Column Technology in Liquid Chromatography

Liquid Chromatography: Fundamentals and Instrumentation

Volumn , Issue , 2013, Pages 41-86

  Unger, K K ^a   Lamotte, S ^b   Machtejevas, E ^c  

^a JOHANNES GUTENBERG UNIVERSITY   (Germany)

^b BASF SE GKC/V M320   (Germany)

^c MERCK KGAA   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84901861611     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1016/B978-0-12-415807-8.00003-1     Document Type: Chapter

References (65)

1. Unger K.K., Machtejevas E., Skudas R., Ditz R. Liquid chromatography - its development and key role in life science applications. Angew Chem Int Ed 2010, 49:2300.
2. Ettre L.S. Chapters in the evolution of chromatography 2008, Imperial College Press, London. J.V. Hinshaw (Ed.).
3. van Deemter J.J., Zuiderweg F.J., Klinkenberg A. Longidutinal diffusion and resistance to mass transfer as causes of nonideality in chromatography. Chem Eng Sci 1956, 5:271.
4. Giddings J.C. Unified separation science 1992, John Wiley & Sons, New York.
5. Wang J.C., Liapis A.I. Design of polymeric porous adsorbent media and the dynamic behavior of transport and adsorption of bioactive molecules in such media. Chem Ing Tech 2011, 83:152.
6. Unger K.K., Skudas R., Schulte M. Particle packed columns and monolithic columns in HPLC - a comparison and critical appraisal. J Chromatogr A 2008, 1184:393.
7. Golay M.J.E. Gas chromatography 1960, Edinburgh 1960, 139. Butterworths, London. R.P.W. Scott (Ed.).
8. Horvath C., Preiss B.A., Lipsky S.R. Fast liquid chromatography: An investigation of operating parameters and the separation of nucleotides on pellicular ion exchangers. Anal Chem 1967, 39:1422.
9. Majors R.J. Twenty-five years of HPLC column development - a commercial perspective. LCGC 1994, 12:508.
10. Vivilecchia R.V., Cotter R.L., Limpert R.J., Thimot N.Z., Little J.N. Considerations of small particles in different modes of liquid chromatography. J Chromatogr 1974, 99:407.
11. Poppe H. Some reflections on speed and efficiency of modern chromatographic methods. J Chromatogr 1997, 778:3. Halasz I, Endele R, Assauer J, Ultimate limits in high pressure liquid chromatography, J Chromatogr 1975:112:7.
12. Neue U.D. HPLC columns: theory, technology and practice 1997, Wiley-VCH, New York.
13. Guiochon G. HPLC: advances and perspectives 1980, vol. 2:1. Academic Press, London. C. Horvath (Ed.).
14. Bente P.F., Zerenner E.H., Dandeneau R.D. U.S. patent 4,293,415, silica chromatographic column October 6, 1981.
15. Hamacher M., Marcus K., Stuehler K., Van Hall A., Wahrscheid B., Meyer H.E. Proteomics in drug research 2006, Wiley-VCH, Weinheim, Germany.
16. Kister H.Z. Distillation design 1992, McGraw-Hill, New York.
17. du Fresne, von Hohenesche C., Ehwald V., Unger K.K. Development of standard operation procedures for the manufacture of n-octadecyl bonded silica particles in certified reference columns for reversed phase liquid chromatogarphy. J Chromatogr A 2004, 1025:177.
18. Avery R.G., Ramsay J.D.F. The sorption of nitrogen in porous compacts of silica and zirconia powders. J Colloid Interface Sci 1973, 42:597.
19. Unger K.K., Tanaka N., Machtejevas E. Monolithic silicas in separation science 2010, Wiley-VCH, Weinheim, Germany.
20. Unger K.K. Packings and stationary phases in chromatographic techniques 1990, Marcel Dekker, New York.
21. Rouquerol F, F, J, Rouquerol J, Singk SW. Table 1.3, Adsorption by powders and poroussolids. New York: Academic Press; 1999. p. 8.
22. Engelhardt H., Elgass H. Liquid chromatography on silica and alumina as stationary phases. HPLC: advances and perspectives 1980, vol. 2:45. Academic Press, New York. C. Horvath (Ed.).
23. Endele R., Halasz I., Unger K.K. Influence of the particle size ( 5 - 35 μm) of spherical silica on column efficiency in HPLC. J Chromatogr 1974, 99:377.
24. Gritti F., Guiochon G. Kinetic investigation of the relationship between the efficiency of column and their diameter. J Chromatogr A 2011, 1218:1592.
25. Barber W.E., Proske A.D., Langlois T. U.S. patent 7,309,426 2007, 18. December.
26. Dewaele C., Verzele M. Influence of the particle size distribution of the paking material in reversed-phase high-performance liquid chromatography. J Chromatogr 1983, 260:13.
27. Rouquerol F., Rouquerol J., Sing K.S.W. Adsorption by powders and porous solids 1999, Academic Press, New York.
28. Liapis A.I., Myers J.J., Grosser O.K. Modeling and simulation of the dynamic behavior of monoliths: effects of pore structure from pore network model analysis and comparison with columns packed with porous spherical particles. J Chromatog A 1999, 865:13.
29. Myers J.J., Nahar S., Ludlow D.K., Liapis A.I. Determination of the pore connectivity and pore size distribution and pore spatial distribution of porous chromatographic particles from nitrogen sorption measurements and pore network modelling theory. J Chromatogr A 2001, 907:57.
30. Unger K.K., Bidlingmaier B., Du Fresne von Hohenesche C., Lubda D. Evaluation and comparison of the pore structure and related properties of particulate and monolithic silica for liquid phase separation processes. Studies in surface science and catalysis 2002, 144:115-122. Elsevier, Amsterdam. F. Rodriguez-Reinoso, B. Mc Enany, J. Rouquerol, K.K. Unger (Eds.).
31. Grimes B.A., Skudas R., Unger K.K., Lubda D. Pore structural characterization of monolithic silica columns by inverse size exclusion chromatography. J Chromatogr A 2007, 1144:14.
32. Myers J.J., Liapis A.I. Network model of the convective flow and diffusion of of molecules adsorbing in continuous beds and in porous particles packed in a chromatographic column. J Chromatogr A 1998, 827:197.
33. Ullmanns encyclopedia of industrial chemistry 1993, vol. A 23. VCH, Weinheim, Germany, Chapter 6.
34. Unger K.K. Porous silica-its properties and use in column liquid chromatography 1979, Elsevier, Amsterdam.
35. Neue U.D. HPLC columns: theory, technology and practice 1997, Table 9.2, p. 173, Wiley-VCH, New York.
36. Vansant E.F., Van Der Voort P., Kraaken K.C. Characterization and chemical modification of the silica surface 1995, Elsevier, Amsterdam.
37. Pfleiderer B., Albert K., Lork K.-D., Unger K.K., Brueckner H., Bayer E Correlation of the dynamic behavior of n-alkyl ligands of stationary phases with the retention of paracelsin peptides by reversed phase HPLC. Angew Chem 1989, 101:336. Hanson M, Unger KK, Schmid J, Albert K, Bayer E, Effect of the chain mobility of polymeric reversed phase stationary phases on polypeptide retention, Anal Chem 1993:65:2249.
38. Knox J.H. High performance liquid chromatography 1978, Edinburgh University Press, Edinburgh.
39. Roumeliotis P., Chatziathanassiou M., Unger K.K. Study on the efficiency of assembled micro bore columns in HPLC. Chromatographia 1984, 19:145. Chatziathanassiou M, Packed microbore columns for HPLC: system development and analytical application, Ph.D. thesis, University of Mainz, Germany, 1987.
40. Guiochon G., Shirazi S.G., Katti A.M. Fundamentals of preparative and nonlinear chromatography 1994, Academic Press, New York.
41. Snyder L.R., Kirkland J.J., Glajch J.L. Practical HPLC development 1997, John Wiley & Sons, New York, p. 50.
42. Comparison guide to C18 reversed phase columns June 2008, MAC-MOD Analytics, Chadds Ford, PA.
43. Neue U.D. Stationary phase characterization and method development. J Sep Sci 2007, 30:164.
44. Engelhardt H., Jungheim M. Comparison and characterization of reversed phases. Chromatographia 1990, 29:59.
45. Sander L.C., Wise S.A. Synthesis and characterization of polymeric C18 stationary phases for liquid chromatography. Anal Chem 1984, 56:504. Sander LC, Wise SA, Shape selectivity in reversed-phase liquid chromatography for the separation of planar and non planar solutes, J Chromatogr A 1993:656:335. Sander LC, Wise SA, Influence of stationary phase chemistry on shape recognition in liquid chromatography, Anal Chem 1995:67:3284.
46. Kimata K., Iwaguchi S., Onishi S., Jinno K., Ekstee R., Hosoya K., et al. Chromatographic characterization of silica C18 packing materials. Correlation between a preparation method and retention behavior of stationary phase. J Chromatogr Sci 1989, 27:721.
47. McCalley D.V. Selection of suitable stationary phases and optimum conditions for their application in the separation of basic compounds by reversed-phase HPLC. J Sep Sci 2003, 26:187. McCalley DV. Effect of organic solvent modifier and nature of solute on the performance of bonded silica reversed-phase columns for the analysis of strongly basic compounds by high-performance liquid chromatography. J Chromatogr A 1996:738:169. McCalley DV. Comparative evaluation of bonded-silica reversed-phase columns for high-performance liquid chromatography using strongly basic compounds and alternative organic modifiers buffered at acidic pH. J Chroatogr A 1997:769:169. Breretron RG, McCalley DV. High-performance liquid chromatography of basic compounds: problems, possible solutions and tests of reversed-phase columns. J Chromatogr A 1998:828:407.
48. McDonald P. The quest for UPLC 2009, Waters Corp, Milford, MA.
49. Setzer C., van Essche G., Pryor N. Oxides: silica. Handbook of porous solids, vol. 3 2002, 1543. Wiley-VCH, Weinheim, Germany. F. Schueth, K.S.W. Sing, J. Weitkamp (Eds.).
50. Iler R.K. The chemistry of silica 1979, John Wiley & Sons, New York.
51. Bergna H.E. The colloid chemistry of silica 1994, American Chemical Society, Washington, DC.
52. Brinker C.J., Scherer G.W. Sol-gel science 1990, Academic Press, New York.
53. Papirer E. Adsorption on silica surfaces 2000, Marcel Dekker, New York.
54. Di Renzo F., Galarneau A., Trens P., Fajula F. Ordered mesoporous oxides: micelle-templated materials. Handbook of porous solids, vol. 3 2002, 1311-1359. Wiley-VCH, Weinheim, Germany. F. Schüth, K.S.W. Sing, J. Weitkamp (Eds.).
55. Noll W. Chemistry and technology of silicones 1968, Academic Press, New York.
56. Bayram-Hahn Z., Grimes B.A., Lind A., Skudas R., Unger K.K., Galarneau A., et al. Pore structural characterization, size exclusion properties and column performance of two mesoporous amorphous silica and their pseudomorphically transformed MCM-41 derivatives. J Sep Sci 2007, 30:3089. Iapichella J, Meneses J-M, Beurroies I, Denoyel R, Bayram-Hahn Z, Unger KK, Galarneau A. Characterization of mesoporous silica and its pseudomorphically transformed derivative by gas and liquid adsorption, Micropor Mesopor Mater 2007:102:111.
57. Tanaka N., Kobayashi H., Ishizuka N., Minaguchi H., Nakanishi K., Hosoya K., et al. Monolithic silica columns for high-efficiency chromatographic separations. J Chromatogr A 2002, 965:35.
58. Gzil P., Verwoort N., Baron G.V., Desmet G. General rules for the optimal external porosity of LC supports. Anal Chem 2004, 76:6707. Desmet G, Clicq D, Gzil P. Geometry-independent plate height representation methods for the direct comparison of the kinetic performance of LC supports with a different size or morphology. Anal Chem 2005:77:4058-4070. Desmet G, Clicq D, Ngguyen DT-T, Guillarme D, Rudaz S, Veuthey J-L, Vervoort N, Torok G, Cabooter D, Gzil P. Practical constraints in the kinetic plot representation of chromatographic performance data: theory and application to experimental data. Anal Chem 2006:78:2150.
59. MacNair J.E., Lewis K.C., Jorgensen J.W. Ultrahigh-pressure reversed phase liquid chromatography in packed capillary columns. Anal Chem 1997, 69:983.
60. Nyiredi S., Szucs Z., Szepezy L. Stationary phase optimized selectivity liquid chromatography: basic possibilities of serial connected columns using the PRISMA principle. J Chromatogr A 2007, 1157:122. Nyiredi S, Szucs Z, Szepezy L. Stationary phase optimized selectivity LC (SOS-LC): separation examples and practical aspects. Chromatographia Supplement 2006:63:S3.
61. Smith R.M., Subba Rao P.V., Dube S., Shah H. Problems of the interlaboaratory transferability of the measurement of the properties of a reversed phase HPLC column. Chromatographia 2003, 57:S-27.
62. Pettersson P., Euerby M.R. Characterization of RPLC columns packed with porous sub-2μm particles. J Sep Sci 2007, 30:2012.
63. De Stefano J., Schuster S.J., Lawhorn J.M., Kirkland J.J. Performance characteristics of new superficially porous particles. J Chromatogr A 2012, 1258:76.
64. Wagner BM., Schuster S.A., Boyes B.E., Kirkland J.J. Superficially porous silica particles with wide pores for biomacromolecular separations. J Chromatogr A 2012, 1264:22.
65. Ekstroem LG, Strategic Directions International Inc, UK.