N,N′-Bis(2,6-diisopropylphenyl)benzamidinates and -pivalamidinates of the s-block metals lithium, potassium, and calcium

European Journal of Inorganic Chemistry

Volumn , Issue 8, 2014, Pages 1312-1321

  Loh, Claas ^a   Seupel, Susanne ^a   Görls, Helmar ^a   Krieck, Sven ^a   Westerhausen, Matthias ^a  

^a FRIEDRICH SCHILLER UNIVERSITY JENA   (Germany)

Author keywords

Alkali metals; Alkaline earth metals; Coordination modes; N ligands; Structure elucidation

Indexed keywords

ALKALINITY; CALCIUM COMPOUNDS; CRYSTAL STRUCTURE; LIGANDS; LITHIUM; POSITIVE IONS; POTASSIUM; ORGANIC SOLVENTS;

ALKALINE-EARTH METALS; AMIDINATES; COORDINATION MODES; METALATIONS; N LIGANDS; N-LIGANDS; S-BLOCK METALS; STRUCTURE ELUCIDATION; TETRA-HYDROFURAN; TETRAHYDROFURANS;

CALCIUM;

EID: 84897585718     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.201301557     Document Type: Article

References (47)

1. F. T. Edelmann, Adv. Organomet. Chem. 2008, 57, 183-352.
2. F. T. Edelmann, Adv. Organomet. Chem. 2013, 61, 55-374.
3. C. Jones, A. Stasch, Top. Organomet. Chem. 2013, 45, 73-101.
4. A. Stasch, C. Jones, Dalton Trans. 2011, 40, 5659-5672.
5. M. Westerhausen, Angew. Chem. 2008, 120, 2215-2217; Angew. Chem. Int. Ed. 2008, 47, 2185 -2187.
6. S. P. Green, C. Jones, A. Stasch, Science 2007, 318, 1754-1757.
7. M. Westerhausen, W. Schwarz, Z. Naturforsch. B 1992, 47, 453-459.
8. M. L. Cole, G. B. Deacon, C. M. Forsyth, K. Konstas, P. C. Junk, Dalton Trans. 2006, 3360-3367.
9. M. L. Cole, P. C. Junk, New J. Chem. 2005, 29, 135-140.
10. C. Glock, C. Loh, H. Görls, S. Krieck, M. Westerhausen, Eur. J. Inorg. Chem. 2013, 3261-3269.
11. A. G. M. Barrett, M. R. Crimmin, M. S. Hill, P. B. Hitchcock, S. L. Lomas, M. F. Mahon, P. A. Procopiou, Dalton Trans. 2010, 39, 7393-7400.
12. F. Feil, S. Harder, Eur. J. Inorg. Chem. 2005, 4438-4443.
13. M. R. Crimmin, A. G. M. Barrett, M. S. Hill, P. B. Hitchcock, P. A. Procopiou, Organometallics 2008, 27, 497-499.
14. T. M. A. Al-Shboul, G. Volland, H. Görls, M. Westerhausen, Z. Anorg. Allg. Chem. 2009, 635, 1568-1572.
15. H. Hu, C. Cui, Organometallics 2012, 31, 1208-1211.
16. C. A. Nijhuis, E. Jellema, T. J. J. Sciarone, A. Meetsma, P. H. M. Budzelaar, B. Hessen, Eur. J. Inorg. Chem. 2005, 2089-2099.
17. R. P. Rose, C. Jones, C. Schulten, S. Aldridge, A. Stasch, Chem. Eur. J. 2008, 14, 8477-8480.
18. C. Jones, C. Schulten, R. P. Rose, A. Stasch, S. Aldridge, W. D. Woodul, K. S. Murray, B. Moubaraki, M. Brynda, G. La Macchia, L. Gagliardi, Angew. Chem. 2009, 121, 7542-7546; Angew. Chem. Int. Ed. 2009, 48, 7406 -7410.
19. C. Jones, L. Furness, S. Nembenna, R. P. Rose, S. Aldridge, A. Stasch, Dalton Trans. 2010, 39, 8788-8795.
20. L. Fohlmeister, S. Liu, C. Schulten, B. Moubaraki, A. Stasch, J. D. Cashion, K. S. Murray, L. Gagliardi, C. Jones, Angew. Chem. 2012, 124, 8419; Angew. Chem. Int. Ed. 2012, 51, 8294-8298.
21. D. Heitmann, C. Jones, D. P. Mills, A. Stasch, Dalton Trans. 2010, 39, 1877-1882.
22. C. Jones, P. C. Junk, J. A. Platts, D. Rathmann, A. Stasch, Dalton Trans. 2005, 2497-2499.
23. C. Jones, S. J. Bonyhady, N. Holzmann, G. Frenking, A. Stasch, Inorg. Chem. 2011, 50, 12315-12325.
24. Y.-C. Tsai, H.-Z. Chen, C.-C. Chang, J.-S. K. Yu, G.-H. Lee, Y. Wang, T.-S. Kuo, J. Am. Chem. Soc. 2009, 131, 12534-12535.
25. N. Nimitsiriwat, V. C. Gibson, E. L. Marshall, P. Takolpuckdee, A. K. Tomov, A. J. P. White, D. J. Williams, M. R. J. Elsegood, S. H. Dale, Inorg. Chem. 2007, 46, 9988-9997.
26. R. T. Boeré, M. L. Cole, P. C. Junk, New J. Chem. 2005, 29, 128-134.
27. A. Xia, H. M. El-Kaderi, M. J. Heeg, C. H. Winter, J. Organomet. Chem. 2003, 682, 224-232.
28. M. L. Cole, P. C. Junk, New J. Chem. 2005, 29, 135-140.
29. M. L. Cole, G. B. Deacon, C. M. Forsyth, K. Konstas, P. C. Junk, Dalton Trans. 2006, 3360-3367.
30. S. Bambirra, D. van Leusen, A. Meetsma, B. Hessen, J. H. Teuben, Chem. Commun. 2003, 522-523.
31. A. V. Karpov, A. S. Shavyrin, A. V. Cherkasov, G. K. Fukin, A. A. Trifonov, Organometallics 2012, 31, 5349-5357.
32. G. Jin, C. Jones, P. C. Junk, K.-A. Lippert, R. P. Rose, A. Stasch, New J. Chem. 2009, 33, 64-75.
33. S. Schmidt, S. Schulz, D. Bläser, R. Boese, M. Bolte, Organometallics 2010, 29, 6097-6103.
34. A. F. Holleman, E. Wiberg, N. Wiberg, Lehrbuch der Anorganischen Chemie, 101. ed., W. de Gruyter, Berlin, 1995.
35. R. T. Boeré, V. Klassen, G. Wolmershäuser, J. Chem. Soc., Dalton Trans. 1998, 4147-4154.
36. M. Westerhausen, W. Schwarz, Z. Anorg. Allg. Chem. 1991, 604, 127-140.
37. M. Westerhausen, M. Hartmann, N. Makropoulos, B. Wieneke, M. Wieneke, W. Schwarz, D. Stalke, Z. Naturforsch. B 1998, 53, 117-125.
38. M. Westerhausen, Trends Organomet. Chem. 1997, 2, 89-105.
39. M. Westerhausen, Coord. Chem. Rev. 1998, 176, 157-210.
40. K. F. Tesh, T. P. Hanusa, J. C. Huffman, Inorg. Chem. 1990, 29, 1584-1586.
41. D. Mootz, A. Zinnius, B. Böttcher, Angew. Chem. 1969, 81, 398-399; Angew. Chem. Int. Ed. Engl. 1969, 8, 378 -379.
42. R. D. Rogers, J. L. Atwood, R. Grüning, J. Organomet. Chem. 1978, 157, 229-237.
43. R. Hooft, COLLECT, Data Collection Software, Nonius B. V., Delft, The Netherlands, 1998.
44. Z. Otwinowski, W. Minor, in: Processing of X-ray Diffraction Data Collected in Oscillation Mode (Eds.:, C. W. Carter, R. M. Sweet), Methods in Enzymology, vol. 276, Macromolecular Crystallography, part A, Academic Press, New York, 1997, p. 307-326.
45. G. M. Sheldrick, Acta Crystallogr., Sect. A 2008, 64, 112-122.
46. A. L. Spek, Acta Crystallogr., Sect. D 2009, 65, 148-155.
47. XP, Siemens Analytical X-ray Instruments Inc., Madison, Wisconsin, USA, 1994.