Online sample concentration in partial-filling chiral electrokinetic chromatography - Mass spectrometry

Chirality

Volumn 26, Issue 11, 2014, Pages 734-738

  Wuethrich, Alain ^a   Haddad, Paul R ^a   Quirino, Joselito P ^a  

^a UNIVERSITY OF TASMANIA   (Australia)

Author keywords

Capillary electrophoresis; Chlorpheniramine; Enantiomeric separation; Field enhanced sample injection; Micelle to solvent stacking

Indexed keywords

ACETONITRILE; AMMONIUM ACETATE; CHLORPHENIRAMINE MALEATE; DODECYLSULFATE AMMONIUM;

ARTICLE; CHIRAL CHROMATOGRAPHY; CONTROLLED STUDY; CRITICAL MICELLE CONCENTRATION; ELECTROPHORETIC MOBILITY; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDRODYNAMICS; LIMIT OF DETECTION; MASS SPECTROMETRY; MICELLAR ELECTROKINETIC CHROMATOGRAPHY; MICELLE; RACEMIC MIXTURE;

EID: 84910134161     PISSN: 08990042     EISSN: 1520636X     Source Type: Journal    
DOI: 10.1002/chir.22257     Document Type: Article

References (35)

1. Armstrong DW, Zhang B. Chiral stationary phases for HPLC. Anal Chem 2001;73:557A-561A.
2. Welch CJ. Microscale chiral HPLC in support of pharmaceutical process research. Chirality 2009;21:114-118.
3. Terabe S, Otsuka K, Ando T. Electrokinetic chromatography with micellar solution and open-tubular capillary. Anal Chem 1985;57:834-841.
4. Terabe S, Shibata M, Miyashita Y. Chiral separation by electrokinetic chromatography with bile salt micelles. J Chromatogr A 1989;480:403-411.
5. Otsuka K, Kawahara J, Tatekawa K. Chiral separations by micellar electrokinetic chromatography with sodium N-dodecanoyl-L-valinate. J Chromatogr A 1991;559:209-214.
6. Fanali S. Celebrating 30 years Chiral separations by CE employing CDs. Electrophoresis 2009;203-210.
7. Aini WAN, Ibrahim WAN, Munirah S, Wahib ABD, Hermawan D, Sanagi MM. Chiral separation of vinpocetine using cyclodextrin-modified micellar electrokinetic chromatography. Chirality 2012;254:252-254.
8. Han Y, Bai Y, Xiao Y, Du F, Liang Y, Tan Z. Simultaneous discrimination of jasmonic acid stereoisomers by CE-QTOF-MS employing the partial filling technique. Electrophoresis 2011;32:2693-2699.
9. Tanaka Y, Otsuka K, Terabe S. Separation of enantiomers by capillary electrophoresis-mass spectrometry employing a partial filling technique with a chiral crown ether. J Chromatogr A 2000;875:323-330.
10. Kumar AP, Park JH. Azithromycin as a new chiral selector in capillary electrophoresis. J Chromatogr A 2011;1218:1314-1317.
11. Wang X, Hou J, Jann M, Hon YY, Shamsi SA. Development of a chiral micellar electrokinetic chromatography-tandem mass spectrometry assay for simultaneous analysis of warfarin and hydroxywarfarin metabolites: application to the analysis of patients serum samples. J Chromatogr A 2013;1271:207-216.
12. Sueyoshi K, Koino H, Kitagawa F, Otsuka K. Sensitive enantioseparation by transient trapping-cyclodextrin electrokinetic chromatography. J Chromatogr A 2012;1269:366-371.
13. Simó C, García-Cañas V, Cifuentes A. Chiral CE-MS. Electrophoresis 2012;31:1442-1456.
14. Vindevogel J, Sandra P. Introduction to Micellar Electrokinetic Chromatography. Huethig, Heidelberg, 1992; Vol. 15, p. 231.
15. Losman JA, Looper RE, Koivunen P, Lee S, Schneider RK, McMahon C, Cowley GS, Root DE, Ebert BL, Kaelin Jr WG. (R)-2-hydroxyglutarate is sufficient to promote leukemogenesis and its effects are reversible. Science 2013;340:1621-1625.
16. Hou J, Rizvi SAA, Zheng J, Shamsi SA. Application of polymeric surfactants in micellar electrokinetic chromatography-electrospray ionization mass spectrometry of benzodiazepines and benzoxazocine chiral drugs. Electrophoresis 2006;27:1263-1275.
17. Wang B, He J, Shamsi SAA. A high-throughput multivariate optimization for the simultaneous enantioseparation and detection of barbiturates inmicellar electrokinetic chromatography-mass spectrometry. J Chromatogr Sci 2010;48:572-583.
18. Yang L, Lee CS. Micellar electrokinetic chromatography-mass spectrometry. J Chromatogr A 1997;780:207-218.
19. Muijselaar PG, Otsuka K, Terabe S. On-line coupling of partial- filling micellar electrokinetic chromatography with mass spectrometry. J Chromatogr A 1998;802:3-15.
20. Quirino JP. Exceeding 5000-fold concentration of dilute analytes in micellar electrokinetic chromatography. Science 1998;282:465-468.
21. Quirino JP, Haddad PR. Online sample preconcentration in capillary electrophoresis using analyte focusing by micelle collapse. Electrophoresis 2008;80:6824-6829.
22. Liu Z, Sam P, Sirimanne SR, McClure PC, Grainger J, Patterson DG. Fieldamplified sample stacking in micellar electrokinetic chromatography for on-column sample concentration of neutral molecules. J Chromatogr A 1994;673:125-132.
23. Kirschner DL, Jaramillo M, Green TK. Enantioseparation and stacking of Cyanobenz[f]isoindole-amino acids by reverse polarity capillary electrophoresis and sulfated beta-cyclodextrin. Anal Chem 2007;79:736-743.
24. Xia S, Zhang L, Lu M, Qiu B, Chi Y, Chen G. Enantiomeric separation of chiral dipeptides by CE-ESI-MS employing a partial fi lling technique with chiral crown ether. Electrophoresis 2009;30:2837-2844.
25. Ge L, Tan SN, Yong JWH, Hua L, Ong ES. Separation of cytokinin isomers with a partial filling-micellar electrokinetic chromatographymass spectrometry approach. Electrophoresis 2008;29:2024-2032.
26. Chen YR, Tseng MC, Chang YZ, Her GR. A low-flow CE/electrospray ionization MS interface for capillary zone electrophoresis, large-volume sample stacking, and micellar electrokinetic chromatography. Anal Chem 2003;75:503-508.
27. Quirino JP. Sweeping of neutral analytes in partial-filling micellar electrokinetic chromatography with electrospray ionization mass spectrometry. Electrophoresis 2011;32:665-668.
28. Mikkers FEP, Everaerts FM, Verheggen TPEM. Concentration distributions in free zone electrophoresis. J Chromatogr A 1979;169:1-10.
29. Chien RL, Burgi DS. Field amplified sample injection in high-performance capillary electrophoresis. J Chromatogr 1991;559:141-152.
30. Quirino JP, Terabe S. Approaching a million-fold sensitivity increase in capillary electrophoresis with direct ultraviolet detection: cationselective exhaustive injection and sweeping. Anal Chem 2000;72:1023-1030.
31. Hirokawa T, Okamoto H, Gas B. High-sensitive capillary zone electrophoresis analysis by electrokinetic injection with transient isotachophoretic preconcentration: electrokinetic supercharging. Electrophoresis 2003;24:498-504.
32. Rabanes HR, Aranas AT, Benbow NL, Quirino JP. Synergistic effect of field enhanced sample injection on micelle to solvent stacking in capillary electrophoresis. J Chromatogr A 2012;1267:74-79.
33. Quirino JP. Micelle to solvent stacking of organic cations in capillary zone electrophoresis with electrospray ionization mass spectrometry. J Chromatogr A 2009;1216:294-299.
34. Guidote AM, Quirino JP. On-line sample concentration of organic anions in capillary zone electrophoresis by micelle to solvent stacking. J Chromatogr A 2010;1217:6290-6295.
35. Cifuentes A, Bernal JL, Diez-Masa JC. Determination of critical micelle concentration values using capillary electrophoresis instrumentation. Anal Chem 1997;69:4271-4274.