Combination of the QuEChERS method with dispersive liquid-liquid microextraction and derivatization in the determination of mycotoxins in grain and mixed feed by gas-liquid chromatography with an electron-capture detector

Journal of Analytical Chemistry

Volumn 68, Issue 6, 2013, Pages 552-557

  Amelin, V G ^a,b   Karaseva, N M ^a,b   Tret'Yakov, A V ^b  

^a VLADIMIR STATE UNIVERSITY   (Russian Federation)

^b Federal Centre for Animal Health (FGI ARRIAH)   (Russian Federation)

Author keywords

deoxynivalenol; dispersive liquid liquid microextraction; electron capture detector; gas liquid chromatography; grain; HT 2; mixed feed; mycotoxins; nivalenol; QuEChERS method; toxin T 2

Indexed keywords

DEOXYNIVALENOL; DISPERSIVE LIQUID-LIQUID MICROEXTRACTION; ELECTRON CAPTURE DETECTORS; GAS-LIQUID CHROMATOGRAPHY; HT-2; MIXED FEED; MYCOTOXINS; NIVALENOL; QUECHERS; TOXIN T-2;

CHEMICAL CONTAMINATION; DETECTORS; GAS CHROMATOGRAPHY; GRAIN (AGRICULTURAL PRODUCT); TOXICITY;

SOLVENT EXTRACTION;

EID: 84878741430     PISSN: 10619348     EISSN: None     Source Type: Journal    
DOI: 10.1134/S1061934813060026     Document Type: Article

References (18)

1. Murfhy, P.A., Hendrich, S., Landgren, C., and Bryant, C.M., J. Food Sci., 2006, vol. 71, p. 5.
2. Drugov, Yu.S. and Rodin, A.A., Analiz zagryaznennykh biosred i pishchevykh produktov (Monitoring of Contaminated Biomedia and Foods), Moscow: BINOM. Laboratoriya znanii, 2007.
3. Pittet, A., Mitt. Lebensm., 2005, vol. 96, p. 424.
4. Sychev, K.S., Sorbts. Khromatogr. Prots., 2004, vol. 4, no. 1, p. 5.
5. Garner, R.C., Whattam, M.M., Taylor, P.J.L., and Stow, M.W., J. Chromatogr., A, 1993, vol. 648, p. 485.
6. Trucksess, M.W. and Tang, Y., J. AOAC Int., 1999, vol. 82, p. 1109.
7. Krska, R., J. Chromatogr., A, 1998, vol. 815, p. 49.
8. Burdaspal, P., Add. Contam., 1997, p. 237.
9. Kotal, F. and Radova, Z., J. Food Sci., 2007, vol. 20, p. 63.
10. Croteau, S.M., Prelusky, D.B., and Trenholm, H.L., J. Agric. Food Chem., 1994, vol. 42, p. 928.
11. Schothorst, R.C. and Jekel, A.A., Food Chem., vol. 73, p. 111.
12. Biselli, S. and Hummert, C., J. Food Add. Contam., 2005, vol. 22, p. 752.
13. GOST (State Standard) R 51116-97: Feed Premixes, Grains, and Their Processing Products. Method to Analysis of Deoxynivalenol, 1999.
14. GOST (State Standard) 28001-88: Forage Grain, Its Processing Products and Feedstuff. Methods to Determination of Micotoxins: T-2 Toxin, Zearalenone, and Ochratoxin A, 1990.
15. Tremasov, M.Ya., Sergeichev, A.I., Smetov, P.K., and Ravilov, A.Z., Veterinariya, 1997, no. 10, p. 45.
16. Anastassiades, M., Stajnbaher, D., and Schenck, F.J., J. AOAC Int., 2003, vol. 86, p. D.135.
17. Hajslova, J., Zachariasova, M., and Cajka, T., Mass Spectrometry in Food Safety: Methods and Protocols, Methods in Molecular Biology, 2011, vol. 747, p. 233.
18. Tretyakov, A., Amelin, V., and Karaseva, N., Abstracts of Papers, 5th Int. Symp. on Recent Advances in Food Analysis, Prague, 2011.