Simultaneous determination of water-soluble vitamins in beverages and dietary supplements by LC-MS/MS

Food Additives and Contaminants - Part A Chemistry, Analysis, Control, Exposure and Risk Assessment

Volumn 31, Issue 12, 2014, Pages 1939-1948

  Kakitani, Ayano ^a   Inoue, Tomonori ^a   Matsumoto, Keiko ^b   Watanabe, Jun ^b   Nagatomi, Yasushi ^a   Mochizuki, Naoki ^a  

^a Asahi Soft Drinks Co Ltd   (Japan)

^b SHIMADZU CORPORATION   (Japan)

Author keywords

LC MS MS; multi mode ODS column; nutrition labelling; quality control; water soluble vitamin

Indexed keywords

BEVERAGES; CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; FOOD ADDITIVES; LIQUID CHROMATOGRAPHY; NUTRITION; QUALITY CONTROL; VITAMINS;

BEVERAGE SAMPLES; CATION EXCHANGE CAPACITIES; CHROMATOGRAPHIC SEPARATIONS; ION-PAIR REAGENTS; LC-MS/MS; ODS COLUMNS; SIMULTANEOUS DETERMINATIONS; WATER SOLUBLE VITAMINS;

DIETARY SUPPLEMENTS;

FORMIC ACID; VITAMIN; WATER; ASCORBIC ACID; SOLVENT; VITAMIN B COMPLEX;

ACCURACY; ANION EXCHANGE; ARTICLE; BEVERAGE; CATION EXCHANGE; CENTRIFUGATION; DIET SUPPLEMENTATION; DISSOCIATION; ENERGY DRINK; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; QUALITY CONTROL; QUANTITATIVE ANALYSIS; TANDEM MASS SPECTROMETRY; ANALYSIS; CALIBRATION; CHEMISTRY; COMPARATIVE STUDY; ELECTROSPRAY MASS SPECTROMETRY; FOOD CONTROL; FOOD PACKAGING; HUMAN; JAPAN; NUTRITIONAL VALUE; PH; PROCEDURES; REPRODUCIBILITY; SOLUBILITY; VALIDATION STUDY;

ASCORBIC ACID; BEVERAGES; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DIETARY SUPPLEMENTS; FOOD INSPECTION; FOOD LABELING; FOOD, FORTIFIED; HUMANS; HYDROGEN-ION CONCENTRATION; JAPAN; NUTRITIVE VALUE; QUALITY CONTROL; REPRODUCIBILITY OF RESULTS; SOLUBILITY; SOLVENTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY; VITAMIN B COMPLEX; VITAMINS;

EID: 84914099270     PISSN: 19440049     EISSN: 19440057     Source Type: Journal    
DOI: 10.1080/19440049.2014.977965     Document Type: Article

References (38)

1. Abbood A, Smadja C, Taverna M, Herrenknecht C. 2010. High performance liquid chromatography separation of structurally related enkephalins on quaternary ammonium-embedded stationary phase in isocratic mode. J Chromatogr A. 1217:450–458.
2. Albala´-Hurtado S, Veciana-Nogue´s MT, Izquierdo-Pulido M, Marine´-Font A. 1997. Determination of water-soluble vitamins in infant milk by high-performance liquid chromatography. J Chromatogr A. 778:247–253.
3. Andrieux P, Fontannaz P, Kilinc T, Giménez EC, Jaudzems G, Dowell D. 2013. Pantothenic acid (vitamin B5) in infant formula and adult/pediatric nutritional formula: first action 2012.16. JAOAC International 96:497–499.
4. Blake CJ. 2007. Analytical procedures for water-soluble vitamins in foods and dietary supplements: a review. Anal Bioanal Chem. 389:63–76.
5. Burdock GA. 1997. Encyclopedia of food and color additives. Vol. 1–3. Boca Raton (FL): CRC Press.
6. Campos-Giménez E, Fontannaz P, Redeuil K, Kilinc T, Dowell D. 2013. Vitamin C in infant formula and adult/pediatric nutritional formula by ultra-performance liquid chromatography with ultraviolet detection: first action 2012.22. J AOAC int. 96:1065–1067.
7. Campos-Giménez E, Fontannaz P, Trisconi M-J, Kilinc T, Gimenez C, Andrieux P, Nelson M. 2012. Determination of vitamin B12 in infant formula and adult nutritionals by liquid chromatography/UV detection with immunoaffinity extraction: first action 2011.08. J AOAC International 95:307–312.
8. Chatzimichalakis PF, Samanidou VF, Verpoorte R, Papadoyannis IN. 2004. Development of a validated HPLC method for the determination of B-complex vitamins in pharmaceuticals and biological fluids after solid phase extraction. J Sep Sci. 27:1181–1188.
9. Chen P, Atkinson R, Wolf WR. 2009. Single-laboratory validation of a high-performance liquid chromatographic-diode array detector-fluorescence detector/mass spectrometric method for simultaneous determination of water-soluble vitamins in multivitamin dietary tablets. JAOAC International 92:680–688.
10. Chen Z, Chen B, Yao S. 2006. High-performance liquid chromatography/electrospray ionization-mass spectrometry for simultaneous determination of taurine and 10 water-soluble vitamins in multivitamin tablets. Anal Chim Acta. 569:169–175.
11. Chen P, Wolf WR. 2007. LC/UV/MS-MRM for the simultaneous determination of water-soluble vitamins in multi-vitamin dietary supplements. Anal Bioanal Chem. 387:2441–2448.
12. Eitenmiller RR, Ye L, Landen WO. 2008. Vitamin analysis for the health and food sciences. 2nd ed. Boca Raton (FL): CRC Press.
13. Gentili A, Caretti F, D’Ascenzo G, Marchese S, Perret D, Di Corcia D., Rocca LM. 2008. Simultaneous determination of water-soluble vitamins in selected food matrices by liquid chromatography/electrospray ionization tandem mass spectrometry. Rapid Commun Mass Spectrom. 22:2029–2043.
14. Hadjmohammadi MR, Sharifi V. 2007. Use of solid phase extraction for sample clean-up and preconcentration of vitamin B12 in multivitamin tablet before HPLC-UV, UV and atomic absorption spectrophotometry. J Food Drug Anal. 15:285–289.
15. Heudi O, Kilinç T, Fontannaz P. 2005. Separation of water-soluble vitamins by reversed-phase high performance liquid chromatography with ultra-violet detection: application to polyvitaminated premixes. J Chromatogr A. 1070:49–56.
16. Heudi O, Kilinç T, Fontannaz P, Marley E. 2006. Determination of vitamin B12 in food products and in premixes by reversed-phase high performance liquid chromatography and immunoaffinity extraction. J Chromatogr A. 1101:63–68.
17. Kirchner U, Degenhardt K, Raffler G, Nelson M. 2012. Determination of vitamin B12 in infant formula and adult nutritionals using HPLC after purification on an immunoaffinity column: first action 2011.09. JAOAC International 95:933–936.
18. Klampfl CW, Buchberger W, Haddad PR. 2001. Fast separation of pyrimidine derivatives by capillary electrochromatography on ion-exchange/reversed-phase mixed-mode stationary phases. J Chromatogr A. 911:277–283.
19. Latimer GW. 2012. Official methods of analysis of AOAC International. 19th ed. Gaithersburg (MD): AOAC International.
20. Li HB, Chen F. 2001. Simultaneous determination of twelve water- and fat-soluble vitamins by high-performance liquid chromatography with diode array detection. Chromatographia. 54:270–273.
21. Majors RE, Lees A, Burkhardt M. 2009. Improving protein separations with mixed-mode chromatography [Internet]. LCGC North America. January 1. Available from: http://www.chromatographyonline.com/lcgc/Column%3A + Column + Watch/Improving-Protein-Separations-with-Mixed-Mode-Chro/ArticleStandard/Article/detail/579013
22. Meisser-Redeuil K, Bénet S, Gimenez C, Campos-Giménez E, Nelson M. 2014. Determination of folate in infant formula and adult/pediatric nutritional formula by ultra-high performance liquid chromatography-tandem mass spectrometry: first action 2013.13. JAOAC International 97:1121–1126.
23. Ministry of Health, Labour, and Welfare, Japan. Food with Health Claims, Food for Special Dietary Uses, and Nutrition Labeling [Internet]. Available from: http://www.mhlw.go.jp/english/topics/foodsafety/fhc/
24. The Ministry of Health and Welfare. 2009. Eight Editions Japan’s Specifications and Standards for Food Additives. Tokyo (Japan): Japan Food Additives Association.
25. Moreno P, Salvadó V. 2000. Determination of eight water- and fat-soluble vitamins in multi-vitamin pharmaceutical formulations by high-performance liquid chromatography. J Chromatogr A. 870:207–215.
26. Morii K, Ohashi M, Tanaka T, Kitada Y. 2004. Determination of water soluble vitamins in foods with nutrient function claims by liquid chromatography. Jpn J Food Chem. 11:19–25.
27. Patil SS, Srivastava AK. 2012. Development and validation of rapid ion-pair RPLC method for simultaneous determination of certain B-complex vitamins along with vitamin C. JAOAC International 95:74–83.
28. The Pharmaceutical Society of Japan. 2010. Methods of analysis in health science. Tokyo (Japan): Kanehara & Co.
29. Santos J, Mendiola JA, Oliveira MBPP, Ibáñez E, Herrero M. 2012. Sequential determination of fat- and water-soluble vitamins in green leafy vegetables during storage. J Chromatogr A. 1261:179–188.
30. Schimpf K, Spiegel R, Thompson L, Dowell D. 2012. Determination of vitamin B12 in infant formula and adult nutritionals by HPLC: first action 2011.10. JAOAC International 95:313–318.
31. Schimpf K, Thompson L, Baugh S. 2013. Vitamin C in infant formula and adult/pediatric nutritional formula by HPLC with UV detection: first action 2012.21. JAOAC International 96:802–807.
32. Stevenson PG, Fairchild JN, Guiochon G. 2011. Retention mechanism divergence of a mixed mode stationary phase for high performance liquid chromatography. J Chromatogr A. 1218:1822–1827.
33. Szpylka J, De Vries J, Cheney A, House S. 2012. Determination of total folates in infant formula and adult nutritionals by trienzyme extraction and UPLC-MS/MS quantitation: first action 2011.06. JAOAC International 95:1547–1554.
34. Vidović S, Stojanović B, Veljković J, Pražić-Arsić L, Roglić G, Manojlović D. 2008. Simultaneous determination of some water-soluble vitamins and preservatives in multivitamin syrup by validated stability-indicating high-performance liquid chromatography method. J Chromatogr A. 1202:155–162.
35. Viñas P, López-Erroz C, Balsalobre N, Hernández-Córdoba M. 2003. Reversed-phase liquid chromatography on an amide stationary phase for the determination of the B group vitamins in baby foods. J Chromatogr A. 1007:77–84.
36. Yang Y, Geng X. 2011. Mixed-mode chromatography and its applications to biopolymers. J Chromatogr A. 1218:8813–8825.
37. Zhang H, Chen S, Liao W, Ren Y. 2009. Fast simultaneous determination of multiple water-soluble vitamins and vitamin like compounds in infant formula by UPLC-MS/MS. J Food Agri Environ. 7:88–93.
38. Zhang K, Dai L, Chetwyn NP. 2010. Simultaneous determination of positive and negative pharmaceutical counterions using mixed-mode chromatography coupled with charged aerosol detector. J Chromatogr A. 1217:5776–5784.