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Volumn 242, Issue , 2014, Pages 155-161

Thermostatted micro-reactor NMR probe head for monitoring fast reactions

Author keywords

Capillary flow NMR; Micro reaction technology; Online NMR spectroscopy; Reaction kinetics; Reaction monitoring; Thermostatted micro reactor

Indexed keywords

CAPILLARITY; CAPILLARY FLOW; KINETICS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION KINETICS;

EID: 84896526099     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2014.02.013     Document Type: Article
Times cited : (32)

References (42)
  • 1
    • 0029252722 scopus 로고
    • NMR spectroscopic and densimetric study of reaction kinetics of formaldehyde polymer formation in water, deuterium oxide, and methanol
    • I. Hahnenstein, M. Albert, H. Hasse, C.G. Kreiter, and G. Maurer NMR spectroscopic and densimetric study of reaction kinetics of formaldehyde polymer formation in water, deuterium oxide, and methanol Ind. Eng. Chem. Res. 34 1995 440 450
    • (1995) Ind. Eng. Chem. Res. , vol.34 , pp. 440-450
    • Hahnenstein, I.1    Albert, M.2    Hasse, H.3    Kreiter, C.G.4    Maurer, G.5
  • 2
    • 0037208108 scopus 로고    scopus 로고
    • Quantitative NMR spectroscopy of complex liquid mixtures: Methods and results for chemical equilibria in formaldehyde-water-methanol at temperatures up to 383 K
    • M. Maiwald, H.H. Fischer, M. Ott, R. Peschla, C. Kuhnert, C.G. Kreiter, G. Maurer, and H. Hasse Quantitative NMR spectroscopy of complex liquid mixtures: methods and results for chemical equilibria in formaldehyde-water- methanol at temperatures up to 383 K Ind. Eng. Chem. Res. 42 2003 259 266 (Pubitemid 36119849)
    • (2003) Industrial and Engineering Chemistry Research , vol.42 , Issue.2 , pp. 259-266
    • Maiwald, M.1    Fischer, H.H.2    Ott, M.3    Peschla, R.4    Kuhnert, C.5    Kreiter, C.G.6    Maurer, G.7    Hasse, H.8
  • 3
    • 33745179571 scopus 로고    scopus 로고
    • Quantitative NMR spectroscopy of complex technical mixtures using a virtual reference: Chemical equilibria and reaction kinetics of formaldehyde-water-1,3, 5-trioxane
    • DOI 10.1007/s00216-006-0477-3
    • M. Maiwald, T. Grützner, E. Ströfer, and H. Hasse Quantitative NMR spectroscopy of complex technical mixtures using a virtual reference: chemical equilibria and reaction kinetics of formaldehyde-water-1,3,5-trioxane Anal. Bioanal. Chem. 385 2006 910 917 (Pubitemid 43893074)
    • (2006) Analytical and Bioanalytical Chemistry , vol.385 , Issue.5 , pp. 910-917
    • Maiwald, M.1    Grutzner, T.2    Strofer, E.3    Hasse, H.4
  • 4
    • 37549007966 scopus 로고    scopus 로고
    • Online NMR spectroscopic study of species distribution in MEA-H2O-CO2 and DEA-H2O-CO2
    • W. Böttinger, M. Maiwald, and H. Hasse Online NMR spectroscopic study of species distribution in MEA-H2O-CO2 and DEA-H2O-CO2 Fluid Phase Equilib. 263 2008 131 143
    • (2008) Fluid Phase Equilib. , vol.263 , pp. 131-143
    • Böttinger, W.1    Maiwald, M.2    Hasse, H.3
  • 5
    • 0010647494 scopus 로고
    • Flow nuclear magnetic resonance investigation of the intermediates formed during the bromination of phenols in acetic acid
    • C.A. Fyfe, and L. Vanveen Flow nuclear magnetic resonance investigation of the intermediates formed during the bromination of phenols in acetic acid J. Am. Chem. Soc. 99 1977 3366 3371
    • (1977) J. Am. Chem. Soc. , vol.99 , pp. 3366-3371
    • Fyfe, C.A.1    Vanveen, L.2
  • 6
    • 0005607059 scopus 로고
    • Apparatus for the measurement of transient species and effects in flowing systems by high-resolution nuclear magnetic resonance spectroscopy
    • C.A. Fyfe, M. Cocivera, S.W.H. Damji, T.A. Hostetter, D. Sproat, and J. O'Brien Apparatus for the measurement of transient species and effects in flowing systems by high-resolution nuclear magnetic resonance spectroscopy J. Magn. Reson. 23 1976 377 384
    • (1976) J. Magn. Reson. , vol.23 , pp. 377-384
    • Fyfe, C.A.1    Cocivera, M.2    Damji, S.W.H.3    Hostetter, T.A.4    Sproat, D.5    O'Brien, J.6
  • 7
    • 34948910187 scopus 로고    scopus 로고
    • 2-methanol up to 35 MPa and 403 K
    • DOI 10.1016/j.supflu.2007.05.009, PII S0896844607002094
    • 1H NMR spectroscopic investigation of hydrogen bonding in supercritical and near critical CO2-methanol up to 35 MPa and 403 K J. Supercrit. Fluids 43 2007 267 275 (Pubitemid 47532378)
    • (2007) Journal of Supercritical Fluids , vol.43 , Issue.2 , pp. 267-275
    • Maiwald, M.1    Li, H.2    Schnabel, T.3    Braun, K.4    Hasse, H.5
  • 8
    • 54949121357 scopus 로고    scopus 로고
    • Online NMR spectroscopic study of species distribution in MDEA-H2O-CO2 and MDEA-PIP-H2O-CO2
    • W. Böttinger, M. Maiwald, and H. Hasse Online NMR spectroscopic study of species distribution in MDEA-H2O-CO2 and MDEA-PIP-H2O-CO2 Ind. Eng. Chem. Res. 47 2008 7917 7926
    • (2008) Ind. Eng. Chem. Res. , vol.47 , pp. 7917-7926
    • Böttinger, W.1    Maiwald, M.2    Hasse, H.3
  • 10
    • 84874604938 scopus 로고    scopus 로고
    • Proof of ether-bridged condensation products in UF resins by 2D NMR spectroscopy
    • E.J. Kibrik, O. Steinhof, G. Scherr, W.R. Thiel, and H. Hasse Proof of ether-bridged condensation products in UF resins by 2D NMR spectroscopy J. Polym. Res. 20 79 2013 1 10
    • (2013) J. Polym. Res. , vol.20 , Issue.79 , pp. 1-10
    • Kibrik, E.J.1    Steinhof, O.2    Scherr, G.3    Thiel, W.R.4    Hasse, H.5
  • 11
    • 0348230481 scopus 로고    scopus 로고
    • Quantitative high-resolution on-line NMR spectroscopy in reaction and process monitoring
    • M. Maiwald, H.H. Fischer, Y. Kim, K. Albert, and H. Hasse Quantitative high-resolution on-line NMR spectroscopy in reaction and process monitoring J. Magn. Reson. 166 2004 135 146
    • (2004) J. Magn. Reson. , vol.166 , pp. 135-146
    • Maiwald, M.1    Fischer, H.H.2    Kim, Y.3    Albert, K.4    Hasse, H.5
  • 13
    • 14844353999 scopus 로고    scopus 로고
    • Kinetics of oligomerization reactions in formaldehyde solutions: NMR experiments up to 373 K and thermodynamically consistent model
    • M. Ott, H.H. Fischer, M. Maiwald, K. Albert, and H. Hasse Kinetics of oligomerization reactions in formaldehyde solutions: NMR experiments up to 373 K and thermodynamically consistent model Chem. Eng. Process. 44 2005 653 660
    • (2005) Chem. Eng. Process. , vol.44 , pp. 653-660
    • Ott, M.1    Fischer, H.H.2    Maiwald, M.3    Albert, K.4    Hasse, H.5
  • 14
    • 34250741416 scopus 로고    scopus 로고
    • Optimising reaction performance in the pharmaceutical industry by monitoring with NMR
    • M.A. Bernstein, M. Stefinovic, and C.J. Sleigh Optimising reaction performance in the pharmaceutical industry by monitoring with NMR Magn. Reson. Chem. 45 2007 564 571
    • (2007) Magn. Reson. Chem. , vol.45 , pp. 564-571
    • Bernstein, M.A.1    Stefinovic, M.2    Sleigh, C.J.3
  • 15
    • 0033635714 scopus 로고    scopus 로고
    • Online NMR for monitoring biocatalysed reactions
    • H. Weber, and L. Brecker Online NMR for monitoring biocatalysed reactions Curr. Opin. Biotechnol. 11 2000 572 578
    • (2000) Curr. Opin. Biotechnol. , vol.11 , pp. 572-578
    • Weber, H.1    Brecker, L.2
  • 17
    • 34548399740 scopus 로고    scopus 로고
    • Flow techniques in NMR spectroscopy
    • P.A. Keifer Flow techniques in NMR spectroscopy Annu. Rep. NMR Spectrosc. 62 2007 1 47
    • (2007) Annu. Rep. NMR Spectrosc. , vol.62 , pp. 1-47
    • Keifer, P.A.1
  • 20
    • 0142232795 scopus 로고    scopus 로고
    • Quantitative on-line high-resolution NMR spectroscopy in process engineering applications
    • DOI 10.1007/s00216-002-1723-y
    • M. Maiwald, H.H. Fischer, Y.-K. Kim, and H. Hasse Quantitative on-line high-resolution NMR spectroscopy in process engineering applications Anal. Bioanal. Chem. 375 2003 1111 1115 (Pubitemid 40890321)
    • (2003) Analytical and Bioanalytical Chemistry , vol.375 , Issue.8 , pp. 1111-1115
    • Maiwald, M.1    Fischer, H.H.2    Kim, Y.-K.3    Hasse, H.4
  • 21
    • 84989640915 scopus 로고
    • On-line NMR in process engineering
    • W. Neudert, and E. Ströfer On-line NMR in process engineering Magn. Reson. Chem. 24 1986 1089 1092
    • (1986) Magn. Reson. Chem. , vol.24 , pp. 1089-1092
    • Neudert, W.1    Ströfer, E.2
  • 23
    • 0034146025 scopus 로고    scopus 로고
    • Small volume flow probe for automated direct-injection NMR analysis: Design and performance
    • R.L. Haner, W. Llanos, and L. Mueller Small volume flow probe for automated direct-injection NMR analysis: design and performance J. Magn. Reson. 143 2000 69 78
    • (2000) J. Magn. Reson. , vol.143 , pp. 69-78
    • Haner, R.L.1    Llanos, W.2    Mueller, L.3
  • 24
    • 0035582655 scopus 로고    scopus 로고
    • Solenoidal microcoil design. Part I: Optimizing RF homogeneity and coil dimensions
    • K.R. Minard, and R.A. Wind Solenoidal microcoil design. Part I: optimizing RF homogeneity and coil dimensions Concepts Magn. Reson. 13 2001 128 142
    • (2001) Concepts Magn. Reson. , vol.13 , pp. 128-142
    • Minard, K.R.1    Wind, R.A.2
  • 26
    • 84875229570 scopus 로고    scopus 로고
    • Radiofrequency microcoils for magnetic resonance imaging and spectroscopy
    • A.G. Webb Radiofrequency microcoils for magnetic resonance imaging and spectroscopy J. Magn. Reson. 229 2013 55 66
    • (2013) J. Magn. Reson. , vol.229 , pp. 55-66
    • Webb, A.G.1
  • 27
  • 28
    • 79959498253 scopus 로고    scopus 로고
    • Small-volume nuclear magnetic resonance spectroscopy
    • R.M. Fratila, and A.H. Velders Small-volume nuclear magnetic resonance spectroscopy Annu. Rev. Anal. Chem. 4 2011 227 249
    • (2011) Annu. Rev. Anal. Chem. , vol.4 , pp. 227-249
    • Fratila, R.M.1    Velders, A.H.2
  • 29
    • 84859723812 scopus 로고    scopus 로고
    • Considerations on the design of flow cells in by-pass systems for process analytical applications and its influence on the flow profile using NMR and CFD
    • F. Dalitz, M. Maiwald, and G. Guthausen Considerations on the design of flow cells in by-pass systems for process analytical applications and its influence on the flow profile using NMR and CFD Chem. Eng. Sci. 75 2012 318 326
    • (2012) Chem. Eng. Sci. , vol.75 , pp. 318-326
    • Dalitz, F.1    Maiwald, M.2    Guthausen, G.3
  • 32
    • 0037442581 scopus 로고    scopus 로고
    • Micromixer-based time-resolved NMR: Applications to ubiquitin protein conformation
    • DOI 10.1021/ac026076q
    • M. Kakuta, D.A. Jayawickrama, A.M. Wolters, A. Manz, and J.V. Sweedler Micromixer-based time-resolved NMR: applications to ubiquitin protein conformation Anal. Chem. 75 2003 956 960 (Pubitemid 36232454)
    • (2003) Analytical Chemistry , vol.75 , Issue.4 , pp. 956-960
    • Kakuta, M.1    Jayawickrama, D.A.2    Wolters, A.M.3    Manz, A.4    Sweedler, J.V.5
  • 37
    • 84856217217 scopus 로고    scopus 로고
    • From single to multiple microcoil flow probe NMR and related capillary techniques: A review
    • O. Gökay, and K. Albert From single to multiple microcoil flow probe NMR and related capillary techniques: a review Anal. Bioanal. Chem. 402 2012 647 669
    • (2012) Anal. Bioanal. Chem. , vol.402 , pp. 647-669
    • Gökay, O.1    Albert, K.2
  • 38
    • 31444443367 scopus 로고    scopus 로고
    • Real-time monitoring of chemical transformations by ultrafast 2D NMR spectroscopy
    • DOI 10.1021/ja0564158
    • M. Gal, M. Mishkovsky, and L. Frydman Real-time monitoring of chemical transformations by ultrafast 2D NMR spectroscopy J. Am. Chem. Soc. 128 2006 951 956 (Pubitemid 43153044)
    • (2006) Journal of the American Chemical Society , vol.128 , Issue.3 , pp. 951-956
    • Gal, M.1    Mishkovsky, M.2    Frydman, L.3
  • 39
    • 47549099789 scopus 로고    scopus 로고
    • Spectrally resolved flow imaging of fluids inside a microfluidic chip with ultrahigh time resolution
    • E. Harel, and A. Pines Spectrally resolved flow imaging of fluids inside a microfluidic chip with ultrahigh time resolution J. Magn. Reson. 193 2008 199 206
    • (2008) J. Magn. Reson. , vol.193 , pp. 199-206
    • Harel, E.1    Pines, A.2
  • 41
    • 0021532101 scopus 로고
    • Direct-linked analytical scale high-performance liquid chromatography/nuclear magnetic resonance spectrometry
    • D.A. Laude, and C.L. Wilkins Direct-linked analytical scale high-performance liquid chromatography/nuclear magnetic resonance spectrometry Anal. Chem. 56 1984 2471 2475
    • (1984) Anal. Chem. , vol.56 , pp. 2471-2475
    • Laude, D.A.1    Wilkins, C.L.2
  • 42
    • 0001217756 scopus 로고
    • A simple multi-nuclear NMR thermometer
    • C. Ammann, P. Meier, and A. Merbach A simple multi-nuclear NMR thermometer J. Magn. Reson. 46 1982 319 321
    • (1982) J. Magn. Reson. , vol.46 , pp. 319-321
    • Ammann, C.1    Meier, P.2    Merbach, A.3


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