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Senapati N. Ultrasound in Chemical Processing. Advances in Sonochemistry 1991, 2. JAI Press. T.J. Mason (Ed.).
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Schram C.J. The Manipulation of Particles in an Ultrasonic Field. Advances in Sonochemistry 1991, 2. JAI Press. T.J. Mason (Ed.).
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84903930191
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BBC Television "The Ultrasonic Bunsen Burner" was shown on the popular science programme Tomorrow's World, February 14th
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BBC Television "The Ultrasonic Bunsen Burner" was shown on the popular science programme Tomorrow's World, February 14th, 1989.
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(b) J. L. Mascarenas, L.A. Sarandeses, L. Casedo and A. Mourino, Tetrahedron 47 (1991) 3485
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14
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84903914676
-
The zinc dust was purified by successive washing under magnetic stirring with 5% HCl (3 min), H2O (10 min), saturated NH4Cl (15 min), H2O (5 min), and EtOH (3h).
-
The solid was filtered, washed with EtOH and ethyl acetate, and dried in a dessicator over P2O5: L. F. Fieser and M. Fieser, "Reagents for Organic Synthesis" John Wiley & Sons
-
The zinc dust was purified by successive washing under magnetic stirring with 5% HCl (3 min), H2O (10 min), saturated NH4Cl (15 min), H2O (5 min), and EtOH (3h). The solid was filtered, washed with EtOH and ethyl acetate, and dried in a dessicator over P2O5: L. F. Fieser and M. Fieser, "Reagents for Organic Synthesis" John Wiley & Sons: 1967; vol 1, p1292.
-
(1967)
, vol.1
-
-
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16
-
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84903915983
-
-
TLC conditions: 20% ethyl acetate/hexane ; 1: Rf 0.55; 2: Rf 0.40; De-A,B-23,24-dinorcholan-8β-o1 (from the hydrogenation of 1: Rf 0.60.
-
TLC conditions: 20% ethyl acetate/hexane ; 1: Rf 0.55; 2: Rf 0.40; De-A,B-23,24-dinorcholan-8β-o1 (from the hydrogenation of 1: Rf 0.60.
-
-
-
-
17
-
-
33947093831
-
-
Flash chromatography was performed using silica gel (Merck 60, 230-400 mesh), according to the method of Still:
-
Still W.C., Mitra A. J. Am. Chem. Soc. 1987, 100:1927. Flash chromatography was performed using silica gel (Merck 60, 230-400 mesh), according to the method of Still:.
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23
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84903932696
-
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Three types of commercially available ultrasonic cleaning baths have been used satisfactorily in our laboratory: Transonic T570/H (frequency 35kHz from Elma, Germany); Sonorex RK 100H (frequency 35kHz from Bandelin Electronics, Germany); Bransonic 220 (frequency 35kHz from Branson, USA)
-
Three types of commercially available ultrasonic cleaning baths have been used satisfactorily in our laboratory: Transonic T570/H (frequency 35kHz from Elma, Germany); Sonorex RK 100H (frequency 35kHz from Bandelin Electronics, Germany); Bransonic 220 (frequency 35kHz from Branson, USA).
-
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27
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0031115790
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a) A.O. Miller, D. Peters, C. Zur, M. Frank and R. Miethchen, J. Fluorine Chem., 82 (1997) 33; b) C. Zur, Ph.D. thesis, University of Rostock, 1997.
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84903924671
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Ph.D. thesis, University of Rostock
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C. Zur, Ph.D. thesis, University of Rostock, 1997.
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Zur, C.1
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84903916921
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From reference 2, reproduced with permission
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From reference 2, pp 361-362, reproduced with permission.
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30
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0029113854
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(b) B. Bollbuck, P. Kraft, W. Tochtermann Tetrahedron, 52 (1996) 4581 and references cited therein
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33
-
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84903921811
-
-
The need for a small quantity of water in this preparation does not seem to be understood.
-
The need for a small quantity of water in this preparation does not seem to be understood.
-
-
-
-
34
-
-
84903912703
-
-
This procedure gives almost quantitative yields and is generally applicable for aromatic and heterocyclic aldehydes. A variety of solvents can be used e.g. EtOH (96%), cyclohexane, 1,4-dioxane and N,N-dimethylformamide.
-
This procedure gives almost quantitative yields and is generally applicable for aromatic and heterocyclic aldehydes. A variety of solvents can be used e.g. EtOH (96%), cyclohexane, 1,4-dioxane and N,N-dimethylformamide.
-
-
-
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35
-
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84903925553
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Raso A.Garcia, Raso J.Garcia, Campaner B., Mestres R., Sinisterra J.V. Synthesis 1982, 1037.
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40
-
-
84903910578
-
-
It is preferable to use the stoichiometric amount of ammonia for this neutralisation. It was observed that the yields are decreased by excess base.
-
It is preferable to use the stoichiometric amount of ammonia for this neutralisation. It was observed that the yields are decreased by excess base.
-
-
-
-
41
-
-
84903921218
-
-
At this stage, it is possible to separate ca. 5 5% of 1,2-isopropylideneglucofuranose.
-
At this stage, it is possible to separate ca. 5 5% of 1,2-isopropylideneglucofuranose.
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44
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84957764688
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Accidents with hydrogen fluoride HF or compounds that are prone to release HF can be one of the most hazardous injuries in the laboratory if precautions are neglected. The effects of HF on human tissue are substantially different from that of ordinary acids. An accident caused by HF, even if it appears minor or the contact is only suspected, must always be treated as a serious accident. Thus, before all experiments involving HF are started protection measures must be in place and a first aid box should be available. For details cf. ref. 5.
-
Accidents with hydrogen fluoride HF or compounds that are prone to release HF can be one of the most hazardous injuries in the laboratory if precautions are neglected. The effects of HF on human tissue are substantially different from that of ordinary acids. An accident caused by HF, even if it appears minor or the contact is only suspected, must always be treated as a serious accident. Thus, before all experiments involving HF are started protection measures must be in place and a first aid box should be available. For details cf. ref. 5.
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49
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From reference 2, reproduced with permission.
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In writing this chapter T.J.M. would like to acknowledge the help of a good friend who died some years ago.
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His name was Professor J. Berlan of the Ecole Nationale Superieure d'Ingenieurs de Genie Chimique, Toulouse, France. He was a true pioneer and innovator in the field of sonochernistry.
-
In writing this chapter T.J.M. would like to acknowledge the help of a good friend who died some years ago. His name was Professor J. Berlan of the Ecole Nationale Superieure d'Ingenieurs de Genie Chimique, Toulouse, France. He was a true pioneer and innovator in the field of sonochernistry.
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