Simultaneous determination of nine trace organophosphorous pesticide residues in fruit samples using molecularly imprinted matrix solid-phase dispersion followed by gas chromatography

Journal of Agricultural and Food Chemistry

Volumn 61, Issue 16, 2013, Pages 3821-3827

  Wang, Xilong ^a   Qiao, Xuguang ^a   Ma, Yue ^a   Zhao, Tao ^a   Xu, Zhixiang ^a  

^a SHANDONG AGRICULTURAL UNIVERSITY   (China)

Author keywords

gas chromatography; matrix solid phase dispersion; molecular imprinting; multipesticide residues

Indexed keywords

ETHYLENE GLYCOL DIMETHACRYLATE; MOLECULAR IMPRINTING; MOLECULARLY IMPRINTED POLYMER; MULTIPESTICIDE RESIDUES; ORGANOPHOS-PHORUS PESTICIDES; ORGANOPHOSPHATE PESTICIDES; ORGANOPHOSPHOROUS PESTICIDES; SIMULTANEOUS DETERMINATIONS;

CROSSLINKING; FRUITS; MATRIX SOLID PHASE DISPERSION; PESTICIDES; POLYMERS;

GAS CHROMATOGRAPHY;

CROSS LINKING REAGENT; ETHYLENE GLYCOL DIMETHACRYLATE; METHACRYLIC ACID DERIVATIVE; ORGANOPHOSPHORUS COMPOUND; PESTICIDE RESIDUE; POLYMER;

ADSORPTION; ARTICLE; CHEMISTRY; FOOD CONTAMINATION; FRUIT; GAS CHROMATOGRAPHY; METHODOLOGY; MOLECULAR IMPRINTING;

ADSORPTION; CHROMATOGRAPHY, GAS; CROSS-LINKING REAGENTS; FOOD CONTAMINATION; FRUIT; METHACRYLATES; MOLECULAR IMPRINTING; ORGANOPHOSPHORUS COMPOUNDS; PESTICIDE RESIDUES; POLYMERS;

MALUS X DOMESTICA; PYRUS;

EID: 84876701255     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf400269q     Document Type: Article

References (25)

1. Stoytcheva, M.; Zlatev, R.; Velkova, Z.; Valdez, B.; Ovalle, M.; Petkov, L. Hybrid electrochemical biosensor for organophosphorus pesticides quantification Electrochim. Acta 2009, 54, 1721-1727
2. Mulchandani, P.; Mulchandani, A.; Kaneva, I.; Chen, W. Biosensor for the direct determination of pesticides Biosens. Bioelectron. 2001, 16, 225-230
3. Mathew, S. B.; Pillai, A. K.; Gupta, V. K. A rapid spectrophotometric assay of some organophosphorus pesticide residues in vegetable samples Spectrochim. Acta A 2007, 67, 1430-1432
4. Russoa, M. V.; Campanella, L.; Avino, P. Determination of organophosphorus pesticide residues in human tissues by capillary gas chromatography-negative chemical ionization mass spectrometry analysis J. Chromatogr., B 2002, 780, 431-441
5. Zhang, Q.; Sun, Q.; Hu, B. S.; Shen, Q.; Yang, G.; Liang, X.; Sun, X.; Liu, F. Q. Development of a sensitive ELISA for the analysis of the organophosphorous insecticide fenthion in fruit samples Food Chem. 2008, 106, 1278-1284
6. García, R. C.; álvarez, L. G.; Puerta, A.; Blanco, E.; Sanz, M. A.; Marina, M. L. Enantiomeric separation of organophosphorus pesticides by capillary electrophoresis: Application to the determination of malathion in water samples after preconcentration by off-line solid-phase extraction Anal. Chim. Acta 2005, 543, 77-83
7. Zhu, X. L.; Cai, J. B.; Yang, J.; Su, Q. D.; Gao, Y. Films coated with molecular imprinted polymers for the selective stir bar sorption extraction of monocrotophos J. Chromatogr., A 2006, 1131, 37-44
8. Lee, H. S.; Kim, Y. A.; Cho, Y. A.; Lee, Y. T. Oxidation of organophosphorus pesticides for the sensitive detection by a cholinesterase-based biosensor Chemosphere 2002, 46, 571-576
9. Xin, J. H.; Qiao, X. G.; Ma, Y.; Xu, Z. X. Simultaneous separation and determination of eight organophosphorous pesticide residues in vegetables through molecularly imprinted solid-phase extraction coupled to gas chromatography J. Sep. Sci. 2012, 35, 3501-3508
10. Kim, D. H.; Heo, G. S.; Lee, D. W. Determination of organophosphorus pesticides in wheat flour by supercritical fluid extraction and gas chromatography with nitrogen-phosphorus detection J. Chromatogr., A 1998, 824, 63-70
11. Rial-Otero, R.; Gaspar, E. M.; Moura, I.; Capelo, J. L. Chromatographic-based methods for pesticide determination in honey: an overview Talanta 2007, 71, 503-514
12. Fytianos, K.; Raikos, N.; Theodoridis, G.; Velinova, Z.; Tsoukali, H. Solid phase microextraction applied to the analysis of organophosphorus insecticides in fruits Chemosphere 2006, 65, 2090-2095
13. Baltussen, E.; Sandra, P.; David, F.; Cramers, C. Stir bar sorptive extraction (SBSE), a novel extraction technique for aqueous samples: theory and principles J. Microcolumn Sep. 1999, 11, 737-747
14. Bolaños, P. P.; Frenich, G. A.; Vidal, M. J. L. Application of gas chromatography-triple quadrupole mass spectrometry in the quantification- confirmation of pesticides and polychlorinated biphenyls in eggs at trace levels J. Chromatogr., A 2007, 1167, 9-17
15. Rezaee, M.; Assadi, Y.; Hosseini, M. R. M.; Aghaee, E.; Ahmadi, F.; Berijani, S. Determination of organic compounds in water using dispersive liquid-liquid microextraction J. Chromatogr., A 2006, 1116, 1-9
16. Barker, S. A. Applications of matrix solid-phase dispersion in food analysis J. Chromatogr., A 2000, 880, 63-68
17. Lu, Y. B.; Zheng, T. L.; He, X.; Lin, X. J.; Chen, L. Y.; Dai, Z. Y. Rapid determination of chloramphenicol in soft-shelled turtle tissues using on-line MSPD-HPLC-MS/MS Food Chem. 2012, 134, 533-539
18. Meng, L.; Qiao, X. G.; Song, J. M.; Xu, Z. X.; Xin, J. H.; Zhang, Y. Study of an online molecularly imprinted solid phase extraction coupled to chemiluminescence sensor for the determination of trichlorfon in vegetables J. Agric. Food Chem. 2011, 59, 12749-12751
19. Turiel, E.; Martin-Esteban, A. Molecularly imprinted polymers: towards highly selective stationary phases in liquid chromatography and capillary electrophoresis Anal. Bioanal. Chem. 2004, 378, 1876-1886
20. Bui, B. T. S.; Haucpt, K. Molecularly imprinted polymers: synthetic receptors in bioanalysis Anal. Bioanal. Chem. 2010, 398, 2481-2492
21. Molinelli, A.; Weiss, R.; Mizaikoff, B. Advanced solid phase extraction using molecularly imprinted polymers for the determination of quercetin in red wine J. Agric. Food Chem. 2002, 50, 1804-1808
22. Haginaka, J. Molecularly imprinted polymers for solid-phase extraction Anal. Bioanal. Chem. 2004, 379, 332-334
23. Xin, J. H.; Qiao, X. G.; Xu, Z. X.; Zhou, J. Molecularly imprinted polymer as sorbent for solid-phase extraction coupling to gas chromatography for the simultaneous determination of trichlorfon and monocrotophos residues in vegetables Food Anal. Methods 2013, 6, 274-281
24. Zhang, Q.; Wang, L. B.; Ahn, K. C.; Sun, Q.; Hu, B. S.; Wang, J.; Liu, F. Q. Hapten heterology for a specific and sensitive indirect enzyme-linked immunosorbent assay for organophosphorus insecticide fenthion Anal. Chim. Acta 2007, 596, 303-311
25. Gong, S. L.; Yu, Z. J.; Meng, L. Z.; Hu, L.; He, Y. B. Dye molecular-imprinted polusiloxanes. II. Preparation, characterization, and recognition behavior J. Appl. Polym. Sci. 2004, 93, 637-643