On the nature of structural disorder in calcium silicate hydrates with a calcium/silicon ratio similar to tobermorite

Cement and Concrete Research

Volumn 52, Issue , 2013, Pages 31-37

  Grangeon, Sylvain ^a   Claret, Francis ^a   Lerouge, Catherine ^a   Warmont, Fabienne ^b   Sato, Tsutomu ^c   Anraku, Sohtaro ^c   Numako, Chiya ^d   Linard, Yannick ^e   Lanson, Bruno ^f  

^a BRGM   (France)

^b CNRS   (France)

^c HOKKAIDO UNIVERSITY   (Japan)

^d UNIVERSITY OF TOKUSHIMA   (Japan)

^e ANDRA   (France)

^f UNIVERSITÉ GRENOBLE ALPES   (France)

Author keywords

Calcium silicate hydrate (CSH); Crystal structure; Spectroscopy TEM; X ray diffraction

Indexed keywords

CALCIUM SILICATE HYDRATE; EXTENDED X-RAY ABSORPTION FINE STRUCTURES; MODELING APPROACH; NANOCRYSTALLINES; NATURALLY OCCURRING; POWDER X RAY DIFFRACTION; REFINEMENT TECHNIQUES; STRUCTURAL DISORDERS;

CALCIUM SILICATE; CRYSTAL STRUCTURE; EXTENDED X RAY ABSORPTION FINE STRUCTURE SPECTROSCOPY; GEOMETRY; HYDRATES; HYDRATION; RIETVELD ANALYSIS; SILICATE MINERALS; TRANSMISSION ELECTRON MICROSCOPY; X RAY DIFFRACTION;

CRYSTAL ATOMIC STRUCTURE;

EID: 84878428404     PISSN: 00088846     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cemconres.2013.05.007     Document Type: Article

References (62)

1. J.J. Chen, J.J. Thomas, H.F.W. Taylor, and H.M. Jennings Solubility and structure of calcium silicate hydrate Cem. Concr. Res. 34 2004 1499 1519
2. H.F.W. Taylor, and D.E. Newbury Calcium hydroxide distribution and calcium silicate hydrate composition in tricalcium silicate and β-dicalcium silicate pastes Cem. Concr. Res. 14 1984 93 98 (Pubitemid 14534372)
3. H. Manzano, J.S. Dolado, A. Guerrero, and A. Ayuela Mechanical properties of crystalline calcium-silicate-hydrates: comparison with cementitious CSH gels Phys. Status Solidi A 204 2007 1775 1780 (Pubitemid 47120176)
4. I.G. Richardson, and G.W. Groves Microstructure and microanalysis of hardened ordinary Portland cement pastes J. Mater. Sci. 28 1993 265 277
5. A. Nonat The structure and stoichiometry of CSH Cem. Concr. Res. 34 2004 1521 1528
6. H.F.W. Taylor Nanostructure of CSH: current status Adv. Cem. Based Mater. 1 1993 38 46
7. I.G. Richardson The nature of CSH in hardened cements Cem. Concr. Res. 29 1999 1131 1147
8. A.V. Girão, I.G. Richardson, R. Taylor, and R.M.D. Brydson Composition, morphology and nanostructure of CSH in 70% white Portland cement-30% fly ash blends hydrated at 55 C Cem. Concr. Res. 40 2010 1350 1359
9. C. Plassard, E. Lesniewska, I. Pochard, and A. Nonat Investigation of the surface structure and elastic properties of calcium silicate hydrates at the nanoscale Ultramicroscopy 100 2004 331 338 (Pubitemid 38834142)
10. M. Atkins, F.P. Glasser, and A. Kindness Cement hydrate phase: solubility at 25 C Cem. Concr. Res. 22 1992 241 246
11. P. Blanc, X. Bourbon, A. Lassin, and E.C. Gaucher Chemical model for cement-based materials: temperature dependence of thermodynamic functions for nanocrystalline and crystalline CSH phases Cem. Concr. Res. 40 2010 851 866
12. K. Fujii, and W. Kondo Heterogeneous equilibrium of calcium silicate hydrate in water at 30 C J. Chem. Soc., Dalton Trans. 1981 645 651
13. 2 - Advances in Cement Research 1997 167 181 (Pubitemid 127544650)
14. P. Blanc, A. Lassin, P. Piantone, M. Azaroual, N. Jacquemet, A. Fabbri, and E.C. Gaucher Thermoddem: a geochemical database focused on low temperature water/rock interactions and waste materials Appl. Geochem. 27 2012 2107 2116
15. G. Renaudin, J. Russias, F. Leroux, F. Frizon, and C. Cau-dit-Coumes Structural characterization of CSH and CASH samples - part I: long-range order investigated by Rietveld analyses J. Solid State Chem. 182 2009 3312 3319
16. G.W. Groves, P.J. Le Sueur, and W. Sinclair Transmission electron microscopy and microanalytical studies of ion-beam-thinned sections of tricalcium silicate paste J. Am. Ceram. Soc. 69 1986 353 356 (Pubitemid 16521052)
17. P. Yu, R.J. Kirkpatrick, B. Poe, P.F. McMillan, and X. Cong Structure of calcium silicate hydrate (CSH): near-, mid-, and far-infrared spectroscopy J. Am. Ceram. Soc. 82 1999 742 748
18. R.J. Kirkpatrick, J.L. Yarger, P.F. McMillan, Y. Ping, and X. Cong Raman spectroscopy of CSH, tobermorite, and jennite Adv. Cement Based Mater. 5 1997 93 99
19. 29Si MAS NMR study of the structure of calcium silicate hydrate Adv. Cement Based Mater. 3 1996 144 156
20. 17O NMR investigation of the structure of some crystalline calcium silicate hydrates Adv. Cement Based Mater. 3 1996 133 143
21. 43Ca NMR spectroscopy of tobermorite and jennite: model compounds for CSH J. Am. Ceram. Soc. 92 2009 545 548
22. N. Lequeux, A. Morau, S. Philippot, and P. Boch Extended X-ray absorption fine structure investigation of calcium silicate hydrates J. Am. Ceram. Soc. 82 1999 1299 1306 (Pubitemid 129692888)
23. A.J. Allen, and J.J. Thomas Analysis of CSH gel and cement paste by small-angle neutron scattering Cem. Concr. Res. 37 2007 319 324 (Pubitemid 46275627)
24. A.J. Allen, J.J. Thomas, and H.M. Jennings Composition and density of nanoscale calcium-silicate-hydrate in cement Nat. Mater. 6 2007 311 316 (Pubitemid 46516823)
25. L.B. Skinner, S.R. Chae, C.J. Benmore, H.R. Wenk, and P.J.M. Monteiro Nanostructure of calcium silicate hydrates in cements Phys. Rev. Lett. 104 2010 195502
26. F.P. Glasser, E.E. Lachowski, and D.E. Macphee Compositional model for calcium silicate hydrate (CSH) gels, their solubilities, and free energies of formation J. Am. Ceram. Soc. 70 1987 481 485
27. 3S hydration under controlled solution P. Colombet, A.-R. Grimmer, H. Zanni, P. Sozzani, Nuclear Magnetic Resonance Spectroscopy of Cement Based Materials 1996 Springer Berlin 197 207
28. I.G. Richardson, and G.W. Groves Models for the composition and structure of calcium silicate hydrate (CSH) gel in hardened tricalcium silicate pastes Cem. Concr. Res. 22 1992 1001 1010 (Pubitemid 23592736)
29. H.F.W. Taylor Proposed structure for calcium silicate hydrate gel J. Am. Ceram. Soc. 69 1986 464 467
30. I.G. Richardson The calcium silicate hydrates Cem. Concr. Res. 38 2008 137 158 (Pubitemid 50017994)
31. E. Bonaccorsi, S. Merlino, and A.R. Kampf The crystal structure of tobermorite 14 Å (plombierite), a CSH phase J. Am. Ceram. Soc. 88 2005 505 512 (Pubitemid 43026512)
32. S. Merlino, E. Bonaccorsi, and T. Armbruster Tobermorites; their real structure and order-disorder (OD) character Am. Mineral. 84 1999 1613 1621 (Pubitemid 30052329)
33. S. Merlino, E. Bonaccorsi, and T. Armbruster The real structures of clinotobermorite and tobermorite 9 Å Eur. J. Mineral. 12 2000 411 429
34. S. Merlino, E. Bonaccorsi, and T. Armbruster The real structure of tobermorite 11 Å Eur. J. Mineral. 13 2001 577 590
35. 29Si NMR in cement: a theoretical study on calcium silicate hydrates J. Phys. Chem. C 116 2012 9755 9761
36. S. Soyer-Uzun, S.R. Chae, C.J. Benmore, H.-R. Wenk, and P.J.M. Monteiro Compositional evolution of calcium silicate hydrate (CSH) structures by total X-ray scattering J. Am. Ceram. Soc. 95 2012 793 798
37. 29Si NMR and thermal behavior Cem. Concr. Res. 33 2003 1515 1523
38. X. Cong, and R.J. Kirkpatrick Effects of the temperature and relative humidity on the structure of CSH gel Cem. Concr. Res. 25 1995 1237 1245
39. T.R. Sweatman, and J.V.P. Long Quantitative electron-probe microanalysis of rock-forming minerals J. Petrol. 10 1969 332 379
40. B. Ravel, and M. Newville ATHENA, ARTEMIS, HEPHAESTUS: data analysis for X-ray absorption spectroscopy using IFEFFIT J. Synchrotron Radiat. 12 2005 537 541 (Pubitemid 41557599)
41. M. Newville IFEFFIT: interactive XAFS analysis and FEFF fitting J. Synchrotron Radiat. 8 2001 322 324 (Pubitemid 33661380)
42. B. Ravel ATOMS: crystallography for the X-ray absorption spectroscopist J. Synchrotron Radiat. 8 2001 314 316 (Pubitemid 33661377)
43. A.L. Ankudinov, and J.J. Rehr Relativistic calculations of spin-dependent X-ray-absorption spectra Phys. Rev. B 56 1997 R1712 R1716
44. B.E. Warren X-ray diffraction in random layer lattices Phys. Rev. 59 1941 693
45. A. Plancon Diffraction by layer structures containing different kinds of layers and stacking faults J. Appl. Crystallogr. 14 1981 300 304
46. A. Plancon CALCIPOW: a program for calculating the diffraction by disordered lamellar structures J. Appl. Crystallogr. 35 2002 377
47. V.A. Drits, and C. Tchoubar X-ray Diffraction by Disordered Lamellar Structures: Theory and Applications to Microdivided Silicates and Carbons 1990 Springer-Verlag Berlin
48. M. Villalobos, B. Lanson, A. Manceau, B. Toner, and G. Sposito Structural model for the biogenic Mn oxide produced by Pseudomonas putida Am. Mineral. 91 2006 489 502
49. W.P. Gates, P.G. Slade, A. Manceau, and B. Lanson Site occupancies by iron in nontronites Clays Clay Miner. 50 2002 223 239
50. S. Grangeon, B. Lanson, M. Lanson, and A. Manceau Crystal structure of Ni-sorbed synthetic vernadite: a powder X-ray diffraction study Mineral. Mag. 72 2008 1279 1291
51. S. Grangeon, B. Lanson, N. Miyata, Y. Tani, and A. Manceau Structure of nanocrystalline phyllomanganates produced by freshwater fungi Am. Mineral. 95 2010 1608 1616
52. 2 + oxidation by the phyllomanganate buserite Am. Mineral. 82 1997 1150 1175
53. S.A. Howard, and K.D. Preston Profile fitting of powder diffraction patterns Rev. Mineral. Geochem. 20 1989 217 275
54. E.D. Crozier A review of the current status of XAFS spectroscopy Nucl. Instrum. Methods Phys. Res. Sect. B Beam Interact. Mater. Atoms 133 1997 134 144 (Pubitemid 127379337)
55. B.K. Teo EXAFS: Basic Principles and Data Analysis 1986 Springer Berlin
56. R. Reynolds Jnr The effect of particle size on apparent lattice spacings Acta Crystallogr. Sect. A 24 1968 319 320
57. V. Trunz The influence of crystallite size on the apparent basal spacings of kaolinite Clays Clay Miner. 24 1976 84 87
58. D.L. Bish, and J.E. Post Modern Powder Diffraction 1990 The Mineralogical Society of America Washington D.C.
59. W.H. Qi, M.P. Wang, and Y.C. Su Size effect on the lattice parameters of nanoparticles J. Mater. Sci. Lett. 21 2002 877 878 (Pubitemid 34811777)
60. T. Mitsuda, and H.F.W. Taylor Influence of aluminium on the conversion of calcium silicate hydrate gels into 11 Å tobermorite at 90 C and 120 C Cem. Concr. Res. 5 1975 203 209
61. 2): an in situ synchrotron study Chem. Geol. 167 2000 129 140 (Pubitemid 30324684)
62. 2O Cem. Concr. Res. 34 2004 1481 1488