메뉴 건너뛰기




Volumn 363, Issue 1, 2013, Pages 50-56

Network connectivity in cesium borosilicate glasses: 17O multiple-quantum MAS and double-resonance NMR

Author keywords

Cesium borosilicate glass; MQMAS; Oxygen 17 NMR; Phase separation; REDOR

Indexed keywords

ALKALI BOROSILICATE GLASS; BRIDGING OXYGEN; CESIUM BOROSILICATE GLASS; COMPOSITIONAL VARIATION; HIGH TEMPERATURE; MAS NMR; MODEL-BASED OPC; MQMAS; NETWORK CONNECTIVITY; OXYGEN-17 NMR; RANDOM NETWORK; REDOR; ROTATIONAL ECHO DOUBLE RESONANCE; SHORT RANGE ORDERS; SOLID STATE NMR;

EID: 84872319694     PISSN: 00223093     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jnoncrysol.2012.12.010     Document Type: Article
Times cited : (31)

References (67)
  • 5
    • 0037213485 scopus 로고    scopus 로고
    • Solid-state NMR study of metastable immiscibility in alkali borosilicate glasses
    • DOI 10.1016/S0022-3093(02)01604-6, PII S0022309302016046
    • L.-S. Du, and J.F. Stebbins Solid-state NMR study of metastable immiscibility in alkali borosilicate glasses J. Non-Cryst. Solids 315 2003 239 255 (Pubitemid 35465893)
    • (2003) Journal of Non-Crystalline Solids , vol.315 , Issue.3 , pp. 239-255
    • Du, L.-S.1    Stebbins, J.F.2
  • 8
    • 0031272134 scopus 로고    scopus 로고
    • The immobilization of high level radioactive wastes using ceramics and glasses
    • I.W. Donald, B.L. Metcalfe, and R.N.J. Taylor The immobilization of high level radioactive wastes using ceramics and glasses J. Mater. Sci. 32 1997 5851 5887 (Pubitemid 127504152)
    • (1997) Journal of Materials Science , vol.32 , Issue.22 , pp. 5851-5887
    • Donald, I.W.1    Metcalfe, B.L.2    Taylor, R.N.J.3
  • 9
    • 0000977152 scopus 로고    scopus 로고
    • NMR and NQR studies of boron in vitreous and crystalline borates
    • P.J. Bray NMR and NQR studies of boron in vitreous and crystalline borates Inorg. Chim. Acta 289 1999 158 173
    • (1999) Inorg. Chim. Acta , vol.289 , pp. 158-173
    • Bray, P.J.1
  • 10
    • 0041179242 scopus 로고    scopus 로고
    • NMR and NQR studies on borate glasses
    • P.J. Bray, and G.L. Peterson NMR and NQR studies on borate glasses Z. Naturforsch. 53a 1998 273 284
    • (1998) Z. Naturforsch. , vol.53 A , pp. 273-284
    • Bray, P.J.1    Peterson, G.L.2
  • 12
    • 31944450059 scopus 로고
    • Nuclear magnetic resonance absorption in glass. I. Nuclear quadrupole effects in boron oxide, soda-boric oxide, and borosilicate glasses
    • A.H. Silver, and P.J. Bray Nuclear magnetic resonance absorption in glass. I. Nuclear quadrupole effects in boron oxide, soda-boric oxide, and borosilicate glasses J. Chem. Phys. 29 1958 984 990
    • (1958) J. Chem. Phys. , vol.29 , pp. 984-990
    • Silver, A.H.1    Bray, P.J.2
  • 13
    • 33745315198 scopus 로고
    • Nuclear magnetic resonance spectra from a crystal rotated at high speed
    • E.R. Andrew, A. Bradbury, and R.G. Eades Nuclear magnetic resonance spectra from a crystal rotated at high speed Nature 183 1958
    • (1958) Nature , vol.183
    • Andrew, E.R.1    Bradbury, A.2    Eades, R.G.3
  • 14
    • 36149028286 scopus 로고
    • Free induction decays of rotating solids
    • I.J. Lowe Free induction decays of rotating solids Phys. Rev. Lett. 2 1959 285 287
    • (1959) Phys. Rev. Lett. , vol.2 , pp. 285-287
    • Lowe, I.J.1
  • 15
    • 0001421829 scopus 로고
    • Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR
    • L. Frydman, and J.S. Harwood Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR J. Am. Chem. Soc. 117 1995 5367 5368
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367-5368
    • Frydman, L.1    Harwood, J.S.2
  • 16
    • 0000769739 scopus 로고
    • Multiple-quantum magic-angle spinning NMR: A new method for the study of quadrupolar nuclei in solids
    • A. Medek, J.S. Harwood, and L. Frydman Multiple-quantum magic-angle spinning NMR: a new method for the study of quadrupolar nuclei in solids J. Am. Chem. Soc. 117 1995 12779 12787 (Pubitemid 126635370)
    • (1995) Journal of the American Chemical Society , vol.117 , Issue.51 , pp. 12779-12787
    • Medek, A.1    Harwood, J.S.2    Frydman, L.3
  • 17
    • 0035501048 scopus 로고    scopus 로고
    • Enhanced resolution and quantitation from 'ultrahigh' field NMR spectroscopy of glasses
    • DOI 10.1016/S0022-3093(01)00693-7, PII S0022309301006937
    • S. Kroeker, P.S. Neuhoff, and J.F. Stebbins Enhanced resolution and quantitation from 'ultrahigh' field NMR spectroscopy of glasses J. Non-Cryst. Solids 293-295 2001 440 445 (Pubitemid 32997875)
    • (2001) Journal of Non-Crystalline Solids , vol.293-295 , Issue.1 , pp. 440-445
    • Kroeker, S.1    Neuhoff, P.S.2    Stebbins, J.F.3
  • 19
    • 0037157160 scopus 로고    scopus 로고
    • Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields
    • DOI 10.1021/ja025849p
    • Z. Gan, P. Gor'kov, T.A. Cross, A. Samoson, and D. Massiot Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields J. Am. Chem. Soc. 124 2002 5634 5635 (Pubitemid 34533491)
    • (2002) Journal of the American Chemical Society , vol.124 , Issue.20 , pp. 5634-5635
    • Gan, Z.1    Gor'Kov, P.2    Cross, T.A.3    Samoson, A.4    Massiot, D.5
  • 23
    • 33746286593 scopus 로고    scopus 로고
    • 17O NMR - An introduction to the background principles and applications to inorganic materials
    • DOI 10.1039/b514051j
    • 17O NMR - an introduction to the background principles and applications to inorganic materials Chem. Soc. Rev. 35 2006 718 735 (Pubitemid 44107175)
    • (2006) Chemical Society Reviews , vol.35 , Issue.8 , pp. 718-735
    • Ashbrook, S.E.1    Smith, M.E.2
  • 25
    • 0032674476 scopus 로고    scopus 로고
    • 17O NMR studies of borate, borosilicate, and boroaluminate glasses
    • 17O NMR studies of borate, borosilicate, and boroaluminate glasses J. Am. Ceram. Soc. 82 1999 1519 1528
    • (1999) J. Am. Ceram. Soc. , vol.82 , pp. 1519-1528
    • Wang, S.1    Stebbins, J.F.2
  • 26
    • 33746498986 scopus 로고    scopus 로고
    • Oxygen sites and network coordination in sodium germanate glasses and crystals: High-resolution oxygen-17 and sodium-23 NMR
    • DOI 10.1021/jp0615510
    • L.-S. Du, and J.F. Stebbins Oxygen sites and network coordination in sodium germanate glasses and crystals: high-resolution oxygen-17 and sodium-23 NMR J. Phys. Chem. B 110 2006 12427 12437 (Pubitemid 44139427)
    • (2006) Journal of Physical Chemistry B , vol.110 , Issue.25 , pp. 12427-12437
    • Du, L.-S.1    Stebbins, J.F.2
  • 28
    • 78649466444 scopus 로고    scopus 로고
    • Effect of pressure on structure of oxide glasses at high pressure: Insights from solid-state NMR of quadrupolar nuclides
    • S.K. Lee Effect of pressure on structure of oxide glasses at high pressure: insights from solid-state NMR of quadrupolar nuclides Solid State NMR 38 2010 45 57
    • (2010) Solid State NMR , vol.38 , pp. 45-57
    • Lee, S.K.1
  • 29
    • 45149145322 scopus 로고
    • Rotational-echo double-resonance NMR
    • T. Gullion, and J. Schaefer Rotational-echo double-resonance NMR J. Magn. Reson. 81 1989 196 200
    • (1989) J. Magn. Reson. , vol.81 , pp. 196-200
    • Gullion, T.1    Schaefer, J.2
  • 30
    • 0000844732 scopus 로고    scopus 로고
    • Introduction to rotational-echo, double-resonance NMR
    • T. Gullion Introduction to rotational-echo, double-resonance NMR Concept. Magnetic Res. 10 1998 277 289
    • (1998) Concept. Magnetic Res. , vol.10 , pp. 277-289
    • Gullion, T.1
  • 31
    • 10444276724 scopus 로고    scopus 로고
    • Medium-range order in cesium borate glasses probed by double-resonance NMR
    • P.M. Aguiar, and S. Kroeker Medium-range order in cesium borate glasses probed by double-resonance NMR Solid State NMR 27 2005 10 15
    • (2005) Solid State NMR , vol.27 , pp. 10-15
    • Aguiar, P.M.1    Kroeker, S.2
  • 33
    • 77956404416 scopus 로고    scopus 로고
    • Liquid-liquid phase separation in model nuclear waste glasses: A solid-state double-resonance NMR study
    • C. Martineau, V.K. Michaelis, S. Schuller, and S. Kroeker Liquid-liquid phase separation in model nuclear waste glasses: a solid-state double-resonance NMR study Chem. Mater. 22 2010 4896 4903
    • (2010) Chem. Mater. , vol.22 , pp. 4896-4903
    • Martineau, C.1    Michaelis, V.K.2    Schuller, S.3    Kroeker, S.4
  • 38
    • 84860442675 scopus 로고    scopus 로고
    • Characterisation of heterogeneous molybdate and chromate phase assemblages in model nuclear waste glasses by multinuclear magnetic resonance spectroscopy
    • B.J. Greer, and S. Kroeker Characterisation of heterogeneous molybdate and chromate phase assemblages in model nuclear waste glasses by multinuclear magnetic resonance spectroscopy Phys. Chem. Chem. Phys. 14 2012 7375 7383
    • (2012) Phys. Chem. Chem. Phys. , vol.14 , pp. 7375-7383
    • Greer, B.J.1    Kroeker, S.2
  • 40
    • 84991994534 scopus 로고    scopus 로고
    • Precipitation of mixed-alkali molybdates during HLW vitrification
    • K.L. Smith, K.R. Whittle, S. Kroeker, B. Uberuaga, Materials Research Society Boston, MA
    • S. Kroeker, C.S. Higman, V.K. Michaelis, N.B. Svenda, and S. Kroeker Precipitation of mixed-alkali molybdates during HLW vitrification K.L. Smith, K.R. Whittle, S. Kroeker, B. Uberuaga, Scientific Basis for Nuclear Waste Management XXXIV 2010 Materials Research Society Boston, MA
    • (2010) Scientific Basis for Nuclear Waste Management XXXIV
    • Kroeker, S.1    Higman, C.S.2    Michaelis, V.K.3    Svenda, N.B.4    Kroeker, S.5
  • 42
    • 0002099140 scopus 로고    scopus 로고
    • Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses
    • PII S0009261499004467
    • P.K. Madhu, A. Goldbourt, L. Frydman, and S. Vega Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses Chem. Phys. Lett. 307 1999 41 47 (Pubitemid 129556367)
    • (1999) Chemical Physics Letters , vol.307 , Issue.1-2 , pp. 41-47
    • Madhu, P.K.1    Goldbourt, A.2    Frydman, L.3    Vega, S.4
  • 44
    • 0036462575 scopus 로고    scopus 로고
    • Procedures for labeling the high-resolution axis of two-dimensional MQ-MAS NMR spectra of half-integer quadrupole spins
    • DOI 10.1006/snmr.2001.0043, PII S0926204001900438
    • Y. Millot, and P.P. Man Procedures for labeling the high-resolution axis of two-dimensional MQ-MAS NMR spectra of half-integer quadrupole spins Solid State NMR 21 2002 21 43 (Pubitemid 34867588)
    • (2002) Solid State Nuclear Magnetic Resonance , vol.21 , Issue.1-2 , pp. 21-43
    • Millot, Y.1    Man, P.P.2
  • 46
    • 44949290573 scopus 로고
    • A quantitative study of aluminum-27 MAS NMR in crystalline YAG
    • D. Massiot, C. Bessada, J.P. Coutures, and F. Taulelle A quantitative study of aluminum-27 MAS NMR in crystalline YAG J. Magn. Reson. 90 1990 231 242
    • (1990) J. Magn. Reson. , vol.90 , pp. 231-242
    • Massiot, D.1    Bessada, C.2    Coutures, J.P.3    Taulelle, F.4
  • 48
    • 0034806736 scopus 로고    scopus 로고
    • 17O multiple-quantum MAS NMR study of high-pressure hydrous magnesium silicates
    • 17O multiple-quantum MAS NMR study of high-pressure hydrous magnesium silicates J. Am. Chem. Soc. 123 2001 6360
    • (2001) J. Am. Chem. Soc. , vol.123 , pp. 6360
    • Ashbrook, S.E.1    Berry, A.J.2    Wimperis, S.3
  • 50
    • 0001057342 scopus 로고
    • High resolution NMR of quadrupolar nuclei in rotating solids
    • A. Samoson High resolution NMR of quadrupolar nuclei in rotating solids Chem. Phys. Lett. 83 1981 229 232
    • (1981) Chem. Phys. Lett. , vol.83 , pp. 229-232
    • Samoson, A.1
  • 52
    • 0042567528 scopus 로고    scopus 로고
    • 17O MAS and 3QMAS NMR on calcium aluminate and low-silica Ca-aluminosilicate glasses
    • 17O MAS and 3QMAS NMR on calcium aluminate and low-silica Ca-aluminosilicate glasses Am. Mineral. 88 2003 949 955
    • (2003) Am. Mineral. , vol.88 , pp. 949-955
    • Allwardt, J.R.1    Lee, S.K.2    Stebbins, J.F.3
  • 56
    • 10444243521 scopus 로고    scopus 로고
    • Site connectivities in sodium aluminoborate glasses: Multinuclear and multiple quantum NMR results
    • L.-S. Du, and J.F. Stebbins Site connectivities in sodium aluminoborate glasses: multinuclear and multiple quantum NMR results Solid State NMR 27 2005 37 49
    • (2005) Solid State NMR , vol.27 , pp. 37-49
    • Du, L.-S.1    Stebbins, J.F.2
  • 57
    • 33746799800 scopus 로고    scopus 로고
    • Disorder and the extent of polymerization in calcium silicate and aluminosilicate glasses: O-17 NMR results and quantum chemical molecular orbital calculations
    • DOI 10.1016/j.gca.2006.06.1550, PII S0016703706018394
    • S.K. Lee, and J.F. Stebbins Disorder and the extent of polymerization in calcium silicate and aluminosilicate glasses: O-17 NMR results and quantum chemical molecular orbital calculations Geochim. Cosmochim. Acta 40 2006 4275 4286 (Pubitemid 44177331)
    • (2006) Geochimica et Cosmochimica Acta , vol.70 , Issue.16 , pp. 4275-4286
    • Lee, S.K.1    Stebbins, J.F.2
  • 60
    • 0035500696 scopus 로고    scopus 로고
    • Direct observation of multiple oxygen sites in oxide glasses: Recent advances from triple-quantum magic-angle spinning nuclear magnetic resonance
    • DOI 10.1016/S0022-3093(01)00653-6, PII S0022309301006536
    • J.F. Stebbins, P. Zhao, S.K. Lee, and J.V. Oglesby Direct observation of multiple oxygen sites in oxide glasses: recent advances from triple-quantum magic-angle spinning nuclear magnetic resonance J. Non-Cryst. Solids 293-295 2001 67 73 (Pubitemid 32997843)
    • (2001) Journal of Non-Crystalline Solids , vol.293-295 , Issue.1 , pp. 67-73
    • Stebbins, J.F.1    Zhao, P.2    Sung Keun Lee3    Oglesby, J.V.4
  • 64
    • 77952832497 scopus 로고    scopus 로고
    • Caesium volatilisation in borosilicate glasses: A multinuclear magnetic resonance study
    • V.K. Michaelis, and S. Kroeker Caesium volatilisation in borosilicate glasses: a multinuclear magnetic resonance study Phys. Chem. Glasses Eur. J. Glass Sci. Technol. B 50 2009 249
    • (2009) Phys. Chem. Glasses Eur. J. Glass Sci. Technol. B , vol.50 , pp. 249
    • Michaelis, V.K.1    Kroeker, S.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.