Synthesis and characterization of homo- and heterometallic metal-organic frameworks based on 1,2,4,5-benzenetetracarboxylate ligand

Inorganic Chemistry Communications

Volumn 36, Issue , 2013, Pages 195-198

  Yang, E ^a,b   Ding, Qing Rong ^a,b   Kang, Yao ^b   Wang, Fei ^b  

^a FUJIAN NORMAL UNIVERSITY   (China)

^b FUJIAN INSTITUTE OF RESEARCH ON THE STRUCTURE OF MATTER   (China)

Author keywords

Crystal structure; Lithium; MOFs; Photoluminescence; Topology; Zinc

Indexed keywords

EID: 84884660513     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2013.08.031     Document Type: Article

References (25)

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19. Crystal data for 1: C17H25N3O9Zn, M = 480.78, Tetragonal, a = 18.9381(3) Å, b = 18.9381(3) Å, c = 21.2008(7) Å, α = β = γ = 90 V = 7603.7(3) Å3, T = 296 K, space group I4(1)/amd, Z = 16, 7103 reflections measured, 1929 independent flections (Rint = 0.0288). The final R1 value was 0.0605 (I > 2σ(I)). The final wR(F2) value was 0.1987 (I > 2σ(I)). The final R1 value was 0.0670 (all data). The final wR(F2) value was 0.2085 (all data). The goodness of fit on F2 was 1.028. Crystal data for 2: C15H17N2O9ZnLi, M = 441.63, Orthorhombic, a = 19.9292(5) Å, b = 25.9815(8) Å, c = 29.2054(10) Å, α = β = γ = 90 V = 15122.3(8) Å3, T = 100 K, space group Fddd, Z = 32, 9122 reflections measured, 3753 independent flections (Rint = 0.0207). The final R1 value was 0.0360 (I > 2σ(I)). The final wR(F2) value was 0.1113 (I > 2σ(I)). The final R1 value was 0.0424 (all data). The final wR(F2) value was 0.1170 (all data). The goodness of fit on F2 was 1.071. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC: 948129, 948128. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (44) 1223 336-033; e-mail: deposit@ccdc.cam.ac.uk).
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