Simultaneous quantitative analysis of the acetate, formate, chloride, phosphate and sulfate anions in biodiesel by ion chromatography

Fuel

Volumn 124, Issue , 2014, Pages 97-101

  Silveira, Eva Lúcia Cardoso ^a   De Caland, Lilia Basílio ^a   Tubino, Matthieu ^a  

^a UNIVERSITY OF CAMPINAS   (Brazil)

Author keywords

Anion; Biodiesel; Green method; Ion chromatography; Quantitative analysis

Indexed keywords

EID: 84894519517     PISSN: 00162361     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.fuel.2014.01.095     Document Type: Article

References (32)

1. G. Knothe, J. Krahl, J.V. Gerpen, and L.P. Ramos Manual de biodiesel 2006 Editora Edgar Blücher São Paulo
2. Agência Nacional do Petróleo (Brazil). Gás Natural e Biocombustíveis. Resolução 2012; 14(18 May).
3. R. Geris, N.A.C. Santos, B.A. Amaral, I.S. Maia, V.D. Castro, and J.R.M. Carvalho Biodiesel de soja-reação de transesterificaçã o para aulas práticas de química orgânica Quim Nova 30 2007 1369 1373
4. L.C. Martiniano, V.R. Abrantes, S.Y. Neto, E.P. Marques, T.C.O. Fonseca, and L.L. Paim et al. Direct simultaneous determination of Pb(II) and Cu(II) in biodiesel by anodic stripping voltammetry at a mercury-film electrode using microemulsions Fuel 103 2013 1164 1167
5. I.P. Lôbo, S.L.C. Ferreira, and R.S. Cruz Parâmetros de qualidade e métodos analíticos Quim Nova 32 2009 1596 1608
6. J. Van Gerpen Biodiesel processing and production Fuel Process Technol 86 2005 1097 1107
7. M. Bowman, D. Hilligoss, S. Rasmussen, and R. Thomas Biodiesel: a renewable and biodegradable fuel Hydrocarbon Process 85 2006 103 106
8. ABNT NBR 15553/2008. Produtos derivados de gorduras e óleos - ésteres metílicos/etílicos de ácidos graxos - Determinação dos teores de cálcio, magnésio, sódio, fósforo e potássio por espectrometria de emissão óptica com plasma indutivamente acoplado (ICP OES).
9. ASTM D4951/2009. Standard test method for determination of additive elements in lubricating oils by inductively coupled plasma atomic emission spectrometry.
10. P.E. Jackson Determination of inorganic ions in drinking water by ion chromatography Trends Anal Chem 20 2001 320 329
11. C. Lopez-Moreno, I. Viera, and A.M. Urbano Validation of an ion chromatographic method for the quantification of anions in water Desalination 261 2010 111 116
12. R. Michalski Ion chromatography as a reference method for determination of inorganic ions in water and wastewater Crit Rev Anal Chem 36 2006 107 127
13. Y. Park, Y. Kim, D.W. Lee, S. Lee, and K. Lee Ion chromatographic determination method for the determination of inorganic anions in environmental samples of Korea Anal Sci 18 2002 343 346
14. J.S.F. Pereira, L.O. Diehl, F.A. Duarte, M.F.P. Santos, R.C.L. Guimarães, and V.L. Dressler et al. Chloride determination by ion chromatography in petroleum coke after digestion by microwave-induced combustion J Chromatogr A 1213 2008 249 252
15. P.L. Buldini, D. Ferri, and J.L. Sharma Determination of some inorganic species in edible vegetable oils and fats by ion chromatography J Chromatogr A 89 1997 549 555
16. P.L. Buldini, S. Cavalli, A. Mevoli, and J.L. Sharma Ion Chromatography and voltammetric determination of heavy and transition metals in honey Food Chem 73 2001 487 495
17. G. Dugo, T.M. Pellicano, L. Pera, V.L. Turco, A. Tamborrino, and M.L. Clodoveo Determination of inorganic anions in commercial seed oils and in virgin olive oils produced from de-stoned olives and traditional extraction methods, using suppressed ion exchange chromatography (IEC) Food Chem 102 2007 599 605
18. S.D. Kumar, G. Narayan, and S. Hassarajani Determination of anionic minerals in black and kombucha tea using ion chromatography Food Chem 111 2008 784 788
19. ABNT/NBR 10894/2007. Álcool etílico - Determinaç ão dos íons cloreto e sulfato - Método da Cromatografia de íons.
20. L.B. Caland, E.L.C. Silveira, and M. Tubino Determination of sodium, potassium, calcium and magnesium cátions in biodiesel by ion chromatography Anal Chim Acta 718 2012 116 120
21. Emmenegger C, Wille A, Steinbach A. Sulfur and halide determination by combustion ion chromatography. The application notebook (Metrohm). 2010. p. 40-43.
22. Hurum D, De Borba B, Rohrer J. Determination of cations in biodiesel using a reagent-free ion chromatography system with suppressed conductivity detection. Application Note 203. Thermo Scientific Dionex.
23. M. Piovezan, A.C.O. Costa, A.V. Jager, M.A.L. Oliveira, and G.A. Micke Development of a fast capillary electrophoresis method to determine inorganic cations in biodiesel samples Anal Chim Acta 673 2010 200 205
24. T. Nogueira, and C.L. Lago Determination of Ca, K, Mg, Na, sulfate, phosphate, formate, acetate, propionate, and glycerol in biodiesel by capillary electrophoresis with capacitively coupled contactless conductivity detection Microchem J 99 2011 267 272
25. J.H.F. Boog, E.L.C. Silveira, L.B. Caland, and M. Tubino Determining the residual alcohol in biodiesel through its flash point Fuel 90 2011 905 907
26. M. Ribani, C.B.G. Bottoli, C.H. Collins, I.C.S.F. Jardim, and L.F.C. Melo Validação em métodos cromatográficos e eletroforéticos Quim Nova 27 2004 771 780
27. Instituto Nacional de Metrologia, Normalização e Qualidade Industrial (INMETRO). Orientação sobre Validação de Métodos Analíticos. DOQ-CGCRE-008. 2010.
28. A.G. Gonzáles, M.A. Herrador, and A.G. Asuero Intra-laboratory by testing of method accuracy from recovery assays Talanta 48 1999 729 736
29. D.A. Skoog, D.M. West, F.J. Holler, and S.R. Crouch Fundamentos de química analítica 8th ed. 2006 Pioneira Thomson Learning São Paulo
30. L.F.B. Lira, D.C.M.B. Santos, M.A.B. Guida, L. Stragevitch, M.G.A. Korn, and M.F. Pimentel et al. Determination of phosphorus in biodiesel using FIA with spectrophotometric detection Fuel 90 2011 3254 3258
31. E.L.C. Silveira, L.B. Caland, and M. Tubino Molecular absorption spectrophotometric method for the determination of phosphorus in biodiesel Fuel 90 2011 3485 3488
32. H.B.P. Ferreira, T.A.F. Lima, and P.J.S. Barbeira Voltammetric determination of chloride ion in automotive fuel ethanol Electroanalysis 20 2008 390 395