Analysis of 136 pesticides in avocado using a modified QuEChERS method with LC-MS/MS and GC-MS/MS

Journal of Agricultural and Food Chemistry

Volumn 61, Issue 10, 2013, Pages 2315-2329

  Chamkasem, Narong ^a   Ollis, Lisa W ^a   Harmon, Tiffany ^a   Lee, Sookwang ^a   Mercer, Greg ^a  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

Author keywords

avocado; gas chromatography; liquid chromatography; pesticide residue analysis; QuEChERS; tandem mass spectrometry; triple quadrupole

Indexed keywords

AVOCADO; PESTICIDE RESIDUE ANALYSIS; QUECHERS; TANDEM MASS SPECTROMETRY; TRIPLE QUADRUPOLE;

EXTRACTION; FRUITS; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; RECOVERY;

PESTICIDES;

PESTICIDE RESIDUE;

CHEMICAL STRUCTURE; CHEMISTRY; CONFERENCE PAPER; EVALUATION STUDY; FOOD CONTAMINATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOLATION AND PURIFICATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; PERSEA; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MOLECULAR STRUCTURE; PERSEA; PESTICIDE RESIDUES; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 84874966943     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf304191c     Document Type: Conference Paper

References (21)

1. Anastassiades, M.; Lehotay, S. J.; Stajnbaher, D.; Schenck, F. J. Fast and easy multiresidue method employing MeCN extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce J. AOAC Int. 2003, 86, 412-431
2. Pesticide residues in foods by MeCN extraction and partitioning with magnesium sulfate. Official Methods of Analysis of AOAC International; AOAC International: Gaithersburg, MD, 2007; Method 2007.1.
3. U.S. Food and Drug Administration. Pesticide Analytical Manual Vol. I, Multiresidue Methods, 3 rd ed.; U.S. Department of Health and Human Services: Washington, DC, 1994
4. Fernandez Moreno, J. L.; Arrebola Lieanas, F. J.; Garrido Frenich, A.; Martinez Vidal, J. L. Evaluation of different sample treatments for determining pesticide residues in fat vegetable matrices like avocado by low-pressure gas chromatography-tandem mass spectrometry J. Chromatogr., A 2006, 1111, 97-105
5. Li, L.; Xu, Y.; Pan, C.; Zhou, Z.; Jiang, S.; Liu, F. Simplified pesticide multiresidue analysis of soybean oil by low-temperature cleanup and dispersive solid-phase extraction coupled with gas chromatography/mass spectrometry J. AOAC Int. 2007, 90 (5) 1387-1393
6. Ferrer, C.; Gómez, M. J.; García-Reyes, J. F.; Ferrer, I. Determination of pesticide residues in olives and olive oil by matrix solid-phase dispersion followed by gas chromatography/mass spectrometry and liquid chromatography/tandem mass spectrometry J. Chromatogr., A 2005, 1069, 183-194
7. Tsoutsi, C.; Konstantinou, C. I.; Hela, D.; Albanis, T. Screening method for organophosphorus insecticides and their metabolites in olive oil samples based on headspace solid-phase microextraction coupled with gas chromatography Anal. Chim. Acta 2006, 573, 216-222
8. Hopper, M. L. Automated one-step supercritical fluid extraction and clean-up system for the analysis of pesticide residues in fatty matrices J. Chromatogr., A 1999, 840, 93-105
9. Lin, Y. Laboratory Information Bulletin 4472, Analysis of Twenty Six Pesticide Residues in Fatty Food Products Using a Modified QuEChERS Method and LC-MS/MS; U.S. Food and Drug Administration, Division of Field Science: Rockville, MD, 2011.
10. Lin, Y.; Chamkasem, N.; Zhang, K.; Wong, J. Inter-laboratory validation of a modified QuEChERS and LC-MS/MS method for analysis of about 250 pesticide residues in six fatty food products. Proceedings of the 58th ASMS Conference on Mass Spectrometry and Allied Topics, Salt Lake City, UT, May 23-27; ASMS: Santa Fe, NM, 2010.
11. Lehotay, S. J.; Mastovska, K.; Yun, S. J. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes J. AOAC Int. 2005, 88 (2) 630-638
12. Koesukwiwat, U.; Lehotay, S. J.; Maštovská, K.; Dorweiler, K. J.; Leepipatpiboon, N. Extension of the QuEChERS method for pesticide residues in cereals to flaxseeds, peanuts, and doughs J. Agric. Food Chem. 2010, 58, 5950-5958
13. EC Council Directive 2002/657/EC of 12 August, 1990 on implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off. J. Eur. Communities 2002, L221, 8.
14. Chamkasem, N.; Harmon, T.; Mitchell, T.; Stromgren, S.; Lin, Y.; Wong, J. Laboratory Information Bulletin 4463, A Rapid LC/MS Method for Determination of Teflubenzuron in Salmon Tissue; U.S. Food and Drug Administration, Division of Field Science: Rockville, MD, 2010
15. Lehotay, S.; Maštovská, K.; Yun, S. J. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes J. AOAC Int. 2005, 88 (2) 615-629
16. Schenck, F.; Wong, J.; Lu, C.; Li, J.; Holdcomb, J. R.; Mitchell, L. M. Multiresidue analysis of 102 organophosphorus pesticides in produce at parts-per-billion levels using a modified QuEChERS method and gas chromatography with pulsed flame photometric detection J. AOAC Int. 2009, 92 (2) 561-573
17. Veneziano, A.; Vacca, G.; Arana, S.; De Simone, F.; Rastrelli, L. Determination of carbendazim, thiabendazole, and thiophanate-methyl in banana (Musa acuminata) samples imported to Italy Food Chem. 2003, 87 (3) 383-386
18. Okihashi, M.; Takatori, S.; Kitagawa, Y.; Tanaka, Y. Simultaneous analysis of 260 pesticide residues in agricultural products by gas chromatography/triple quadrupole mass spectrometry J. AOAC Int. 2007, 90 (4) 1165-1179
19. Wong, J.; Zhang, K.; Tech, K.; Hayward, D. G.; Makovi, C. M.; Krynistky, A. J.; Schenck, F. J.; Banerjee, K.; Dasgupta, S.; Brown, D. Multiresidue pesticide analysis in fresh produce by capillary gas chromatography-mass spectrometry/selective ion monitoring (GC-MS/SIM) and -tandem mass spectrometry (GC-MS/MS) J. Agric. Food Chem. 2010, 58, 5868-5883
20. Korta, E.; Bakkali; Berrueta, L. A.; Gallo, G.; Vicente, F.; Kilchenmann, V.; Bogdanov, S. Study of acaricide stability in honey. Characterization of amitraz degradation products in honey and beeswax J. Agric. Food Chem. 2001, 49, 5835-5842
21. Zrostlíková, J.; Hajšlová, J.; Godula, M.; Maštovská, K. Performance of programmed temperature vaporizer, pulsed splitless and on-column injection techniques in analysis of pesticide residues in plant matrices J. Chromatogr., A 2001, 1937, 73-86