Design and operation of a fluidized bed hydrator for steam reactivation of calcium sorbent

Industrial and Engineering Chemistry Research

Volumn 52, Issue 8, 2013, Pages 2793-2802

  Wang, Alan ^a   Wang, Dawei ^a   Deshpande, Niranjani ^a   Phalak, Nihar ^a   Wang, William ^a   Fan, L S ^a  

^a The Ohio State University   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CALCIUM; CARBON DIOXIDE; CHEMICAL REACTORS; HEAT PUMP SYSTEMS; HIGH TEMPERATURE APPLICATIONS; HYDRATION; SORBENTS; SORPTION; STEAM;

CALCIUM SORBENTS; CHEMICAL HEAT PUMPS; DESIGN AND OPERATIONS; FLUIDIZED BED REACTORS; HIGH TEMPERATURE; PROCESS HEAT INTEGRATION; REACTION PARAMETERS; THERMO-GRAVIMETRIC;

FLUIDIZED BEDS;

EID: 84874631626     PISSN: 08885885     EISSN: 15205045     Source Type: Journal    
DOI: 10.1021/ie302611z     Document Type: Article

References (74)

1. 2 Emissions: A Review of Technologies; EPA/600/R-00/093; U.S. EPA: Research Triangle Park, NC, 2000. Available at http://cfpub.epa.gov/si/si-public-file-download.cfm?p-download-id= 438450 (accessed 08/12/12).
2. 3 Mitigation; BR-1781; The Babcock & Wilcox Company: Barberton, OH, 2006. Available at http://www.babcock.com/library/pdf/ br-1781.pdf (accessed 01/22/13).
3. Karma, V. K. and Jain, A. K. Emissions of Sulfuric, Hydrochloric, and Hydrofluoric Acid from Combination Boilers. Proceedings of the TAPPI Environmental Conference, 2002.
4. IEA, (2011. International Energy Agency. Key World Energy Statistics 2011. Available at http://www.iea.org/textbase/nppdf/free/2011/key-world-energy- stats.pdf (accessed 01/22/13).
5. 2 Emissions from Fuel Combustion 2011.
6. National Academies Press, Committee on Energy Futures and Air Pollution in Urban China and the United States. Energy Futures and Urban Air Pollution: Challenges for China and the United States; Washington, DC, 2007. Available at http://www.nap.edu/catalog/12001.html (accessed 08/13/12).
7. Katzer, J., Ansolabehere, S., Beer, J., Deutch, J., Ellerman, A. D., Friedmann, S. J., Herzog, H., Jacoby, H. D., Joskow, P. L., McRae, G., Lester, R., Moniz, E. J., and Steinfeld, E. The Future of Coal-Options for a Carbon-Constrained World; Massachusetts Institute of Technology: Cambridge, MA, 2007.
8. Moniz, E. J., Jacoby, H. D., and Meggs, A. J. M.; The Future of Natural Gas; Massachusetts Institute of Technology: Cambridge, MA, 2011.
9. U.S. Energy Information Administration. International Energy Outlook 2011; DOE/EIA-0484(2011); U.S. Energy Information Administration: Washington, DC, 2011. Available at http://www.eia.gov/forecasts/ieo/pdf/0484%282011%29.pdf (accessed 01/22/13).
10. Fan, L.-S. Chemical Looping Systems for Fossil Energy Conversions; John Wiley & Sons: Hoboken, NJ, 2010.
11. Fan, L.-S.; Li, F. Chemical Looping Technology and Its Fossil Energy Conversion Applications Ind. Eng. Chem. Res. 2010) 49, 10200-10211
12. 2 Acceptor Gasification Process-Studies of Acceptor Properties Adv. Chem. Ser. 1967, 69, 141-165
13. Balasubramanian, B.; Lopez Ortiz, A.; Kaytakoglu, S.; Harrison, D. P. Hydrogen from Methane in a Single Step Process Chem. Eng. Sci. 1999, 54, 3543-3552
14. Ziock, H.-J.; Lackner, K. S.; Harrison, D. P. Zero Emission Coal Power, a New Concept. Available at www.netl.doe.gov/publications/proceedings/01/carbon- seq/2b2.pdf (accessed 01/22/13).
15. 2-Acceptor Chem. Eng. Sci. 2006, 61, 1195-1202
16. Barelli, L.; Bidini, G.; Gallorini, F.; Servili, S. Hydrogen Production through Sorption-Enhanced Steam Methane Reforming and Membrane Technology: A Review Energy 2008, 33, 554-570
17. Ramkumar, S.; Fan, L.-S. Calcium Looping Process (CLP) for Enhanced Non-catalytic Hydrogen Production with Integrated Carbon Dioxide and Sulfur Capture Energy Fuels 2010, 24, 4408-4418
18. Ramkumar, S.; Phalak, N.; Fan, L.-S. Calcium Looping Process (CLP) for Enhanced Steam Methane Reforming Ind. Eng. Chem. Res. 2012, 51, 1186-1192
19. Phalak, N.; Ramkumar, S.; Deshpande, N.; Wang, A.; Wang, W.; Statnick, R.; Fan, L.-S. Calcium Looping Process (CLP) for Clean Coal Conversion: Design and Operation of the Sub-Pilot Scale Carbonator Ind. Eng. Chem. Res. 2012, 51, 9938-9944
20. Connell, D. P.; Lewandowski, D.; Ramkumar, S.; Phalak, N.; Statnick, R.; Fan, L.-S. Process Simulation and Economic Analysis of the Calcium Looping Process (CLP) for Hydrogen and Electricity Production from Coal and Natural Gas. Fuel In press. Available at http://dx.doi.org/10.1016/j.fuel.2012.07.006 (accessed 01/22/13).
21. 2 Using a Carbonation/Calcination Cycle of CaO/CaCO3 Chem. Eng. J. 2002, 90, 303-306
22. 3 Looping at Pilot Scale Chem. Eng. Technol. 2009, 32, 425-434
23. 2 Capture System Using CaO Chem. Eng. J. 2009, 147, 252-258
24. 2 Capture Cycle and Coal-Fired Power Plants. A Comparative Study for Different Sorbents Energy Fuels 2010, 24, 728-736
25. 2 Capture in Existing Power Plants AIChE J. 2011, 57, 2599-2607
26. t Calcium Looping Pilot in La Pereda. 2nd International Workshop on OXYCFB. Stuttgart, Germany, June 2012. Available at http://www.caoling.eu/documentos/ 2ndInternationalWorkshoponOXYCFBStuttgartCaOlingProjectFirstexperiencesonthe17M WtcalciumloopingpilotinLaPereda.pdf (accessed 01/22/13).
27. 2 Capture Prog. Energy Combust. Sci. 2010, 36, 260-279
28. 2 Capture-A Review Energy Fuels 2012, 26, 2751-2767
29. 2 Separation from Flue Gas Using Calcium Based Sorbents. Masters Thesis, The Ohio State University, Columbus, OH, 2007.
30. 2 Carrying Capacity of CaO in Isothermal Recarbonation-Decomposition Cycles Ind. Eng. Chem. Res. 2007, 46, 4633-4638
31. Yu, F.-C.; Phalak, N.; Sun, Z.; Fan, L.-S. Activation Strategies for Calcium-Based Sorbents for CO2 Capture Ind. Eng. Chem. Res. 2012, 51, 2133-2142
32. 2 Capture of Limestone Modified by Hydration-Dehydration Technology for Carbonation/Calcination Looping Chem. Eng. J. 2011, 173, 158-163
33. 2 Capture and Carbonaceous Fuel Conversion-Prospect and Opportunity Energy Environ. Sci. 2012, 5, 7254-7280
34. Gupta, H.; Fan, L.-S. Carbonation-Calcination Cycle Using High Reactivity Calcium Oxide for Carbon Dioxide Separation from Flue Gas Ind. Eng. Chem. Res. 2002, 41, 4035-4042
35. Iyer, M. V.; Gupta, H.; Sakadjian, B.; Fan, L.-S. Multicyclic Study on the Simultaneous Carbonation and Sulfation of High-Reactivity CaO Ind. Eng. Chem. Res. 2004, 43, 3939-3947
36. 2 Capture Facility using Solid Sorbents. Proceedings of the Twenty-fifth International Pittsburgh Coal Conference, September 2008, Pittsburgh, PA, USA.
37. st Meeting of the High Temperature Solid Looping Cycles Network, September 2009, Oveido, Spain.
38. 2 and Sulfur Capture from Coal-Fired Power Plants Ind. Eng. Chem. Res. 2010, 49, 5094-5101
39. 2 Capture from Coal Fired Power Plants. Presented at The 10th Annual Carbon Capture and Sequestration Conference, May 2011, Pittsburgh, PA.
40. 2 and Sulfur Removal Using Carbonation-Calcination Reaction (CCR) Process: Results from Computer Simulations and Experiments. Presented at The 2011 AIChE Annual Meeting, October 2011, Minneapolis, MN, USA.
41. Arias, B.; Grasa, G. S.; Abanades, J. C. Effect of Sorbent Hydration on the Average Activity of CaO in a Ca-Looping System Chem. Eng J. 2010, 163, 324-330
42. Wang, W.; Ramkumar, S.; Wong, D.; Fan, L.-S. Simulations and Process Analysis of the Carbonation-Calcination Reaction Process with Intermediate Hydration Fuel 2012, 92, 94-106
43. 2 Capture for the Carbonation-Calcination Reaction (CCR) Process: Parametric Effects and Comparisons with Alternative Processes. Fuel In press. Available at http://dx.doi.org/10.1016/j.fuel.2012.04.043 (accessed 01/22/13).
44. 2 in a Fluidized Bed Combustor Ind. Eng. Chem. Res. 2004, 43, 5529-5539
45. 2 Capture Cycles Environ. Sci. Technol. 2007, 41, 1420-1425
46. 2 Capture Int. J. Greenhouse Gas Control. 2008, 2, 203-209
47. 2 Carrying Capacity of Reactivated CaO by Hydration Energy Fuels 2011, 25, 1294-1301
48. 2 Ind. Eng. Chem. Res. 2011, 50, 5927-5932
49. Sun, Z.; Chi, H.; Fan, L.-S. Physical and Chemical Mechanism for Increased Surface Area and Pore Volume of CaO in Water Hydration Ind. Eng. Chem. Res. 2012, 51, 10793-10799
50. Phalak, N.; Deshpande, N.; Fan, L.-S. Investigation of High-Temperature Steam Hydration of Naturally Derived Calcium Oxide for Improved Carbon Dioxide Capture Capacity over Multiple Cycles Energy Fuels 2012, 26, 3903-3909
51. 2 Chemical Heat Pump System Energy Convers. Manage. 2002, 43, 947-960
52. 2 Chemical Heat Pump Systems Exergy, an International Journal 2002, 2, 6-14
53. 2 Reaction Chem. Eng. J. 2002, 86, 3-10
54. Schaube, F.; Wörner, A.; Tamme, R. High Temperature Thermochemical Heat Storage for Concentrated Solar Power Using Gas-Solid Reactions J. Solar Eng. 2011, 133, 031006-1-031006-7
55. 2O Partial Pressures for Thermo-Chemical Heat Storage Thermochim. Acta 2012, 538, 9-20
56. th ed.; Kogel, J. E.; Trivedi, N. C.; Barker, J. M.; Krukowski, S. T., Eds.; Society for Mining, Metallurgy, and Exploration: Littleton, 2006; Part 2-Lime.
57. Corson, B. L. Dry Lime Hydrate and Process for Producing Same. U.S. Patent 2,309,168, 1943.
58. Corson, B. L. Methods of Conditioning and Treating Lime and Product Thereof. U.S. Patent 2,409,546, 1946.
59. Corson, B. L. Process for Producing Dry Lime Hydrate. U.S. Patent 3,106,453, 1963.
60. Wajer, M. T.; Witkowski, J. T.; Smith, D. M. Stabilized Pressure-Hydrated Magnesium Hydroxide Slurry from Burnt Magnesite and Process for Its Production. U.S. Patent Re. 36,369-Reissue of U.S. Patent 5,487,879, 1999.
61. Hansen, J. P.; Jensen, L. S. Method and Apparatus for Hydration of a Particulate or Pulverent Material Containing CaO, Hydrated Product, and Use of Hydrated Product. U.S. Patent 7,595,037 B2, 2009.
62. Herrera, C. A.; Levy, E. K. Bubbling Characteristics of Sound-Assisted Fluidized Beds Powder Technol. 2001, 119, 229-240
63. Xu, C.; Zhu, J. Parametric Study of Fine Particle Fluidization under Vibration Powder Technol. 2006, 161, 135-144
64. Wang, Z.; Kwauk, M.; Li, H. Fluidization of Fine Particles Chem. Eng. Sci. 1998, 53, 377-395
65. Dave, R.; Wu, C.; Chaudhuri, B.; Watano, S. Magnetically Mediated Flow Enhancement for Controlled Powder Discharge of Cohesive Powders Powder Technol. 2000, 112, 111-125
66. Qian, G.; Bagyi, I.; Burdick, I. W.; Pfeffer, R.; Shaw, H. Gas-Solid Fluidization in a Centrifugal Field AIChE J. 2001, 47, 1022-1034
67. Alavi, S.; Caussat, B. Experimental Study on Fluidization of Micronic Powders Powder Technol. 2005, 157, 114-120
68. Nezzal, A.; Release, J. F.; Guigon, P. Fluidization Behavior of Very Cohesive Powders Under Mechanical Agitation. Proceedings of the Eighth Engineering Foundation Conference on Fluidization, Tours, France, 1995, May 14-19.
69. Kunii, D.; Levenspiel, O. Bubbling Bed Model- Model for Flow of Gas through a Fluidized Bed Ind. Sci. Eng. Chem. Fund. 1968, 3, 446
70. Lin, S.; Harada, M.; Suzuki, Y.; Hatano, H. CaO Hydration Rate at High Temperature (1023 K) Energy Fuels 2006, 20, 903-908
71. Shearer, J. A.; Smith, G. W.; Moulton, D. S.; Smyk, E. B.; Myles, K. M.; Swift, W. M.; Johnson, I. Hydration Process for Reactivating Spent Limestone and Dolomite Sorbent for Reuse in Fluidized-Bed Coal Combustion. Proceedings of the Sixth International Conference on Fluidized Bed Combustion. 1980, April 9-11
72. 2 Reversible Thermochemical Reaction for Thermal Energy Storage by Means of Chemical Reaction Kagaku Kogaku Ronbunshu 1985, 11, 542-548
73. Serris, E.; Favergeon, L.; Pijolat, M.; Soustelle, M.; Nortier, P.; Gaertner, R. S.; Chopin, T.; Habib, Z. Study of the Hydration of CaO Powder by Gas-Solid Reaction Cem. Concr. Res. 2011, 41, 1078-1084
74. HSC Chemistry, version 5.0; Outotec Research Oy: Pori, Finland, 2008.