Large-scale preparation of barium sulphate nanoparticles in a high-throughput tube-in-tube microchannel reactor

Chemical Engineering Journal

Volumn 149, Issue 1-3, 2009, Pages 473-478

  Wang, Qi An ^a   Wang, Jie Xin ^a   Li, Min ^a   Shao, Lei ^a   Chen, Jian Feng ^a   Gu, Lin ^b   An, Yong Tao ^b  

^a BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY   (China)

^b ADVANCED TECHNOLOGY AND MATERIALS CO LTD   (China)

Author keywords

Barium sulphate; High throughput; Large scale preparation; Micromixing; Tube in tube microchannel reactor

Indexed keywords

BARIUM; FLOW RATE; MICROCHANNELS; MICROPOROSITY; NANOPARTICLES; PARTICLE SIZE; THROUGHPUT;

BARIUM SULPHATE; HIGH THROUGHPUT; LARGE-SCALE PREPARATION; MICROMIXING; TUBE-IN-TUBE MICROCHANNEL REACTOR;

TUBES (COMPONENTS);

EID: 63149110016     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2009.02.018     Document Type: Article

References (25)

1. Panić S., Loebbecke S., Tuercke T., Antes J., and Bošković D. Experimental approaches to a better understanding of mixing performance of microfluidic devices. Chem. Eng. J. 101 (2004) 409-419
2. Löwe H., and Ehrfeld W. State-of-the-art in microreaction technology: concepts, manufacturing and applications. Electrochim. Acta. 44 (1999) 3679-3689
3. Jensen K.F. Microreaction engineering-is small better?. Chem. Eng. Sci. 56 (2001) 293-303
4. Jahnisch K., Hessel V., Löwe H., and Baerns M. Chemistry in microstructured reactors. Angew. Chem. Int. Ed. 43 (2004) 406-446
5. Cushing B.L., Kolesnichenko V.L., and O'Connor C.J. Recent advances in the liquid-phase syntheses of inorganic nanoparticles. Chem. Rev. 104 (2004) 3893-3946
6. deMello J., and deMello A. Microscale reactors: nanoscale products. Lab. Chip 4 (2004) 11N-15N
7. Yen B.K.H., Stott N.E., Jensen K.F., and Bawendi M.G. A continuous-flow microcapillary reactor for the preparation of a size series of CdSe nanocrystals. Adv. Mater. 15 (2003) 1858-1862
8. Chan E.M., Mathies R.A., and Alivisatos A.P. Size-controlled growth of CdSe nanocrystals in microfluidic reactors. Nano Lett. 3 (2003) 199-201
9. Edel J.B., Fortt R., deMello J.C., and deMello A.J. Microfluidic routes to the controlled production of nanoparticles. Chem. Commun. 2 (2002) 1136-1137
10. Lin X.Z., Terepka A.D., and Yang H. Synthesis of silver nanoparticles in a continuous flow tubular microreactor. Nano Lett. 4 (2004) 2227-2232
11. Wagner J., Kirner T., Mayer G., Albert J., and Köhler J.M. Generation of metal nanoparticles in a microchannel reactor. Chem. Eng. J. 101 (2004) 251-260
12. Khan S.A., l Gunther A., Schmidt M.A., and Jensen K.F. Microfluidic synthesis of colloidal silica. Langmuir 20 (2004) 8604-8611
13. Ju J.X., Zeng C.F., Zhang L.X., and Xu N.P. Continuous synthesis of zeolite NaA in a microchannel reactor. Chem. Eng. J. 116 (2006) 115-121
14. Kawaguchi T., Miyata H., Ataka K., Mae K., and Yoshida J. Room-temperature swern oxidations by using a microscale flow system. Angew. Chem. Int. Ed. 44 (2005) 2413-2416
15. Ying Y., Chen G.W., Zhao Y.C., Li S.L., and Yuan Q. A high throughput methodology for continuous preparation of monodispersed nanocrystals in microfluidic reactors. Chem. Eng. J. 135 (2008) 209-215
16. Okamoto H., Ushijima T., and Kitoh O. New methods for increasing productivity by using microreactors of planar pumping and alternating pumping types. Chem. Eng. J. 101 (2004) 57-63
17. Chen G.G., Luo G.S., Li S.W., Xu J.H., and Wang J.D. Experimental approaches for understanding mixing performance of a minireactor. AIChE. J. 51 (2005) 2923-2929
18. McCarthy E.D., Dunk W.A.E., and Boodhoo K.V.K. Application of an intensified narrow channel reactor to the aqueous phase precipitation of barium sulphate. J. Colloid Interf. Sci. 305 (2007) 72-87
19. Aoun M., Plasari E., David R., and Villermaux J. Are barium sulphate kinetics sufficiently known for testing precipitation reactor models?. Chem. Eng. Sci. 51 (1996) 2449-2458
20. Barresi A.A., Marchisio D., and Baldi G. On the role of micro- and mesomixing in a continuous Couette-type precipitator. Chem. Eng. Sci. 54 (1999) 2339-2349
21. Baldyga J., and Wojciech O. Barium sulphate precipitation in a pipe-an experimental study and CFD modeling. Chem. Eng. Sci. 56 (2001) 2435-2444
22. Pohorecki R., and Baldyga J. The use of a new model of micromixing for determination of crystal size in precipitation. Chem. Eng. Sci. 38 (1985) 79-83
23. Judat B., Racina A., and Kind M. Macro- and micromixing in a Taylor-Couette reactor with axial flow and their influence on the precipitation of barium sulphate. Chem. Eng. Technol. 27 (2004) 287-292
24. Trippa G., and Jachuck R.J.J. Precipitation of calcium carbonate using narrow channel reactors. Trans. IChemE A 81 (2003) 766-772
25. Kucher M., Babic D., and Kind M. Precipitation of barium sulphate: experimental investigation about the influence of supersaturation and free lattice ion ratio on particle formation. Chem. Eng. Proc. 4 (2006) 900-907