Factorial design optimization of experimental variables in preconcentration of carbamates pesticides in water samples using solid phase extraction and liquid chromatography-electrospray-mass spectrometry determination

Talanta

Volumn 117, Issue , 2013, Pages 392-398

  Latrous El Atrache, Latifa ^a,b   Ben Sghaier, Rafika ^a   Bejaoui Kefi, Bochra ^c   Haldys, Violette ^d,e   Dachraoui, Mohamed ^a   Tortajada, Jeanine ^d,e  

^a FACULTÉ DES SCIENCES DE TUNIS   (Tunisia)

^b UNIVERSITÉ DE TUNIS EL MANAR   (Tunisia)

^c Institut National de Recherche et d'Analyse Physico Chimique Tunis   (Tunisia)

^d UNIVERSITÉ D EVRY VAL D ESSONNE   (France)

^e Centre National de la Recherche Scientifique   (France)

Author keywords

Carbamates pesticides; Experimental design; Method validation; Solid phase extraction; Water

Indexed keywords

DESIGN OF EXPERIMENTS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; ORGANIC COMPOUNDS; PESTICIDES; PHASE SEPARATION; STATISTICS; SURFACE WATERS; WATER;

DETECTION AND QUANTIFICATION LIMIT; ELECTROSPRAY MASS SPECTROMETRY; FACTORIAL DESIGN OPTIMIZATION; FULL FACTORIAL DESIGN; LIQUID CHROMATOGRAPHY ELECTROSPRAY; METHOD VALIDATIONS; RELATIVE STANDARD DEVIATIONS (R.S.D.); SOLID-PHASE EXTRACTION;

EXTRACTION;

ACETONITRILE; ACETONITRILE DERIVATIVE; CARBAMIC ACID DERIVATIVE; FRESH WATER; PESTICIDE; WATER;

ARTICLE; CARBAMATES PESTICIDES; CHEMISTRY; ELECTROSPRAY MASS SPECTROMETRY; EXPERIMENTAL DESIGN; FACTORIAL ANALYSIS; ISOLATION AND PURIFICATION; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY; METHOD VALIDATION; METHODOLOGY; SOLID PHASE EXTRACTION; WATER POLLUTANT;

CARBAMATES PESTICIDES; EXPERIMENTAL DESIGN; METHOD VALIDATION; SOLID PHASE EXTRACTION; WATER;

ACETONITRILES; CARBAMATES; CHROMATOGRAPHY, LIQUID; FACTOR ANALYSIS, STATISTICAL; FRESH WATER; LIMIT OF DETECTION; PESTICIDES; RESEARCH DESIGN; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; WATER POLLUTANTS, CHEMICAL;

EID: 84885636714     PISSN: 00399140     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.talanta.2013.09.032     Document Type: Article

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