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In contrast, a diffraction peak corresponding to the (101) plane of PdO at 2θ = 33.9° was not detected. The observed peak at 2θ = 39.3° was broad and its half-width was 0.035 radian Other definitive diffraction peaks were not observed. X-ray diffraction studies were performed for a sample obtained by using the following specific preparation conditions: initial concentration of tetrachloropalladate ions is 10 mM, isopropyl alcohol 100 mM, irradiation time 60 min.
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note
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When the concentration of t-BuOH is 1 mM, OH radicals produced by the sonolysis of water are perfectly scavenged in our experiment.
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