Development and validation of an LC-MS/MS based method for quantification of 25 hydroxyvitamin D2 and 25 hydroxyvitamin D3 in human serum and plasma

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 961, Issue , 2014, Pages 62-70

  Zhang, Stanley ^a   Jian, Wenying ^b   Sullivan, Sheryl ^a   Sankaran, Banu ^a   Edom, Richard W ^b   Weng, Naidong ^b   Sharkey, David ^a  

^a Ortho McNeil Pharmaceutical Incorporated   (United States)

^b JANSSEN RESEARCH AND DEVELOPMENT   (Belgium)

Author keywords

25 Hydroxyvitamin D; LC MS MS; Matrix comparison; Method comparison; Stability; Validation

Indexed keywords

CONVERGENCE OF NUMERICAL METHODS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PLASMAS; PROTEINS; VITAMINS;

25-HYDROXYVITAMIN D; LC-MS/MS; LIQUID-LIQUID EXTRACTION PROCEDURE; METHOD COMPARISON; POTENTIAL INTERFERENCES; QUADRUPOLE MASS SPECTROMETRY; VALIDATION; VITAMIN D-BINDING PROTEINS;

BODY FLUIDS;

25 HYDROXYERGOCALCIFEROL; CALCIFEDIOL; COLECALCIFEROL;

ANIMAL; BLOOD; CHILD; COMPARATIVE STUDY; DRUG STABILITY; FEMALE; HORSE; HUMAN; LIMIT OF DETECTION; LIQUID LIQUID EXTRACTION; MALE; PROCEDURES; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY; VALIDATION STUDY;

25-HYDROXYVITAMIN D 2; ANIMALS; CALCIFEDIOL; CHILD; CHOLECALCIFEROL; DRUG STABILITY; FEMALE; HORSES; HUMANS; LIMIT OF DETECTION; LIQUID-LIQUID EXTRACTION; MALE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

EID: 84901311405     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2014.05.006     Document Type: Article

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