Quantification of C=C and C=O surface carbons in detonation nanodiamond by NMR

Journal of Physical Chemistry C

Volumn 118, Issue 18, 2014, Pages 9621-9627

  Cui, J F ^a   Fang, X W ^a   Schmidt Rohr, K ^a  

^a IOWA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AROMATIC COMPOUNDS; BOND LENGTH; CARBON; DETONATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROTONATION;

AROMATIC FRACTION; CARBON FRACTION; CROSS POLARIZATIONS; DETONATION NANODIAMOND; DIAMOND PARTICLES; NANO-DIAMOND PARTICLES; SURFACE CARBON; SURFACE FRACTION;

NANODIAMONDS;

EID: 84900415095     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/jp503053r     Document Type: Article

References (48)

1. Greiner, N. R.; Phillips, D. S.; Johnson, J. D.; Volk, F. Diamonds in Detonation Soot Nature (London) 1988, 333, 440-442
2. Iakoubovskii, K.; Baidakova, M. V.; Wouters, B. H.; Stesmans, A.; Adriaenssens, G. J.; Vul, A. Y.; Grobet, P. J. Structure and Defects of Detonation Synthesis Nanodiamond Diamond Relat. Mater. 2000, 9, 861-865
3. Iakoubovskii, K.; Mitsuishi, K.; Furuya, K. High-Resolution Electron Microscopy of Detonation Nanodiamond Nanotechnology 2008, 19, 155705/155701-155705/155705
4. Krueger, A.; Kataoka, F.; Ozawa, M.; Fujino, T.; Suzuki, Y.; Aleksenskii, A. E.; Vul, A. Y.; Osawa, E. Unusually Tight Aggregation in Detonation Nanodiamond: Identification and Disintegration Carbon 2005, 43, 1722-1730
5. Ozawa, M.; Inaguma, M.; Takahashi, M.; Kataoka, F.; Krüger, A.; Ōsawa, E. Preparation and Behavior of Brownish, Clear Nanodiamond Colloids Adv. Mater. 2007, 19, 1201-1206
6. Dolmatov, V. Y. Detonation Synthesis Ultradispersed Diamonds: Properties and Applications Russ. Chem. Rev. 2001, 70, 607-626
7. Mochalin, V. N.; Shenderova, O.; Ho, D.; Gogotsi, Y. The Properties and Applications of Nanodiamonds Nat. Nanotechnol. 2012, 7, 11-23
8. Behler, K. D.; Stravato, A.; Mochalin, V.; Korneva, G.; Yushin, G.; Gogotsi, Y. Nanodiamond-Polymer Composite Fibers and Coatings ACS Nano 2009, 3, 363-369
9. Zhang, Q.; Neitzel, I.; Mochalin, V. N.; Knoke, I.; Wotton, D. M.; Gogotsi, Y.; Lelkes, P. I.; Zhou, J. G. PLLA-Nanodiamond Composites and Their Application in Bone Tissue Engineering Proc. ASME Global Congr. NanoEng. Med. Biol. 2010, 241-242
10. Maitra, U.; Prasad, K. E.; Ramamurty, U.; Rao, C. N. R. Mechanical Properties of Nanodiamond-Reinforced Polymer-Matrix Composites Solid State Commun. 2009, 149, 1693-1697
11. Neitzel, I.; Mochalin, V.; Knoke, I.; Palmese, G. R.; Gogotsi, Y. Mechanical Properties of Epoxy Composites with High Contents of Nanodiamond Compos. Sci. Technol. 2011, 71, 710-716
12. Zhang, J.; Su, D. S.; Blume, R.; Schlögl, R.; Wang, R.; Yang, X.; Gajović, A. Surface Chemistry and Catalytic Reactivity of a Nanodiamond in the Steam-Free Dehydrogenation of Ethylbenzene Angew. Chem., Int. Ed. 2010, 49, 8640-8644
13. Liu, K.-K.; Zheng, W.-W.; Wang, C.-C.; Chiu, Y.-C.; Cheng, C.-L.; Lo, Y.-S.; Chen, C.; Chao, J.-I. Covalent Linkage of Nanodiamond-Paclitaxel for Drug Delivery and Cancer Therapy Nanotechnology 2010, 21, 315106/315101-315106/ 315114
14. Chow, E. K.; Zhang, X.-Q.; Chen, M.; Lam, R.; Robinson, E.; Huang, H.; Schaffer, D.; Osawa, E.; Goga, A.; Ho, D. Nanodiamond Therapeutic Delivery Agents Mediate Enhanced Chemoresistant Tumor Treatment Sci. Transl. Med. 2011, 3, 73ra21
15. Krueger, A. The Structure and Reactivity of Nanoscale Diamond J. Mater. Chem. 2008, 18, 1485-1492
16. Krueger, A.; Lang, D. Functionality is Key: Recent Progress in the Surface Modification of Nanodiamond Adv. Funct. Mater. 2012, 22, 890-906
17. Fang, X.; Mao, J.; Levin, E. M.; Schmidt-Rohr, K. Nonaromatic Core-Shell Structure of Nanodiamond from Solid-State NMR Spectroscopy J. Am. Chem. Soc. 2009, 131, 1426-1435
18. Raty, J. Y.; Galli, G. In Synthesis, Properties and Applications of Ultrananocrystalline Diamond; Gruen, D.; Shenderova, O.; Vul , A., Eds.; Springer: Netherlands, 2005; Vol. 192, pp 15-24.
19. Barnard, A. S.; Sternberg, M. Substitutional Nitrogen in Nanodiamond and Bucky-Diamond Particles J. Phys. Chem. B 2005, 109, 17107-17112
20. Butenko, Y. V.; Kuznetsov, V. L.; Paukshtis, E. A.; Stadnichenko, A. I.; Mazov, I. N.; Moseenkov, S. I.; Boronin, A. I.; Kosheev, S. V. The Thermal Stability of Nanodiamond Surface Groups and Onset of Nanodiamond Graphitization Fullerenes, Nanotubes, Carbon Nanostruct. 2006, 14, 557-564
21. Kuznetsov, V. L.; Butenko, Y. V. In Synthesis, Properties and Applications of Ultrananocrystalline Diamond; Gruen, D.; Shenderova, O.; Vul , A., Eds.; Springer: Netherlands, 2005; Vol. 192, pp 199-216.
22. Petit, T.; Arnault, J.-C.; Girard, H. A.; Sennour, M.; Bergonzo, P. Early Stages of Surface Graphitization on Nanodiamond Probed by X-Ray Photoelectron Spectroscopy Phys. Rev. B: Condens. Matter Mater. Phys. 2011, 84, 233407/233401-233407/233405
23. Petit, T.; Arnault, J. C.; Girard, H. A.; Sennour, M.; Kang, T.-Y.; Cheng, C.-L.; Bergonzo, P. Oxygen Hole Doping of Nanodiamond Nanoscale 2012, 4, 6792-6799
24. 13C Magic Angle Spinning NMR Spectroscopy Characterization of Particle Size Structural Variations in Synthetic Nanodiamonds Mater. Chem. Phys. 2004, 85, 310-315
25. Dubois, M.; Guerin, K.; Petit, E.; Batisse, N.; Hamwi, A.; Komatsu, N.; Giraudet, J.; Pirotte, P.; Masin, F. Solid-State NMR Study of Nanodiamonds Produced by the Detonation Technique J. Phys. Chem. C 2009, 113, 10371-10378
26. Dubois, M.; Guerin, K.; Batisse, N.; Petit, E.; Hamwi, A.; Komatsu, N.; Kharbache, H.; Pirotte, P.; Masin, F. Solid State NMR Study of Nanodiamond Surface Chemistry Solid State Nucl. Magn. Reson. 2011, 40, 144-154
27. Shenderova, O.; Panich, A. M.; Moseenkov, S.; Hens, S. C.; Kuznetsov, V.; Vieth, H. M. Hydroxylated Detonation Nanodiamond: FTIR, XPS, and NMR Studies J. Phys. Chem. C 2011, 115, 19005-19011
28. Panich, A. M.; Shames, A. I.; Sergeev, N. A.; Olszewski, M.; McDonough, J. K.; Mochalin, V. N.; Gogotsi, Y. Nanodiamond Graphitization: A Magnetic Resonance Study J. Phys. Condens. Matter 2013, 25, 245303
29. Osswald, S.; Yushin, G.; Mochalin, V.; Kucheyev, S. O.; Gogotsi, Y. Control of sp2/sp3 Carbon Ratio and Surface Chemistry of Nanodiamond Powders by Selective Oxidation in Air J. Am. Chem. Soc. 2006, 128, 11635-11642
30. Durham, P. J. Theory of XANES Chem. Anal. (N. Y.) 1988, 92, 53-84
31. Penner-Hahn, J. E. X-Ray Absorption Spectroscopy in Coordination Chemistry Coord. Chem. Rev. 1999, 190-192, 1101-1123
32. Newville, M. Fundamentals of XAFS; Consortium for Advanced Radiation Sources: Chicago, 2004.
33. Panich, A. M.; Shames, A. I.; Vieth, H. M.; Osawa, E.; Takahashi, M.; Vul, A. Y. Nuclear Magnetic Resonance Study of Ultrananocrystalline Diamonds Eur. Phys. J. B 2006, 52, 397-402
34. Panich, A. M. Nuclear Magnetic Resonance Studies of Nanodiamonds Crit. Rev. Solid State Mater. Sci. 2012, 37, 276-303
35. Chen, J.; Deng, S. Z.; Chen, J.; Yu, Z. X.; Xu, N. S. Graphitization of Nanodiamond Powder Annealed in Argon Ambient Appl. Phys. Lett. 1999, 74, 3651-3653
36. Zeppilli, S.; Arnault, J. C.; Gesset, C.; Bergonzo, P.; Polini, R. Thermal Stability and Surface Modifications of Detonation Diamond Nanoparticles Studied with X-Ray Photoelectron Spectroscopy Diamond Relat. Mater. 2010, 19, 846-853
37. Mochalin, V. N.; Osswald, S.; Portet, C.; Yushin, G.; Hobson, C.; Havel, M.; Gogotsi, Y. High Temperature Functionalization and Surface Modification of Nanodiamond Powders Mater. Res. Soc. Symp. Proc. 2008, 1039, 1039-P1011-1003
38. Bennett, A. E.; Rienstra, C. M.; Auger, M.; Lakshmi, K. V.; Griffin, R. G. Heteronuclear Decoupling in Rotating Solids J. Chem. Phys. 1995, 103, 6951-6958
39. Mao, J. D.; Schmidt-Rohr, K. Accurate Quantification of Aromaticity and Nonprotonated Aromatic Carbon Fraction in Natural Organic Matter by 13C Solid-State Nuclear Magnetic Resonance Environ. Sci. Technol. 2004, 38, 2680-2684
40. Morcombe, C. R.; Zilm, K. W. Chemical Shift Referencing in MAS Solid State NMR J. Magn. Reson. 2003, 162, 479-486
41. Zhang, X. B.; Zhang, X. F.; Bernaerts, D.; Van Tendeloo, G.; Amelinckx, S.; Van Landuyt, J.; Ivanov, V.; Nagy, J. B.; Lambin, P.; Lucas, A. A. The Texture of Catalytically Grown Coil-Shaped Carbon Nanotubules Europhys. Lett. 1994, 27, 141-146
42. Aoki, Y.; Mitsuoka, Y.; Nakamuta, Y. Arrowhead-like Diamond Crystals Formed by Hot-Filament Chemical Vapor Deposition Diamond Relat. Mater. 1999, 8, 1310-1314
43. Bursill, L. A.; Fullerton, A. L.; Bourgeois, L. N. Size and Surface Structure of Diamond Nanocrystals Int. J. Mod. Phys. B 2001, 15, 4087-4102
44. Shames, A. I.; Osipov, V. Y.; Aleksenskiy, A. E.; Osawa, E.; Vul, A. Y. Locating Inherent Unpaired Orbital Spins in Detonation Nanodiamonds through the Targeted Surface Decoration by Paramagnetic Probes Diamond Relat. Mater. 2011, 20, 318-321
45. Scholze, A.; Schmidt, W. G.; Bechstedt, F. Structure of the Diamond (111) Surface: Single-Dangling-Bond Versus Triple-Dangling-Bond Face Phys. Rev. B 1996, 53, 13725-13733
46. Mao, J. D.; Schmidt-Rohr, K. Recoupled Long-Range C-H Dipolar Dephasing in Solid-State NMR, and Its Use for Spectral Selection of Fused Aromatic Rings J. Magn. Reson. 2003, 162, 217-227
47. Raty, J. Y.; Galli, G. Optical Properties and Structure of Nanodiamonds J. Electroanal. Chem. 2005, 584, 9-12
48. Butenko, Y. V.; Krishnamurthy, S.; Chakraborty, A. K.; Kuznetsov, V. L.; Dhanak, V. R.; Hunt, M. R. C.; Šiller, L. Photoemission Study of Onionlike Carbons Produced by Annealing Nanodiamonds Phys. Rev. B 2005, 71, 075420