Solid-state NMR concepts for the investigation of supported transition metal catalysts and nanoparticles

Solid State Nuclear Magnetic Resonance

Volumn 55-56, Issue , 2013, Pages 1-11

  Gutmann, Torsten ^a   Grünberg, Anna ^a   Rothermel, Niels ^a   Werner, Mayke ^a   Srour, Mohamad ^a   Abdulhussain, Safaa ^a   Tan, Shulin ^a   Xu, Yeping ^a   Breitzke, Hergen ^a   Buntkowsky, Gerd ^a  

^a DARMSTADT UNIVERSITY OF TECHNOLOGY   (Germany)

Author keywords

2H solid state NMR; Heterogeneous catalysis; Immobilized catalyst; Solid state NMR; Transition metal nanoparticles

Indexed keywords

CHARACTERIZATION TOOLS; HOMOGENEOUS TRANSITION; IMMOBILIZED CATALYSTS; ORGANIC TRANSFORMATIONS; SOLID STATE NMR; SOLID-STATE NMR SPECTROSCOPY; TRANSITION METAL CATALYSTS; TRANSITION METAL SURFACES;

CATALYSIS; CATALYSTS; CHARACTERIZATION; CHEMICAL ENGINEERING; HYBRID MATERIALS; METAL NANOPARTICLES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLID STATE PHYSICS; SURFACES;

TRANSITION METALS;

EID: 84887991195     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ssnmr.2013.06.004     Document Type: Review

References (146)

1. G. Ertl Angew. Chem. 102 1990 1258
2. R. Schlögl Angew. Chem. Int. Ed. 42 2003 2004
3. B.H. Davis, and M.L. Occelli Fischer-Tropsch Synthesis, Catalysts and Catalysis 2007 Elsevier Amsterdam
4. S. Shetty, and R.A. van Santen Catal. Today 171 2011 168
5. C.X. Xiao, Z.P. Cai, T. Wang, Y. Kou, and N. Yan Angew. Chem. Int. Ed. 47 2008 746
6. A. Gual, M.R. Axet, K. Philippot, B. Chaudret, A. Denicourt-Nowicki, A. Roucoux, S. Castillon, and C. Claver Chem. Commun. 2008 2759
7. A. Roucoux, C. Copéret, and B. Chaudret Stabilized Noble Metal Nanoparticles: An Unavoidable Family of Catalysts for Arene Derivative Hydrogenation Surface and Interfacial Organometallic Chemistry and Catalysis 2005 Springer Berlin/Heidelberg
8. X. Zhou, T. Wu, B. Hu, T. Jiang, and B. Han J. Mol. Catal. A 306 2009 143
9. X.S. Zhao, X.Y. Bao, W. Guo, and F.Y. Lee Mater. Today 9 2006 32
10. S. Hermes, M.K. Schröter, R. Schmid, L. Khodeir, M. Muhler, A. Tissler, R.W. Fischer, and R.A. Fischer Angew. Chem. Int. Ed. 44 2005 6237
11. J. Evans, A.B. Zaki, M.Y. El-Sheikh, and S.A. El-Safty J. Phys. Chem. B 104 2000 10271
12. A.J. Sandee, J.N.H. Reek, P.C.J. Kamer, and P.W.N.M. van Leeuwen J. Am. Chem. Soc. 123 2001 8468
13. J.K. Lee, T.J. Yoon, and Y.K. Chung Chem. Commun. 2001 1164
14. W.H. Cheung, W.Y. Yu, W.P. Yip, N.Y. Zhu, and C.M. Che J. Org. Chem. 67 2002 7716
15. R. Becker, H. Parala, F. Hipler, O.P. Tkachenko, K.V. Klementiev, W. Grünert, H. Wilmer, O. Hinrichsen, A. Birkner, M. Muhler, C. Wöll, S. Schäfer, and R.A. Fischer Angew. Chem. Int. Ed. 43 2004 2839
16. J.O. Krause, O. Nuyken, K. Wurst, and M.R. Buchmeiser Chem. Eur. J. 10 2004 777
17. A. Crosman, and W.E. Hoelderich J. Catal. 232 2005 43
18. A.M.J. Rost, H. Schneider, J.P. Zoller, W.A. Herrmann, and F.E. Kühn J. Organomet. Chem. 690 2005 4712
19. M. Hartmann, and C. Streb J. Porous Mater. 13 2006 347
20. T. Posset, and J. Bluemel J. Am. Chem. Soc. 128 2006 8394
21. J.W. Wiench, C. Michon, A. Ellern, P. Hazendonk, A. Iuga, R. Angelici, and M. Pruski J. Am. Chem. Soc. 131 2009 11801
22. J.R. Rapp, Y. Huang, M. Natella, Y. Cai, V.S.Y. Lin, and M. Pruski Solid State NMR 35 2009 82
23. K. Mao, J.W. Wiench, V.S.Y. Lin, and M. Pruski J. Magn. Reson. 196 2009 92 ("This paper demonstrates the possible sensitivity gain in surface NMR by indirectly detected through-bond chemical shift correlation NMR spectroscopy in solids under fast MAS")
24. T. Joseph, S.S. Deshpande, S.B. Halligudi, A. Vinu, S. Ernst, and M. Hartmann J. Mol. Catal. A 206 2003 13
25. B. Chaudret C. R. Phys. 6 2005 117
26. P. Lara, K. Philippot, and B. Chaudret ChemCatChem 5 2013 28
27. B. Chaudret Synthesis and surface reactivity of organometallic nanoparticles Topics in Organometallic Chemistry 2005 Springer-Verlag Berlin, Heidelberg 233 259
28. K. Philippot, and B. Chaudret C. R. Chim. 6 2003 1019
29. F. Hoffmann, M. Cornelius, J. Morell, and M. Froba Angew. Chem. Int. Ed. 45 2006 3216
30. D.Y. Zhao, Q.S. Huo, J.L. Feng, B.F. Chmelka, and G.D. Stucky J. Am. Chem. Soc. 120 1998 6024
31. J. Lu, and P.H. Toy Chem. Rev. 109 2009 815
32. B.M.L. Dioos, I.F.J. Vankelecom, and P.A. Jacobs Adv. Synth. Catal. 348 2006 1413
33. J. Bluemel Coord. Chem. Rev. 252 2008 2410 ("This review gives an excellent overview about the immobilization and classical as well as modern SSNMR methods of oxide bound metal catalysts")
34. J.S. Beck, J.C. Vartuli, W.J. Roth, M.E. Leonowicz, C.T. Kresge, K.D. Schmitt, C.T.W. Chu, D.H. Olson, E.W. Sheppard, S.B. McCullen, J.B. Higgins, and J.L. Schlenker J. Am. Chem. Soc. 114 1992 10834
35. D. Zhao, J. Feng, Q. Huo, N. Melosh, G.H. Fredrickson, B.F. Chmelka, and G.D. Stucky Science 279 1998 548
36. G. Buntkowsky, H. Breitzke, A. Adamczyk, F. Roelofs, T. Emmler, E. Gedat, B. Grünberg, Y. Xu, H.H. Limbach, I. Shenderovich, A. Vyalikh, and G.H. Findenegg Phys. Chem. Chem. Phys. 9 2007 4843
37. H.X. Li, F. Zhang, H. Yin, Y. Wan, and Y.F. Lu Green Chem. 9 2007 500
38. L. Huang, and S. Kawi Catal. Lett. 90 2003 165
39. L. Huang, C.J. Wu, and S. Kawi React. Kinet. Catal. Lett. 82 2004 65
40. L. Huang, and S. Kawi Catal. Lett. 92 2004 57
41. V. Dufaud, F. Beauchesne, and L. Bonneviot Angew. Chem. Int. Ed. 44 2005 3475
42. E. Dulière, M. Devillers, and J. Marchand-Brynaert Organometallics 22 2003 804
43. C. Copéret, M. Chabanas, R.P. Saint-Arroman, and J.M. Basset Angew. Chem. Int. Ed. 42 2003 156 181
44. F. Lefebvre, and J.M. Basset J. Mol. Catal. A 146 1999 3
45. F. Lefebvre, P. Putaj, J.M. Basset, X.X. Wang, and X.Z. Fu Sci. China-Chem. 53 2010 1862
46. C. Copéret, and J.M. Basset Adv. Synth. Catal. 349 2007 78
47. S. Jansat, D. Picurelli, K. Pelzer, K. Philippot, M. Gomez, G. Muller, P. Lecante, and B. Chaudret New J. Chem. 30 2006 115
48. D. González-Gálvez, P. Lara, O. Rivada-Wheelaghan, S. Conejero, B. Chaudret, K. Philippot, and P.W.N.M. van Leeuwen Catal. Sci. Technol. 3 2013 99
49. D. Astruc Nanoparticles and Catalysis 2008 Wiley-VCH Weinheim
50. J. Bluemel Nachr. Chem. 54 2006 632
51. A. Gruenberg, H. Breitzke, and G. Buntkowsky Spectrosc. Prop. Inorg. Organomet. Compd. 43 2012 289 ("This review gives a very detailed overview about solid-state NMR of immobilized catalysts and nanocatalysts.")
52. C. Merckle, and J. Bluemel Top. Catal. 34 2005 5
53. J. Trebosc, J.W. Wiench, S. Huh, V.S.Y. Lin, and M. Pruski J. Am. Chem. Soc. 127 2005 3057
54. J. Trebosc, J.W. Wiench, S. Huh, V.S.Y. Lin, and M. Pruski J. Am. Chem. Soc. 127 2005 7587
55. A. Gruenberg, Y.P. Xu, H. Breitzke, and G. Buntkowsky Chem. Eur. J. 16 2010 6993 ("This paper demonstrates that the combination of multinuclear MAS-SSNMR is able to reveal the detailed binding of a homogeneous catalysts to an oxide species.")
56. A. Gruenberg, T. Gutmann, N. Rothermel, Y. Xu, H. Breitzke, and G. Buntkowsky Z. Phys. Chem. 227 2013 901 915
57. A. Adamczyk, Y. Xu, B. Walaszek, F. Roelofs, T. Pery, K. Pelzer, K. Philippot, B. Chaudret, H.-H. Limbach, H. Breitzke, and G. Buntkowsky Top. Catal. 48 2008 75
58. M.J. Bennett, and P.B. Donaldson Inorg. Chem. 16 1977 655
59. S.J. La Placa, and J.A. Ibers Inorg. Chem. 4 1965 778
60. J.A. Osborn, F.H. Jardine, J.F. Young, and G.J. Wilkinson J. Chem. Soc. A 1966 1711
61. J. Kramer, E. Nöllen, W. Buijs, W.L. Driessen, and J. Reedijk React. Funct. Polym. 57 2003 1
62. C. Merckle, S. Haubrich, and J. Bluemel J. Organomet. Chem. 627 2001 44
63. D. Duraczynska, E.M. Serwicka, A. Waksmundzka-Gora, A. Drelinkiewicz, and Z. Olejniczak J. Org. Chem. 693 2008 510
64. M.E. Quiroga, E.A. Cagnola, D.A. Liprandi, and P.C. Ĺ Argentière J. Mol. Catal. A 149 1999 147
65. S. Komiya Synthesis of Organometallic Compounds 1997 John Wiley & Sons, Inc. Chichester, New York, Weinheim, Brisbane, Singapore, Toronto
66. K.S. MacFarlane, A.M. Joshi, S.J. Rettig, and B.R. James Inorg. Chem. 35 1996 7304
67. P. Hoffman, and K. Caulton J. Am. Chem. Soc. 97 1975 4221
68. L. Bemi, H.C. Clark, J.A. Davies, C.A. Fyfe, and R.E. Wasylishen J. Am. Chem. Soc. 104 1982 438 ("This paper presents their pioneering 31 P NMR investigations of metal containing phoshine complexes.")
69. L. Bemi, H.C. Clark, J.A. Davies, D. Drexler, C.A. Fyfe, and R. Wasylishen J. Organomet. Chem. 224 1982 C5 ("This paper presents their pioneering 31P NMR investigations of metal containing phoshine complexes.")
70. B. Beele, J. Guenther, M. Perera, M. Stach, T. Oeser, and J. Bluemel New J. Chem. 34 2010 2729 ("This paper presents an alternative linker type for the immobilization of Wilkinson's catalyst.")
71. R. Fetouaki, A. Seifert, M. Bogza, T. Oeser, and J. Bluemel Inorg. Chim. Acta 359 2006 4865
72. G. Wu, and R.E. Wasylishen Organometallics 11 1992 3242 ("This paper discusses the utility of 2D COSY and homonuclear J-resolved 31P CP-MAS NMR for the investigation of metal containing phosphine complexes.")
73. R.H. Crabtree The Organometallic Chemistry of Transition Metals 2009 John Wiley & Sons, Inc. Hoboken, New Jersey
74. J.W. Diesveld, E.M. Menger, H.T. Edzes, and W.S. Veeman J. Am. Chem. Soc. 102 1980 7935
75. G. Wu, and R.E. Wasylishen Inorg. Chem. 31 1992 145 ("This paper discusses the application of homonuclear 31P J-resolved 2D SSNMR for the investigation of rhodium(I) phosphine complexes.")
76. G. Wu, and R.E. Wasylishen J. Chem. Phys. 98 1993 6138 ("This paper gives a general description of magic-angle spinning (MAS) nuclear magnetic resonance spectra arising from a pair of chemically equivalent nuclear spins and discusses techniques to resolve them in case of magnetic inequivalence.")
77. G.A. Somorjai, H. Frei, and J.Y. Park J. Am. Chem. Soc. 131 2009 16589
78. T.M. Duncan, K.W. Zilm, D.M. Hamilton, and T.W. Root J. Phys. Chem. 93 1989 2583
79. M.J. Hostetler, J.E. Wingate, C.-J. Zhong, J.E. Harris, R.W. Vachet, M.R. Clark, D.J. Londono, S.J. Green, J.J. Stokes, G.D. Wignall, G.L. Glish, M.D. Porter, N.D. Evans, and R.W. Murray Langmuir 14 1998 17
80. P.K. Babu, J.H. Chung, S.T. Kuk, T. Kobayashi, E. Oldfield, and A. Wieckowski J. Phys. Chem. B 109 2005 2474
81. P.K. Babu, H.S. Kim, J.H. Chung, E. Oldfield, and A. Wieckowski J. Phys. Chem. B 108 2004 20228
82. K. Tedsree, A.T.S. Kong, and S.C. Tsang Angew. Chem. Int. Ed. 48 2009 1443
83. A. Badia, L. Demers, L. Dickinson, F.G. Morin, R.B. Lennox, and L. Reven J. Am. Chem. Soc. 119 1997 11104
84. A. Badia, W. Gao, S. Singh, L. Demers, L. Cuccia, and L. Reven Langmuir 12 1996 1262
85. R. Bronger, T.D. Le, S. Bastin, J. GarcIa-Anton, C. Citadelle, B. Chaudret, P. Lecante, A. Igau, and K. Philippot New J. Chem. 35 2011 2653
86. D. González-Gálvez, P. Nolis, K. Philippot, B. Chaudret, and P.W.N.M. van Leeuwen ACS Catal. 2 2012 317
87. E. Rafter, T. Gutmann, F. Löw, G. Buntkowsky, K. Philippot, B. Chaudret, and P.W.N.M. van Leeuwen Catal. Sci. Technol. 3 2013 595 ("In this paper the synthesis and SS-NMR characterization of the first secondary phosphine oxide stabilized ruthenium nanoparticles is presented in the context of structure and catalytic activity relationship.")
88. P. Lara, T. Ayvali, M.-J. Casanove, P. Lecante, A. Mayoral, P.-F. Fazzini, K. Philippot, and B. Chaudret Dalton Trans. 42 2013 372
89. P. Lara, M.-J. Casanove, P. Lecante, P.-F. Fazzini, K. Philippot, and B. Chaudret J. Mater. Chem. 22 2012 3578
90. P. Lara, O. Rivada-Wheelaghan, S. Conejero, R. Poteau, K. Philippot, and B. Chaudret Angew. Chem. Int. Ed. 50 2011 12080 ("This paper shows the pioneering work on synthesis and solid-state NMR surface studies of N-Heterocyclic Carbene stabilized nanoparticles")
91. P.-J. Debouttière, Y. Coppel, A. Denicourt-Nowicki, A. Roucoux, B. Chaudret, and K. Philippot Eur. J. Inorg. Chem. 8 2012 1229
92. F. Novio, K. Philippot, and B. Chaudret Catal. Lett. 140 2010 1
93. T. Gutmann, I. del Rosal, B. Chaudret, R. Poteau, H.-H. Limbach, and G. Buntkowsky ChemPhysChem 2013 10.1002/cphc.201300200 ("This paper gives a detailed overview about the application of 2H solid-state NMR for the study of ruthenium containing hydrogenation catalysts").)
94. B. Walaszek, A. Adamczyk, T. Pery, Y.P. Xu, T. Gutmann, N.D. Amadeu, S. Ulrich, H. Breitzke, H.M. Vieth, S. Sabo-Etienne, B. Chaudret, H.H. Limbach, and G. Buntkowsky J. Am. Chem. Soc. 130 2008 17502 ("This paper presents a detailed 2H-NMR study of a series of mononuclear transition metal polyhydrides.")
95. T. Gutmann, B. Walaszek, Y. Xu, M. Waechtler, I.d. Rosal, A. Grünberg, R. Poteau, R. Axet, G. Lavigne, B. Chaudret, H.-H. Limbach, and G. Buntkowsky J. Am. Chem. Soc. 132 2010 11759 ("This paper presents a detailed 2H-NMR and DFT study of a series of deuterated ruthenium compounds and clusters.")
96. I. del Rosal, T. Gutmann, L. Maron, F. Jolibois, B. Chaudret, B. Walaszek, H.H. Limbach, R. Poteau, and G. Buntkowsky Phys. Chem. Chem. Phys. 11 2009 5657 ("This paper describes how the combination of 2H solid-state NMR and DFT calculations can be used to get information about the local environment of hydrogen atoms, and more particularly the coordination mode of hydrides in such complexes.")
97. I. del Rosal, T. Gutmann, B. Walaszek, I. Gerber, B. Chaudret, H.-H. Limbach, G. Buntkowsky, and R. Poteau Phys. Chem. Chem. Phys. 13 2011 20199 ("This paper presents 2H NMR calculations on solid polynuclear transition metal complexes.")
98. I. del Rosal, L. Maron, R. Poteau, and F. Jolibois Dalton Trans. 2008 3959 3970
99. T. Pery, K. Pelzer, G. Buntkowsky, K. Philippot, H.H. Limbach, and B. Chaudret ChemPhysChem. 6 2005 605 ("This paper presents 2H-SSNMR results about the mobility of deuterium on ruthenium nanoparticles.")
100. L.A. Truflandier, I. Del Rosal, B. Chaudret, R. Poteau, and I.C. Gerber ChemPhysChem. 10 2009 2939
101. I. del Rosal, L. Truflandier, R. Poteau, and I.C. Gerber J. Phys. Chem. C 115 2011 2169
102. F. Schröder, D. Esken, M. Cokoja, M.W.E v.d. Berg, O. Lebedev, G.V. Tendeloo, B. Walaszek, G. Buntkowsky, H.-H. Limbach, B. Chaudret, and R.A. Fischer J. Am. Chem. Soc. 130 2008 6119 ("This paper presents the characterization of ruthenium nanoparticles embebbed in a metal organic framework (MOF) including 2H-NMR investigations.")
103. B. Walaszek, Y. Xu, A. Adamczyk, H. Breitzke, K. Pelzer, H.-H. Limbach, J. Huang, H. Li, and G. Buntkowsky Solid State NMR 35 2009 164 ("This paper presents 2H-SSNMR results on the deuterium adsorption on a heterogeneous ruthenium catalyst.")
104. J. Garcia-Anton, M.R. Axet, S. Jansat, K. Philippot, B. Chaudret, T. Pery, G. Buntkowsky, and H.H. Limbach Angew. Chem. Int. Ed. 47 2008 2074 ("This paper describes reactions of olefins with novel ruthenium hydride nanoparticles. It is shown that 2H-SSNMR is able to reveal transient reaction intermediates on the surface.")
105. A.W. Overhauser Phys. Rev. 92 1953 411
106. T.P. Carver, and C.P. Slichter Phys. Rev. 92 1953 212
107. T.P. Carver, and C.P. Slichter Phys. Rev. 102 1956 975
108. K.L. Felch, B.G. Danly, H.R. Jory, K.E. Kreischer, W. Lawson, B. Levush, and R.J. Temkin Proc. IEEE 87 1999 752
109. C. Song, K.N. Hu, C.G. Joo, T.M. Swager, and R.G. Griffin J. Am. Chem. Soc. 128 2006 11385
110. T. Maly, G.T. Debelouchina, V.S. Bajaj, K. Hu, C. Joo, M.L. Mak-Jurkauskas, J.R. Sirigiri, P.C.A v.d. Wel, J. Herzfeld, R.J. Temkin, and R.G. Griffin J. Chem. Phys. 128 2008 052211 ("This paper reviews the classical DNP mechanisms and recent developments of DNP at high magnetic fields which have an enormous potential for sensitivity enhancement in solid-state NMR.")
111. L.R. Becerra, G.J. Gerfen, R.J. Temkin, D.J. Singel, and R.G. Griffin Phys. Rev. Lett. 71 1993 3561
112. A. Lesage, M. Lelli, D. Gajan, M.A. Caporini, V. Vitzthum, P. Mieville, J. Alauzun, A. Roussey, C. Thieuleux, A. Mehdi, G. Bodenhausen, C. Coperet, and L. Emsley J. Am. Chem. Soc. 132 2010 15459 ("This paper shows that surface NMR spectra can be greatly enhanced using dynamic nuclear polarization. Polarization is transferred from the protons of the solvent to the rare nuclei (here 13C at natural isotopic abundance) at the surface, yielding at least a 50-fold signal enhancement for surface species covalently incorporated into a silica framework.")
113. M. Lelli, D. Gajan, A. Lesage, M.A. Caporini, V. Vitzthum, P. Mieville, F. Heroguel, F. Rascon, A. Roussey, C. Thieuleux, M. Boualleg, L. Veyre, G. Bodenhausen, C. Coperet, and L. Emsley J. Am. Chem. Soc. 133 2011 2104 2107
114. C.R. Bowers, and D.P. Weitekamp Phys. Rev. Lett. 57 1986 2645
115. T.C. Eisenschmidt, R.U. Kirss, P.P. Deutsch, S.I. Hommeltoft, R. Eisenberg, and J. Bargon J. Am. Chem. Soc. 109 1987 8089
116. M.G. Pravica, and D.P. Weitekamp Chem. Phys. Lett. 145 1988 255
117. P. Carson, C. Bowers, and D. Weitekamp J. Am. Chem. Soc. 123 2001 11821
118. A.Y. Rozovskii, and G.I. Lin Kinet. Catal. 40 1999 773
119. J. Martins, C. Taft, S. Lie, and E. Longo J. Mol. Struct. - Theochem 528 2000 161
120. H. Henning, M. Dyballa, M. Scheibe, E. Klemm, and M. Hunger Chem. Phys. Lett. 555 2013 258 ("This paper describes in-situ MAS NMR PHIP spectroscopy.")
121. S.S. Arzumanov, and A.G. Stepanov J. Phys. Chem. C 117 2013 2888
122. M. Hunger Catal. Today 97 2004 3 ("This paper describes in-situ MAS NMR spectroscopy for the investigation of heterogeneous catalysis.")
123. T. Ratajczyk, T. Gutmann, S. Dillenberger, S. Abdulhussaein, J. Frydel, H. Breitzke, U. Bommerich, T. Trantzschel, J. Bernarding, and P. Magusin Solid State Nucl. Magn. Reson. 43-44 2012 14
124. J. Brossel, and A. Kastler Hebd. Seances Acad. Sci. 229 1949 1213
125. W. Happer, E. Miron, S. Schaefer, W.A. Schreiber, W.A. van Wijngaarden, and X. Zeng Phys. Rev. A 29 1984 3092
126. C.R. Bowers, T. Pietrass, E. Barash, A. Pines, and R.K. Grubbs J. Phys. Chem. 98 1994 9400
127. C.J. Jameson, A.K. Jameson, and S.M. Cohen J. Chem. Phys. 59 1973 4540
128. T. Pietrass, A. Bifone, and A. Pines Surf. Sci. 334 1995 L730
129. R.J. Fitzgerald, K.L. Sauer, and W. Happer Chem. Phys. Lett. 284 1998 87
130. G. Navon, Y.Q. Song, T. Room, S.T.R.E. Appelt, and A. Pines Science 271 1996 1848
131. L.J. Smith, J. Smith, E. MacNamara, K. Knagge, and D. Raftery J. Phys. Chem. B 105 2001 1412
132. E. MacNamara, C.V. Rice, J. Smith, L.J. Smith, and D. Raftery Chem. Phys. Lett. 317 2000 165
133. E. MacNamara, G. Fischer, J. Smith, C.V. Rice, S.J. Hwang, and D. Raftery J. Phys. Chem. B 103 1999 1158
134. J. Smith, K. Knagge, E. MacNamara, and D. Raftery J. Magn. Reson. 159 2002 111
135. B.C. Gerstein, R.G. Pembleton, R.C. Wilson, and L.M. Ryan J. Chem. Phys. 66 1977 361
136. L.S. Du, A. Samoson, T. Tuherm, and C.P. Grey Chem. Mater. 12 2000 3611
137. A. Samoson D.M. Grant, R.K. Harris, Extended Magic-Angle Spinning 2002 John Wiley & Sons Chichester 59 64
138. M. Ernst, A. Detken, A. Böckmann, and B.H. Meier J. Am. Chem. Soc. 125 2003 15807
139. M. Ernst, M.A. Meier, T. Tuherm, A. Samoson, and B.H. Meier J. Am. Chem. Soc. 126 2004 4764
140. Y. Ishii, and R. Tycko J. Magn. Reson. 142 2000 199 ("This paper started the application of indirect detection schemes for fast MAS SSNMR spectroscopy.")
141. T.M. Hsin, S. Chen, E. Guo, C.H. Tsai, M. Pruski, and V.S.Y. Lin Top. Catal. 53 2010 746
142. S. Nedd, T. Kobayashi, C.H. Tsai, I.I. Slowing, M. Pruski, and M.S. Gordon J. Phys. Chem. C 115 2011 16333
143. T. Kobayashi, K. Mao, S.G. Wang, V.S.Y. Lin, and M. Pruski Solid State Nucl. Magn. Reson. 39 2011 65
144. K. Mao, T. Kobayashi, J.W. Wiench, H.T. Chen, C.H. Tsai, V.S.Y. Lin, and M. Pruski J. Am. Chem. Soc. 132 2010 12452
145. J.W. Wiench, Y.S. Avadhut, N. Maity, S. Bhaduri, G.K. Lahiri, M. Pruski, and S. Ganapathy J. Phys. Chem. B 111 2007 3877 ("This paper shows that indirectly detected natural abundance 1H-13C-HETCOR spectra of functionalized silica materials allow a 15 times faster experiment than conventional detection.")
146. K. Mao, and M. Pruski J. Magn. Reson. 201 2009 165 ("This paper presents directly and indirectly detected through-bond heteronuclear correlation solid-state NMR spectroscopy under fast MAS".)