Preparation of barium sulfate nanoparticles in an interdigital channel configuration micromixer SIMM-V2

Industrial and Engineering Chemistry Research

Volumn 52, Issue 15, 2013, Pages 5313-5320

  Wu, Hui ^a   Wang, Chongqing ^a   Zeng, Changfeng ^a   Zhang, Lixiong ^a  

^a NANJING TECH UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

AVERAGE PARTICLE SIZE; BARIUM SULFATE; CHANNEL CONFIGURATION; INTERDIGITAL; MEAN PARTICLE SIZE; PREPARATION PROCESS; SATURATION CONCENTRATION; SYNTHESIS SOLUTION;

FLOW RATE; MIXERS (MACHINERY); NANOPARTICLES; PARTICLE SIZE; PARTICLE SIZE ANALYSIS; PRECIPITATION (CHEMICAL); SODIUM; WASTEWATER RECLAMATION;

SYNTHESIS (CHEMICAL);

EID: 84876476063     PISSN: 08885885     EISSN: 15205045     Source Type: Journal    
DOI: 10.1021/ie302825b     Document Type: Article

References (47)

1. Zhang, M.; Zhang, B.; Li, X. H.; Yin, Z. L.; Guo, X. Y. Synthesis and Surface Properties of Submicron Barium Sulfate Particles Appl. Surf. Sci. 2011, 258, 24
2. Romero-Ibarra, I. C.; Manero, O. Hierarchically Nanostructured Barium Sulfate Fibers Langmuir 2010, 26, 6954
3. 4 Nano-powder by Polymeric Template Process and Its Characterisation Powder Technol. 2012, 224, 51
4. Cushing, B. L.; Kolesnichenko, V. L.; O'Connor, C. J. Recent Advances in the Liquid-Phase Syntheses of Inorganic Nanoparticles Chem. Rev. 2004, 104, 3893
5. Wong, D. C. Y.; Jaworski, Z.; Nienow, A. W. Effect of ion Excess on Particle Size and Morphology during Barium Sulphate Precipitation: An Experimental Study Chem. Eng. Sci. 2001, 56, 727
6. Ying, Y.; Chen, G. S.; Zhao, Y. C.; Li, S. L.; Yuan, Q. A High Throughput Methodology for Continuous Preparation of Monodispersed Nanocrystals in Microfluidic Reactors Chem. Eng. J. 2008, 135, 209
7. Schwarzer, H. C.; Peukert, W. Experimental Investigation into the Influence of Mixing on Nanoparticle Precipitation Chem. Eng. Technol. 2002, 25, 657
8. Schwarzer, H. C.; Peukert, W. Combined Experimental/Numerical Study on the Precipitation of Nanoparticles AIChE J. 2004, 50, 3234
9. Gradl, J.; Schwarzer, H. C.; Schwertfirm, F.; Manhart, M.; Peukert, W. Precipitation of Nanoparticles in a T-Mixer: Coupling the Particle Population Dynamics with Hydrodynamics through Direct Numerical Simulation Chem. Eng. Process. 2006, 45, 908
10. Kockmann, N.; Kastner, J.; Woias, P. Reactive Particle Precipitation in Liquid Microchannel Flow Chem. Eng. J. 2008, 135, S110
11. 4 Chem. Eng. Technol. 2011, 34, 1567
12. McCarthy, E. D.; Dunk, W. A. E.; Boodho, K. V. K. Application of an Intensified Narrow Channel Reactor to the Aqueous Phase Precipitation of Barium Sulfate J. Colloid Interface Sci. 2007, 305, 72
13. Kucher, M.; Babic, D.; Kind, M. Precipitation of Barium Sulfate: Experimental Investigation about the Influence of Supersaturation and Free Lattice Ion Ratio on Particle Formation Chem. Eng. Process. 2006, 45, 900
14. Jeevarathinam, D.; Gupta, A. K.; Pitchumani, B.; Mohan, R. Effect of Gas and Liquid Flowrates on the Size Distribution of Barium Sulfate Nanoparticles Precipitated in a Two Phase Flow Capillary Microreactor Chem. Eng. J. 2011, 173, 607
15. Su, Y. F.; Kim, H.; Kovenklioglu, S.; Lee, W. Y. Continuous Nanoparticle Production by Microfluidic-Based Emulsion, Mixing and Crystallization J. Solid State Chem. 2007, 180, 2625
16. Li, S. W.; Xu, J. H.; Wang, Y. J.; Luo, G. S. Controllable Preparation of Nanoparticles by Drops and Plugs Flow in a Microchannel Device Langmuir 2008, 24, 4194
17. Lv, Y. F.; Wu, X. J.; Wu, D. X.; Huo, D. X.; Zhao, S. C. Synthesis of Barium Fluoride Nanoparticles by Precipitation in Ethanol-Aqueous Mixed Solvents Powder Technol. 2007, 173, 174
18. Wang, Q. A.; Wang, J. X.; Chen, J. F. Large-Scale Preparation of Barium Sulfate Nanoparticles in a High-throughput Tube-in-Tube Microchannel Reactor Chem. Eng. J. 2009, 149, 473
19. Dreher, S.; Kockman, N.; Woias, P. Unsteady Laminar Flow Regimes and Mixing in T-Shaped Micromixers ASME Conf. Proc. 2007, 671, 30041
20. Kockmann, N.; Kiefer, T.; Engler, M.; Woias, P. Silicon Microstructures for High Throughput Mixing Devices Microfluid. Nanofluid. 2006, 2, 327
21. Hessel, V.; Löwe, H.; Müller, A.; Kolb, G. Chemical Micro Process Engineering; Wiley-VCH: New York, 2005; pp 132.
22. MicroChem (Dalian) Co. Ltd. Home Page. http://www.microchem.com.cn (accessed Nov 7, 2011).
23. Sun, P. Y; Sun, J.; Yao, J. F.; Zhang, L. X.; Xu, N. P. Continuous Production of Biodiesel from High Acid Value Oils in Microstructured Reactor by Acid-Catalyzed Reactions Chem. Eng. J. 2010, 162, 364
24. Yao, X. J.; Zeng, C. F.; Wang, C. Q.; Zhang, L. X. Two-Step Continuous Synthesis of Tetraethylthiuram Disulfide in Microstructured Reactors Korean J. Chem. Eng. 2011, 28, 723
25. Wilms, D.; Klos, J.; Kilbinger, A. F. M.; Löwe, H.; Frey, H. Ionic Liquids on Demand in Continuous Flow Org. Process Res. 2009, 13, 961
26. Pelleter, J.; Renaud, F. Facile, Fast and Safe Process Development of Nitration and Bromination Reactions Using Continuous Flow Reactors Org. Process Res. 2009, 13, 698
27. Tsunoyama, H.; Ichikuni, N.; Tsukuda, T. Microfluidic Synthesis and Catalytic Application of PVP-Stabilized ∼1 nm Gold Clusters Langmuir 2008, 24, 11327
28. Luty-Błocho, M.; Fitzner, K.; Hessel, V.; Löb, P.; Maskos, M.; Metzke, D.; Pacławski, K.; Wojnicki, M. Synthesis of Gold Nanoparticles in an Interdigital Micromixer Using Ascorbic Acid and Sodium Borohydride as Reducers Chem. Eng. J. 2011, 171, 279
29. 4(s) J. Chem. Educ. 1968, 45, 542
30. Hessel, V.; Kiesewalter, S. Process Technology of Tomorrow; IMM: Germany, 2004; pp 9.
31. James, G. S. Lange's Handbook of Chemistry, 16 th ed.; McGraw-Hill: New York, 2005; section 3, pp 18 and 52.
32. 4 Nano-particles Using Micro-emulsion Technique Adv. Appl. Sci. Res. 2010, 1, 197
33. Shen, Y.; Li, C.; Zhu, X.; Xie, A.; Qiu, L. Study on the Preparation and Formation Mechanism of Barium Sulfate Nanoparticles Modified by Different Organic Acids J. Chem. Sci. 2007, 119, 319
34. Kastner, J.; Kockmann, N.; Woias, P. Convective Mixing and Reactive Precipitation of Barium Sulfate in Microchannels Heat Transfer Eng. 2009, 30, 148
35. Schwarzer, H. C.; Peukert, W. Prediction of Aggregation Kinetics Based on Surface Properties of Nanoparticles Chem. Eng. Sci. 2005, 60, 11
36. He, S. L.; Oddo, J. E.; Tomson, M. B. The Nucleation Kinetics of Barium Sulfate in NaCl Solutions up to 6 m and 90 C J. Colloid Interface Sci. 1995, 174, 319
37. Erbacher, C.; Bessoth, F.; Busch, M.; Verpoorte, E.; Manz, A. Towards Integrated Continuous-Flow Chemical Reactors Microchim Acta. 1999, 131, 19
38. Zhang, Z.; Zhao, P.; Xiao, G.; Lin, M.; Cao, X. Focusing-Enhanced Mixing in Microfluidic Channels Biomicrofluidics 2008, 2, 014101
39. Ehrfeld, W.; Golbig, K.; Hessel, V.; Löwe, H.; Richter, T. Characterization of Mixing in Micromixers by a Test Reaction: Single Mixing Units and Mixer Arrays Ind. Eng. Chem. Res. 1999, 38, 1075
40. Trippa, G.; Jachuck, R. J. J. Process Intensification: Precipitation of Calcium Carbonate Using Narrow Channel Reactors Trans. IChemE. 2003, Part A, 81, 766
41. Vicum, L.; Mazzotti, M.; Baldyga, J. Applying a Thermodynamic Model to the Nonstochiometric Precipitation of Barium Sulfate Chem. Eng. Technol. 2003, 26, 325
42. Monnin, C. A. Thermodynamic Model for the Solubility of Barite and Celestite in Electrolyte Solutions and Seawater to 200 C and to 1 kbar Chem. Geol. 1999, 153, 187
43. Bromley, L. A. Thermodynamic Properties of Strong Electrolytes in Aqueous Solutions AIChE J. 1973, 19, 313
44. Jaworski, Z.; Nienow, A. CFD Modelling of Continuous Precipitation of Barium Sulphate in a Stirred Tank Chem. Eng. J. 2003, 91, 167
45. Öncül, A. A.; Sundmacher, K.; Seidel-Morgenstern, A.; Thévenin, D. Numerical and Analytical Investigation of Barium Sulphate Crystallization Chem. Eng. Sci. 2006, 61, 652
46. Aguiar, R.; Muhr, H.; Plasari, E.; Burty, M.; Rocabois, P. Comparative Study of the Influence of Homogeneous and Heterogeneous (Multi-phase) Precipitation Processes on the Particle Size Distribution Chem. Eng. Technol. 2003, 26, 292
47. Dehkordi, A. M.; Vafaeimanesh, A. Synthesis of Barium Sulfate Nanoparticles Using a Spinning Disk Reactor: Effects of Supersaturation, Disk Rotation Speed, Free Ion Ratio, and Disk Diameter Ind. Eng. Chem. Res. 2009, 48, 7574