Bulk derivatization and direct injection of human cerebrospinal fluid for trace-level quantification of endogenous estrogens using trap-and-elute liquid chromatography with tandem mass spectrometry

Journal of Separation Science

Volumn 37, Issue 15, 2014, Pages 2010-2017

  Fan, Hui ^a   Papouskova, Barbora ^b   Lemr, Karel ^b   Wigginton, Jane G ^c   Schug, Kevin A ^a  

^a UNIVERSITY OF TEXAS AT ARLINGTON   (United States)

^b PALACKÝ UNIVERSITY   (Czech Republic)

^c UNIVERSITY OF TEXAS SOUTHWESTERN MEDICAL CENTER   (United States)

Author keywords

Endogenous estrogen; Estrogenic neuroprotection; Human cerebrospinal fluid; Restricted access media; Streamlined sample preparation

Indexed keywords

BRAIN; CHLORINE COMPOUNDS; DIFFUSION IN LIQUIDS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

ENDOGENOUS ESTROGEN; HUMAN CEREBROSPINAL FLUID; NEUROPROTECTION; RESTRICTED-ACCESS MEDIA; SAMPLE PREPARATION;

CEREBROSPINAL FLUID;

DANSYL CHLORIDE; ESTRADIOL; ESTRIOL; ESTRONE; ESTROGEN;

ACCURACY; ARTICLE; BLOOD BRAIN BARRIER; CALIBRATION; CEREBROSPINAL FLUID; CEREBROSPINAL FLUID ANALYSIS; DERIVATIZATION; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; LIMIT OF DETECTION; MASS SPECTROMETRY; PRIORITY JOURNAL; REPRODUCIBILITY; TANDEM MASS SPECTROMETRY; CHEMISTRY; EVALUATION STUDY; PROCEDURES;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ESTROGENS; HUMANS; TANDEM MASS SPECTROMETRY;

EID: 84904643824     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201400165     Document Type: Article

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