A multi-residue method for the determination of 124 pesticides in rice by modified QuEChERS extraction and gas chromatography-tandem mass spectrometry

Food Chemistry

Volumn 138, Issue 2-3, 2013, Pages 1198-1205

  Hou, Xue ^a,b,c   Han, Mei ^a   Dai, Xiaohang ^a   Yang, Xiaofeng ^a   Yi, Shengguo ^a  

^a CROP RESEARCH INSTITUTE   (China)

^b CHENGDU INSTITUTE OF ORGANIC CHEMISTRY   (China)

^c UNIVERSITY OF CHINESE ACADEMY OF SCIENCES   (China)

Author keywords

GC MS MS; Multi residue analysis; Pesticides; QuEChERS method; Rice; Validation

Indexed keywords

GC-MS/MS; MULTI-RESIDUE ANALYSIS; QUECHERS; RICE; VALIDATION;

ACETONITRILE; GAS CHROMATOGRAPHY; MASS SPECTROMETRY;

PESTICIDES;

ACETONITRILE; PESTICIDE; PESTICIDE RESIDUE;

ANALYTIC METHOD; ARTICLE; CHEMICAL ANALYSIS; DISPERSION; FOOD QUALITY; GAS CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; QUERCHER METHOD; RICE; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; ORYZA SATIVA; PESTICIDE RESIDUES; SOLID PHASE EXTRACTION;

EID: 84873709931     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.11.089     Document Type: Article

References (17)

1. M. Anastassiades, S.J. Lehotay, D. Štajnbaher, and F.J. Schenck Fast and easy multi-residue method employing acetonitirile extraction/ partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce Journal of AOAC International 86 2003 412 431
2. M. Anastassiades, E. Scherbaum, B. Taşdelen, and D. Štajnbaher Recent developments in QuEChERS methodology for pesticide multiresidue analysis Pesticide chemistry: Crop protection, public health, environmental safety 2007 WILEY-VCH Verlag GmbH & Co. KGaA Weinheim 439
3. C. Díez, W.A. Traag, P. Zommer, P. Marinero, and J. Atienza Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for the extraction of herbicide residues in barley samples Journal of Chromatography A 1131 2006 11 20
4. European Commission Commission Decision 2002/657/EC, Implementing council directive 96/23/EC concerning the performance of analytical methods and the interpretation of results Official Journal of the European Communities 221 2002 8 36
5. European Commission Regulation (EC) No. 299/2008 of the European parliament and of the council of 11 March 2008 on maximum residue levels of pesticides in or on food and feed of plant and animal origin Official Journal of the European Communities 9 2008 67
6. J. Fenik, M. Tankiewicz, and M. Biziuk Properties and determination of pesticides in fruits and vegetables Trends in Analytical Chemistry 30 2011 814 825
7. A. Ferrero, and A. Tinarelli Pesticide risk assessment in rice paddies: Theory and practice 2008 Elsevier Amsterdam
8. U. Koesukwiwat, K. Sanguankaew, and N. Leepipatpiboon Rapid determination of phenoxy acid residues in rice by modified QuEChERS extraction and liquid chromatography-tandem mass spectrometry Analytica Chimica Acta 626 2008 10 20
9. D.A. Lambropoulou, and T.A. ALbanis Development of an analytical procedure for the determination of emerging and priority organic pollutants in leafy vegetables by pressurized solvent extraction followed by GC-MS determination Analytical and Bioanalytical Chemistry 389 2007 1663 1683
10. S.J. Lehotay, A. de Kok, M. Hiemstra, and P. Van Bodegraven Validation of a fast and easy method for the determination of 229 pesticide residues in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection Journal of AOAC International 88 2005 595 614
11. S.J. Lehotay, K. Mastovská, and S.J. Yun Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes Journal of AOAC International 86 2005 630 638
12. P.Y. Liu, Q.X. Liu, Y.S. Ma, J.W. Liu, and X. Jia Analysis of pesticide multiresidues in rice by gas chromatography-mass spectrometry coupled with solid phase extraction Electrochimica Acta 24 2006 228 234
13. K. Mastovska, K.J. Dorweiler, S.J. Lehotay, J.S. Wegscheid, and K.A. Szpylka Pesticide multiresidue analysis in cereal grains using modified QuEChERS method combined with automated direct sample introduction GC-TOFMS and UPLC-MS/MS techniques Journal of Agricultural and Food Chemistry 58 2010 5959 5972
14. L. Pareja, A.R. Fernández-Alba, V. Cesio, and H. Heinzen Analytical methods for pesticide residues in rice Trends in Analytical Chemistry 30 2011 270 291
15. SANCO/10684/2009 (2010). Method validation and quality control procedures for pesticide residues analysis in food and feed. Commission of the European Communities, 8, 18.
16. A. Wilkowska, and M. Biziuk Determination of pesticide residues in food matrices using the QuEChERS methodology Food Chemistry 125 2011 803 812
17. W.G. Zhang, X.G. Chu, H.X. Cai, J. An, and C.J. Li Simultaneous determination of 109 pesticides in unpolished rice by a combination of gel permeation chromatography and florisil column purification, and gas chromatography/mass spectrometry Rapid Communications in Mass Spectrometry 20 2006 609 617