Comparison of superficially porous and fully porous silica supports used for a cyclofructan 6 hydrophilic interaction liquid chromatographic stationary phase

Journal of Chromatography A

Volumn 1365, Issue , 2014, Pages 124-130

  Dolzan, Maressa D ^a,b   Spudeit, Daniel A ^a,b   Breitbach, Zachary S ^a   Barber, William E ^c   Micke, Gustavo A ^b   Armstrong, Daniel W ^a,d  

^a UNIVERSITY OF TEXAS AT ARLINGTON   (United States)

^b FEDERAL UNIVERSITY OF SANTA CATARINA   (Brazil)

^c AGILENT TECHNOLOGIES   (United States)

^d AZYP LLC   (United States)

Author keywords

Core shell; Cyclofructan 6; FRULIC; HILIC; Superficially porous particles

Indexed keywords

HYDROPHILICITY; LIQUID CHROMATOGRAPHY; POLYMETHYL METHACRYLATES; SILICA;

CORE SHELL; CYCLOFRUCTAN 6; FRULIC; HILIC; SUPERFICIALLY POROUS PARTICLES;

POROUS MATERIALS;

CYCLOFRUCTAN 6; FRUCTAN; SILICON DIOXIDE; UNCLASSIFIED DRUG;

ANALYTICAL PARAMETERS; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL BOND; CHEMICAL INTERACTION; CHEMICAL PARAMETERS; COLUMN CHROMATOGRAPHY; COMPARATIVE STUDY; FLOW RATE; HIGH THROUGHPUT SCREENING; HYDROPHILIC INTERACTION LIQUID CHROMATOGRAPHIC STATIONARY PHASE; LIQUID CHROMATOGRAPHY; PHYSICAL CHEMISTRY; POROSITY; CHEMICAL PHENOMENA; CHEMISTRY; DEVICES;

CHROMATOGRAPHY, LIQUID; FRUCTANS; HYDROPHOBIC AND HYDROPHILIC INTERACTIONS; POROSITY; SILICON DIOXIDE;

EID: 84908072696     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2014.09.010     Document Type: Article

References (30)

1. Destefano J.J., Langlois T.J., Kirkland J.J. Characteristics of superficially-porous silica particles for fast HPLC: some performance comparisons with sub-2-μm particles. J. Chromatogr. Sci. 2008, 46:254-260.
2. Wang X.L., Barber W.E., Long W.J. Applications of superficially porous particles: high speed, high efficiency or both?. J. Chromatogr. A 2012, 1228:72-88.
3. Gritti F., Guiochon G. Facts and legends on columns packed with sub-3-μm core-shell particles. LCGC N. Am. 2012, 7:586-595.
4. Horvath C.G., Preiss B.A., Lipsky S.R. Fast liquid chromatography investigation of operating parameters and the separation of nucleotides on pellicular ion exchangers. Anal. Chem. 1967, 39:1422-1428.
5. Kirkland J.J. Controlled surface porosity supports for high-speed gas and liquid chromatography. Anal. Chem. 1969, 41:218-220.
6. Kirkland J.J. Columns for modern analytical liquid chromatography. Anal. Chem. 1971, 43:36A-48A.
7. Kirkland J.J. Superficially porous silica microspheres for the fast high-performance liquid chromatography of macromolecules. Anal. Chem. 1992, 64:1239-1245.
8. Chauve B., Guillarme D., Cleon P., Veuthey J.L. Evaluation of various HILIC materials for the fast separation of polar compounds. J. Sep. Sci. 2010, 33:752-764.
9. Fekete S., Olah E., Fekete J. Fast liquid chromatography: the domination of core-shell and very fine particles review. J. Chromatogr. A 2012, 1228:57-71.
10. Periat A., Kohler I., Veuthey J.L., Guillarme D. Advances in hydrophilic interaction liquid chromatography for pharmaceutical analysis. LCGC Eur. 2013, 5:17-23.
11. Ruta J., Zurlino D., Grivel C., Heinisch S., Veuthey J.L.D. Guillarme evaluation of columns packed with shell particles with compounds of pharmaceutical interest. J. Chromatogr. A 2012, 1228:221-231.
12. Kirkland J.J., Schuster S.A., Johnson W.L., Boyes B.E. Fused-core particle technology in high-performance liquid chromatography: an overview. J. Pharma. Anal. 2013, 3:303-312.
13. McCalley D.V. Evaluation of the properties of a superficially porous silica stationary phase in hydrophilic interaction chromatography. J. Chromatogr. A 2008, 1193:85-91.
14. Olah E., Fekete S., Fekete J., Ganzler K. Comparative study of new shell-type, sub-2μm fully porous and monolith stationary phases, focusing on mass-transfer resistance. J. Chromatogr. A 2010, 1217:3642-3653.
15. Gritti F., Pereira A.D., Sandra P., Guiochon G. Efficiency of the same neat silica column in hydrophilic interaction chromatography and per aqueous liquid chromatography. J. Chromatogr. A 2010, 1217:683-688.
16. Gritti F., Leonardis I., Shock D., Stevenson P., Shalliker A., Guiochon G. Performance of columns packed with the new shell particles, Kinetex-C18. J. Chromatogr. A 2010, 1217:1589-1603.
17. Qiu H.X., Loukotkova L., Sun P., Tesarova E., Bosakova Z., Armstrong D.W. Cyclofructan 6 based stationary phases for hydrophilic interaction liquid chromatography. J. Chromatogr. A 2011, 1218:270-279.
18. Padivitage N.L.T., Dissanayake M.K., Armstrong D.W. Separation of nucleotides by hydrophilic interaction chromatography using the FRULIC-N column. Anal. Bioanal. Chem. 2013, 405:8837-8848.
19. Nawrocki J. The silanol group and its role in liquid chromatography. J. Chromatogr. A 1997, 779:29-71.
20. O'Gara J.E., Alden B.A., Gendreau C.A., Iraneta P.C., Walter T.H. Dependence of yano bonded phase hydrolytic stability on ligand structure and solution pH. J. Chromatogr. A 2000, 893:245-251.
21. Lomsadze K., Jibuti G., Farkas T., Chankvetadze B. Comparative high-performance liquid chromatography enantioseparations on polysaccharide based chiral stationary phases prepared by coating totally porous and core-shell silica particles. J. Chromatogr. A 2012, 1234:50-55.
22. Gritti F., Guiochon G. Mass transfer mechanism in chiral reversed phase liquid chromatography. J. Chromatogr. A 2014, 1332:35-45.
23. Gritti F., Guiochon G. The van Deemter equation: assumptions, limits, and adjustment to modern high performance liquid chromatography. J. Chromatogr. A 2013, 1302:1-13.
24. Heaton J.C., Wang X., Barber W.E., Buckenmaier S.M., McCalley D.V. Practical observations on the performance of bare silica in hydrophilic interaction compared with C18 reversed-phase liquid chromatography. J. Chromatogr. A 2014, 1328:7-15.
25. Spudeit D.A., Dolzan M.D., Breitbach Z.S., Barber W.E., Micke G.A., Armstrong D.W. Superficially porous particles vs. fully porous particles for bonded high performance liquid chromatographic chiral stationary phases: isopropyl cyclofructan 6. J. Chromatogr. A 2014, in press. 10.1016/j.chroma.2014.08.022.
26. Dihn N.P., Jonsson T., Irgum K. Water uptakeon polar stationary phases under conditions for hydrophilic interaction chromatography and its relation to solute retention. J. Chromatogr. A 2013, 1320:33-47.
27. Broeckhoven K., Cabooter D., Desmet G. Kinetic performance of fully and superficially porous partilces with sizes ranging beween 2.7μm and 5μm: intrinsic evaluatio and applicationto a pharmaceutical test compound. J. Pharma. Anal. 2013, 3:313-323.
28. Gritti F., Guiochon G. Unusual behavior of the height equivalent to a theoretical plate of a new poroshell stationary phase at high temperatures. J. Chromatogr. A 2007, 1169:125-138.
29. Gritti F., Guiochon G. Mass transfer mechanism in hydrophilic interaction chromatography. J. Chromatogr. A 2013, 1302:55-64.
30. Gritti F., Guiochon G. Impact of the nature and composition of the mobile phase on the mass transfer mechanism in chiral reversed phase liquid chromatography. Application to the minimization of the solvent cost in chiral separations. J. Chromatogr. A 2014, 1327:57-65.