Electrochemical discharge of nanocrystalline magnetite: Structure analysis using X-ray diffraction and X-ray absorption spectroscopy

Physical Chemistry Chemical Physics

Volumn 15, Issue 42, 2013, Pages 18539-18548

  Menard, Melissa C ^a,b   Takeuchi, Kenneth J ^a   Marschilok, Amy C ^a,b   Takeuchi, Esther S ^a,b,c  

^a STONY BROOK UNIVERSITY   (United States)

^b Stony Brook University   (United States)

^c BROOKHAVEN NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

LITHIUM; MAGNETITE NANOPARTICLE;

ARTICLE; CHEMISTRY; ELECTROCHEMISTRY; PARTICLE SIZE; X RAY ABSORPTION SPECTROSCOPY; X RAY DIFFRACTION;

ELECTROCHEMISTRY; LITHIUM; MAGNETITE NANOPARTICLES; PARTICLE SIZE; X-RAY ABSORPTION SPECTROSCOPY; X-RAY DIFFRACTION;

EID: 84885597289     PISSN: 14639076     EISSN: None     Source Type: Journal    
DOI: 10.1039/c3cp52870g     Document Type: Article

References (40)

1. D. C. Bock A. C. Marschilok K. J. Takeuchi E. S. Takeuchi Batteries used to power implantable biomedical devices Electrochim. Acta 2012 84 155 164
2. G. L. Soloveichik, Battery Technologies for Large-Scale Stationary Energy Storage, in Annual Review of Chemical and Biomolecular Engineering, vol. 2. Annual Review of Chemical and Biomolecular Engineering 2, ed., J. M. Prausnitz, Annual Reviews, Palo Alto, 2011, pp. 503-527
3. M. Mahmoudi S. Sant B. Wang S. Laurent T. Sen Superparamagnetic iron oxide nanoparticles (SPIONs): development, surface modification and applications in chemotherapy Adv. Drug Delivery Rev. 2011 63 1-2 24 46
4. D. A. Marsh M. W. Szyndler R. M. Corn A. S. Borovik Preparation of monolithic superparamagnetic nanoparticle-polymer composites using a polymerizable acetylacetonate and magnetite nanoparticles Polym. Chem. 2012 3 10 2852 2856
5. 4 nanocrystals Phys. Chem. Chem. Phys. 2010 12 9 2063 2066
6. A. M. Yashchenok D. A. Gorin M. Badylevich A. A. Serdobintsev M. Bedard Y. G. Fedorenko et al. Impact of magnetite nanoparticle incorporation on optical and electrical properties of nanocomposite LbL assemblies Phys. Chem. Chem. Phys. 2010 12 35 10469 10475
7. M. M. Thackeray Spinel electrodes for lithium batteries J. Am. Ceram. Soc. 1999 82 12 3347 3354 (Pubitemid 30541065)
8. 4 Electrochem. Solid-State Lett. 2009 12 4 A91 A94
9. S. Zhu A. C. Marschilok E. S. Takeuchi G. T. Yee G. Wang K. J. Takeuchi Nanocrystalline magnetite: synthetic crystallite size control and resulting magnetic and electrochemical properties J. Electrochem. Soc. 2010 157 A1158 A1163
10. 4) microspheres: the highly powerful storage versus lithium as an anode for lithium ion batteries J. Phys. Chem. C 2012 116 10 6495 6502
11. 4 fuzzy spheroids as anode materials for lithium-ion batteries Mater. Lett. 2012 71 151 153
12. 4 nanoparticles and its application in lithium ion batteries Mater. Chem. Phys. 2011 130 1260 1264
13. 4 J. Solid State Chem. 1988 77 1 180 189
14. 4 J. Appl. Phys. 1986 59 1918 1926
15. 4 sample by the X-ray Rietveld method J. Mater. Sci. 1987 22 1001 1005 (Pubitemid 17569939)
16. 4 as a cathode material J. Power Sources 2005 146 1-2 319 322
17. 4 nanoparticles and its application in lithium ion battery Mater. Lett. 2009 63 30 2701 2703
18. Y. Joseph M. Wuhn A. Niklewski W. Ranke W. Weiss C. Woll et al. Interaction of ethylbenzene and styrene with iron oxide model catalyst films at low coverages: a NEXAFS study Phys. Chem. Chem. Phys. 2000 2 22 5314 5319
19. W. Ra M. Nakayama W. Cho M. Wakihara Y. Uchimoto Electronic and local structural changes in Li2+xTi3O7 ramsdellite compounds upon electrochemical Li-ion insertion reactions by X-ray absorption spectroscopy Phys. Chem. Chem. Phys. 2006 8 7 882 889
20. 4 - a comparative study Phys. Chem. Chem. Phys. 2011 13 45 20215 20222
21. L. Signorini L. Pasquini L. Saini R. Carboni F. Boscherini E. Bonetti et al. Size-dependent oxidation in iron/iron oxide core-shell nanoparticles Phys. Rev. B: Condens. Matter Mater. Phys. 2003 68 195423
22. 2 (A = K, Rb, Cs) family: a comparitive study of structures and structural phase transitions J. Solid State Chem. 2010 183 752 759
23. A. C. Larson, R. B. Von Dreele, General Structure Analysis System (GSAS), Los Alamos National Laboratory Report LAUR, 2000, 86-748
24. B. H. Toby EXPGUI, a graphical user interface for GSAS J. Appl. Crystallogr. 2001 34 210 213 (Pubitemid 32290310)
25. C. J. Howard J. Appl. Crystallogr. 1982 15 615 620
26. P. Thompson D. E. Cox J. B. Hastings J. Appl. Crystallogr. 1987 20 79 83
27. A. L. Patterson The Scherrer formula for X-ray particle size determination Phys. Rev. 1939 56 10 978 982
28. 3 J. Appl. Crystallogr. 1987 20 2 79 83
29. B. Ravel M. Newville ATHENA, ARTEMIS, HEPHAESTUS: data analysis for X-ray absorption spectroscopy using IFEFFIT J. Synchrotron Radiat. 2005 12 537 541 (Pubitemid 41557599)
30. 4 Hyperfine Interact. 1986 28 769 772
31. M. C. Menard A. C. Marschilok K. J. Takeuchi E. S. Takeuchi Variation in the iron oxidation states of magnetite nanocrystals as a function of crystallite size: the impact on electrochemical capacity Electrochim. Acta 2012 94 320 326
32. 4 in aprotic Li and Na salt electrolytes Electrochem. Commun. 2008 10 1276 1279
33. 3 (0 < x < 2) Mater. Res. Bull. 1982 17 6 785 793
34. V. M. Goldschmidt, T. Barth, D. Holmsen, G. Lunde, W. Zachariasen, Geochemische Verteilungsgesetze VI. Ueber die Kristallstrukturen vom Rutiltypus, mit Bemerkungen zur Geochemie zweiwertiger und vierwertiger Elemente (FeO), Skrifter utgitt av det Norske Videnskaps-Akademi i Oslo 1: Matematisk- Naturvidenskapelig Klasse, 1926, 1, 21
35. ed., P. C. Doresy, V. G. Harris, D. B. Christy, P. Lubitz, J. S. Horowitz, and, N. C. Koon, Applications of Synchrotron Radiation Techniques to Materials Science, Materials Research Society, Pittsburg, 1995
36. V. G. Harris N. C. Koon C. M. Williams Q. Zhang M. Abe J. P. Kirkland et al. Direct measurement fo octahedral and tetrahedral site environments in NiZn-Ferrites IEEE Trans. Magn. 1995 31 3473 3475
37. 3 with various particle sizes J. Electrochem. Soc. 2003 150 12 A1643 A1650
38. N. A. Godshall I. D. Raistrick R. A. Huggins Relationships among electrochemical, thermodynamic, and oxygen potential quantities in lithium-transition metal-oxygen molten salt cells J. Electrochem. Soc. 1984 131 3 543 549 (Pubitemid 14551748)
39. R. Kohlhaas P. Duenner N. Schmitz-Pranghe Ueber die Temperaturabhaengigkeit der Gitterparameter von Eisen, Kobalt und Nickel im Bereich hoher Temperaturen Z. Angew. Phys. 1967 23 245 249
40. M. M. Thackeray L. A. De Picciotto A. DK P. J. Johnson V. A. Nicholas K. T. Adendorff Spinel electrodes for lithium batteries-a review J. Power Sources 1987 21 1 8