Multiresidue pesticide analysis of ginseng and other botanical dietary supplements

ACS Symposium Series

Volumn 1081, Issue , 2011, Pages 333-350

  Wong, Jon W ^a   Zhang, Kai ^a   Shi, Feng ^a   Hayward, Douglas G ^a   Makovi, Carolyn M ^a   Krynitsky, Alexander J ^a   Tech, Katherine ^b   DiBenedetto, Alex L ^b   Lee, Nathaniel S ^b  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

^b UNIVERSITY OF MARYLAND   (United States)

Author keywords

Botanical dietary supplements; Gas chromatography mass spectrometry; High performance liquid chromatography mass spectrometry; Multiresidue pesticide analysis

Indexed keywords

DIETARY SUPPLEMENTS; FOOD ADDITIVES; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; NUTRITION; ORGANIC POLYMERS; SOLVENT EXTRACTION; VITAMINS;

BOTANICAL DIETARY SUPPLEMENTS; CAPILLARY GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY-MASS SPECTROMETRIES; LOW CONCENTRATIONS; MULTIRESIDUE; PESTICIDE ANALYSIS; SOLID-PHASE EXTRACTION;

PESTICIDES;

EID: 84905158289     PISSN: 00976156     EISSN: 19475918     Source Type: Book Series    
DOI: 10.1021/bk-2011-1081.ch023     Document Type: Conference Paper

References (28)

1. Dietary Supplement Health and Education Act of 1994, Pub. L. No. 103-417, 108 Stat. 4323, 1994.
2. Farley, D. FDA questions safety of dietary supplements. Consum. Res. 1994, 77, 15-18.
3. Thomas, P. R. Food for thought about dietary supplements. Nutr. Today 1996, 31, 46-54.
4. Dvorkin, L.; Gardiner, P. M. Regulation of dietary supplements in the United States of America. Clin. Res. Reg. Affairs 2003, 20, 313-325.
5. Bent, S.; Ko, R. Commonly used herbal medicines in the United States: A review. Amer. J. Med. 2004, 116, 478-485.
6. Huggett, D. B.; Khan, I. A.; Allgood, J. C.; Blosck, D. S.; Schlenk, D. Organochlorine pesticides and metals in select botanical dietary supplements. Bull. Environ. Contam. Toxicol. 2001, 66, 150-155.
7. Khan, I. A.; Allgood, J.; Walker, L. A.; Abourashed, E. A.; Schlenk, D.; Benson, W. H. Determination of heavy metals and pesticides in ginseng products. J. AOAC Int. 2001, 84, 936-939.
8. Bicchi, C.; Cordero, C.; Ioro, C.; Rubiolo, P.; Sandra, P.; Yariwake, J. H.; Zuin, V. G. SBSE-GC-ECD/FPD in the analysis of pesticide residues in Passiflora alata Dryander herbal teas. J. Agric. Food Chem. 2003, 51, 27-33.
9. Huggett, D. B.; Block, D. S.; Khan, I. A.; Allgood, J. C.; Benson, W. H. Environmental contaminants in the botanical dietary supplement ginseng and potential human risk. Hum. Ecol. Risk Assess. 2000, 6, 767-776.
10. Zuin, V. G.; Vilegas, J. H. Y. Pesticide residues in medicinal plants and phytomedicines. Phytotheraphy Res. 2000, 14, 73-88.
11. Wong, J. W.; Zhang, K.; Tech, K.; Hayward, D. G.; Krynitsky, A. J.; Cassias, I.; Schenck, F. J.; Banerjee, K.; Dasgupta, S.; Brown, D. Multiresidue pesticide analysis of ginseng powders using acetonitrileor acetone-based extraction, solid-phase extraction cleanup, and gas chromatography-mass spectrometry/selective ion monitoring (GC-MS/SIM) or-tandem mass spectrometry (GC-MS/MS). J. Agric. Food Chem. 2010, 58, 5884-5896.
12. Wong, J. W.; Hao, C.; Zhang, K.; Yang, P.; Banerjee, K.; Hayward, D.; Iftakhar, I.; Schreiber, A.; Tech, K.; Sack, C.; Smoker, M.; Chen, X.; Utture, S. C.; Oulkar, D. P. Development and interlaboratory validation of a QuEChERS-based liquid chromatography-tandem mass spectrometry method for multiresidue pesticide analysis. J. Agric. Food Chem. 2010, 5897-5903.
13. Jaggi, S.; Sood, C.; Kumar, V.; Ravindranath, S. D.; Shanker, A. Leaching of pesticides in tea brew. J. Agric. Food Chem. 2001, 49, 5479-5483.
14. Moltó, J. C.; Lejeune, B.; Prognon, P.; Pradeau, D. GC-MS determination of organochlorine pesticides in five medicinal plants. Int. J. Environ. Anal. Chem. 1994, 54, 81-91.
15. Saha, T.; Chatterjee, S.; Saha, K.; Chowdhury, A.; Somchoudhury, A.; Bhattacharyya, A. Residues of amitraz, a new acaricide, on tea. Bull. Environ. Contam. Toxicol. 2000, 65, 215-221.
16. Srivastava, L. P.; Gupta, K. P.; Raizada, R. B. Organochlorine pesticide residues in herbal ayurvedic preparations. Bull. Environ. Contam. Toxicol. 2000, 64, 502-507.
17. Srivastava, L. P.; Budhwar, R; Raizada, R. B. Organochlorine pesticide residues in Indian spices. Bull. Environ. Contam. Toxicol. 2001, 67, 856-862.
18. Teng, F.; Yue, Y.; Hua, R.; Ge, S.; Tang, J. Development of methods for determination of the residues of 15 pesticides in medicinal herbs Isatis indigotica Fort. by capillary gas chromatography with electron capture or flame photometric detection. J. AOAC Int. 2005, 88, 720-728.
19. Wu, J.; Li, L.; Zou, Y. Determination of carbamate insecticides in Chinese medicinal herbs by gas chromatography with a nitrogen-phosphorus detector. J. AOAC Int. 2005, 88, 1261-1264.
20. Yi, X.; Lu, Y. Multiresidue determination of organophosphorus pesticides in Gingko leaves by accelerated solvent extraction and gas chromatography with flame photometric detection. J. AOAC Int. 2005, 88, 729-735.
21. Anastassiades, M.; Lehotay, S. J.; Stajnbaher, D.; Schenck, F. J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. J. AOAC Int. 2003, 86 (2), 412-431.
22. Fillion, J.; Hindle, R.; Lacroix, M; Selwyn, J. Multiresidue determination of pesticides in fruit and vegetables by gas chromatography-mass selective detection and liquid chromatography with fluorescence detection. J. AOC Int. 1995, 78, 1252-1266.
23. Fillion, J.; Sauvé, F.; Selwyn, J. Multiresidue method for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromatography with fluorescence detection. J. AOAC Int. 2000, 83, 698-713.
24. Sannino, A.; Bolzoni, L.; Bandini, M. Application of liquid chromatography with electrospray tandem mass spectrometry to the determination of a new generation of pesticides in processed fruits and vegetables. J. Chromatogr., A. 2004, 1036, 161-169.
25. Ortelli, D.; Edder, P.; Corvi, C. Multiresidue analysis of 74 pesticides in fruits and vegetables by liquid chromatography-electrospray-tandem mass spectrometry. Anal. Chim. Acta. 2004, 520, 33-45.
26. Lehotay, S. J. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J. AOAC Int. 2007, 90 (2), 485-520.
27. Klein, J.; Alder, L. Applicability of gradient liquid chromatography with tandem mass spectrometry to the simultaneous screening for about 100 pesticides in crops. J. AOAC Int. 2003, 86, 1015-1037.
28. European Commission Council Directive 96/23/EEC and 2002/657/EC. http://ec.europa.eu/food/food/chemicalsafety/residues/council-directive-96-23ec. pdf and http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2002:221: 0008:0036:EN:PDF.