Quantitative analysis of conjugated and free estrogens in swine manure: Solutions to overcome analytical problems due to matrix effects

Journal of Chromatography A

Volumn 1305, Issue , 2013, Pages 203-212

  Singh, Ashok K ^a   Gupta, Shveta ^a   Kumar, Kuldip ^c   Gupta, Satish ^b   Chander, Yogesh ^a   Gupta, Arun ^a   Saxena, Richa ^a  

^a UNIVERSITY OF MINNESOTA   (United States)

^b UNIVERSITY OF MINNESOTA   (United States)

^c Research and Development Department   (United States)

Author keywords

Chromatography; Conjugated; Estrogens; Manure; Mass spectrometry; Matrix effects

Indexed keywords

CHROMATOGRAPHIC METHODS; CONJUGATED; CONJUGATED ESTROGENS; ENVIRONMENTAL ESTROGENS; ESTROGENS; HYDROPHILIC LIPOPHILIC BALANCE; LABELED INTERNAL STANDARDS; MATRIX EFFECTS;

CALIBRATION; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DESORPTION; ENDOCRINOLOGY; HORMONES; LIQUIDS; MANURES; MASS SPECTROMETERS; MASS SPECTROMETRY;

EXTRACTION;

ACETIC ACID ETHYL ESTER; CARBON; CONJUGATED ESTROGEN; DEUTERIUM; ESTROGEN; WATER;

ACIDIFICATION; ARTICLE; CALIBRATION; CONTROLLED STUDY; DEGRADATION KINETICS; DESORPTION; ELUTION; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHILICITY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIPOPHILICITY; MANURE; MASS FRAGMENTOGRAPHY; NONHUMAN; PH; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SEPARATION TECHNIQUE; STANDARD; STORAGE TEMPERATURE; SWINE; TANDEM MASS SPECTROMETRY;

(13)C-FE2; (13)C-GE2; (13)C-IS; (13)C-LABELED ESTRADIOL GLUCURONIDE; (13)C-LABELED ESTRADIOL SULFATE; (13)C-LABELED FREE ESTRADIOL; (13)C-LABELED INTERNAL STANDARD; (13)C-SE2; ALPHA ESTRADIOL-FREE; CHROMATOGRAPHY; CONJUGATED; DEUTERATED ESTRADIOL GLUCURONIDE; DEUTERATED ESTRADIOL SULFATE; DEUTERATED ESTRIOL GLUCURONIDE; DEUTERATED ESTRIOL SULFATE; DEUTERATED ESTRONE GLUCURONIDE; DEUTERATED ESTRONE SULFATE; DEUTERATED FREE BETA ESTRADIOL; DEUTERATED FREE ESTRIOL; DEUTERATED FREE ESTRONE; DEUTERATED INTERNAL STANDARD; DFE1; DFE2; DFE3; DGE1; DGE2; DGE3; DIS; DSE1; DSE2; DSE3; ESTRADIOL GLUCURONIDE; ESTRADIOL SULFATE; ESTRIOL GLUCURONIDE; ESTRIOL SULFATE; ESTROGENS; ESTRONE GLUCURONIDE; ESTRONE SULFATE; FΑE2; FE1; FE2; FE3; FP; FREE BETA-ESTRADIOL; FREE ESTRIOL; FREE ESTRONE; FREE PROGESTERONE; FREE TESTOSTERONE; FT; GE1; GE2; GE3; GT; INTERNAL STANDARD; IS; MANURE; MASS SPECTROMETRY; MATRIX EFFECTS; SE1; SE2; SE3; ST; TESTOSTERONE GLUCURONIDE; TESTOSTERONE SULFATE;

ANIMALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ESTROGENS; LIMIT OF DETECTION; MANURE; MASS SPECTROMETRY; REFERENCE STANDARDS; SWINE;

ANIMALIA; SUIDAE;

EID: 84881312931     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.06.026     Document Type: Article

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