Sonochemical preparation of ultrafine palladium particles

Chemistry of Materials

Volumn 8, Issue 2, 1996, Pages 315-317

  Okitsu, Kenji ^a   Bandow, Hiroshi ^a   Maeda, Yasuaki ^a   Nagata, Yoshio ^a  

^a Osaka Prefecture University   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000968452     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm950285s     Document Type: Article

References (26)

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20. In contrast, a diffraction peak corresponding to the (101) plane of PdO at 2θ = 33.9° was not detected. The observed peak at 2θ = 39.3° was broad and its half-width was 0.035 radian Other definitive diffraction peaks were not observed. X-ray diffraction studies were performed for a sample obtained by using the following specific preparation conditions: initial concentration of tetrachloropalladate ions is 10 mM, isopropyl alcohol 100 mM, irradiation time 60 min.
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26. When the concentration of t-BuOH is 1 mM, OH radicals produced by the sonolysis of water are perfectly scavenged in our experiment.