. Sci. 2014, 37:2215-2224.
36. Martinez Vidal J.L., Padilla Sanchez J.A., Plaza-Bolanos P., Garrido Frenich A., Romero-Gonzalez R. Use of pressurized liquid extraction for the simultaneous analysis of 28 polar and 94 non-polar pesticides in agricultural soils by GC/QqQ-MS/MS and UPLC/QqQ-MS/MS. J. AOAC Int. 2010, 93:1715-1731.
37. Lesueur C., Gartner M., Mentler A., Fuerhacker M. Comparison of four extraction methods for the analysis of 24 pesticides in soil samples with gas chromatography-mass spectrometry and liquid chromatography-ion trap-mass spectrometry. Talanta 2008, 75:284-293.
38. Jesus Garcia-Galan M., Silvia Diaz-Cruz M., Barcelo D. Determination of triazines and their metabolites in environmental samples using molecularly imprinted polymer extraction, pressurized liquid extraction and LC-tandem mass spectrometry. J. Hydrol. 2010, 383:30-38.
39. Cerqueira M.B.R., Caldas S.S., Primel E.G. New sorbent in the dispersive solid phase extraction step of quick, easy, cheap, effective, rugged, and safe for the extraction of organic contaminants in drinking water treatment sludge. J. Chromatogr. A 2014, 1336:10-22.
40. Moreno D., Ferrera V,Z., Rodriguez J. Sample extraction method combining micellar extraction-SPME and HPLC for the determination of organochlorine pesticides in agricultural soils. J. Agric. Food Chem. 2006, 54:7747-7752.
41. Lu H., Lin Y., Wilson P. Organic-solvent-free extraction method for determination of carbamate and carbamoyloxime pesticides in soil and sediment samples. Bull. Environ. Contam. Toxicol. 2009, 83:621-625.
42. Bruzzoniti M.C., Checchini L., De Carlo R.M., Orlandini S., Rivoira L., Del Bubba M. QuEChERS sample preparation for the determination of pesticides and other organic residues in environmental matrices: a critical review. Anal. Bioanal. Chem. 2014, 406:4089-4116.
43. Carmona E., Andreu V., Pico Y. Occurrence of acidic pharmaceuticals and personal care products in Turia River Basin: from waste to drinking water. Sci. Total Environ. 2014, 484:53-63.
44. Vazquez-Roig P., Segarra R., Blasco C., Andreu V., Pico Y. Determination of pharmaceuticals in soils and sediments by pressurized liquid extraction and liquid chromatography tandem mass spectrometry. J. Chromatogr. A 2010, 1217:2471-2483.
45. Anastassiades M., Lehotay S.J., Stajnbaher D., Schenck F.J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and dispersive solid-phase extraction for the determination of pesticide residues in produce. J. AOAC Int. 2003, 86:412-431.
46. Masia A., Ibanez M., Blasco C., Sancho J.V., Pico Y., Hernandez F. Combined use of liquid chromatography triple quadrupole mass spectrometry and liquid chromatography quadrupole time-of-flight mass spectrometry in systematic screening of pesticides and other contaminants in water samples. Anal. Chim. Acta 2013, 761:117-127.
47. Guidance document on pesticide residue analytical methods. SANCO/825/00 rev. 8.1, EUROPEAN COMMISSION, Directorate General Health and Consumer Protection (16/11/2010) pp. 1-16.
48. Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed. SANCO/12571/2013 Supersedes SANCO/12495/2011 Implemented by 01/01/2014, EUROPEAN COMMISSION HEALTH & CONSUMER PROTECTION DIRECTORATE-GENER (19 November 2013 rev. 0) pp. 1-42.
49. Campo J., Masia A., Blasco C., Pico Y. Occurrence and removal efficiency of pesticides in sewage treatment plants of four Mediterranean River Basins. J. Hazard. Mater. 2013, 263:146-157.