Ultrahigh-field NMR spectroscopy of quadrupolar transition metals: 55Mn NMR of several solid manganese carbonyls

Inorganic Chemistry

Volumn 45, Issue 21, 2006, Pages 8492-8499

  Ooms, Kristopher J ^a   Feindel, Kirk W ^a   Terskikh, Victor V ^b   Wasylishen, Roderick E ^a  

^a UNIVERSITY OF ALBERTA   (Canada)

^b UNIVERSITY OF OTTAWA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33750418331     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0608445     Document Type: Article

References (67)

1. Ooms, K. J.; Wasylishen, R. E. J. Am. Chem. Soc. 2004, 126, 10972-10980.
2. Bryce, D. L.; Wasylishen, R. E. Phys. Chem. Chem. Phys. 2002, 4, 3591-3600.
3. Bryce, D. L.; Wasylishen, R. E. Phys. Chem. Chem. Phys. 2001, 3, 5154-5157.
4. Lipton, A. S.; Heck, R. W.; Ellis, P. D. J. Am. Chem. Soc. 2004, 126, 4735-4739.
5. De Lacaillerie, J. B. D.; Barberon, F.; Romanenko, K. V.; Lapina, O. B.; Le Polles, L.; Gautier, R.; Gan, Z. H. J. Phys. Chem. B 2005, 109, 14033-14042.
6. Larsen, F. H.; Farnan, I.; Lipton, A. S. J. Magn. Reson. 2006, 178, 228-236.
7. Can. Chem. News 2006, April, 5.
8. Pyykkö, P. Mol. Phys. 2001, 99, 1617-1629.
9. Wadsworth, M.; France, P. W. J. Magn. Reson. 1983, 51, 424-429.
10. Pribula, C. D.; Brown, T. L.; Münck, E. J. Am. Chem. Soc. 1974, 96, 4149-4154.
11. Harris, R. K.; Becker, E. D.; De Menezes, S. M. C.; Goodfellow, R.; Granger, P. Pure Appl. Chem. 2001, 73, 1795-1818.
12. Rehder, D.; Bechthold, H.-Ch.; Keçeci, A.; Schmidt, H.; Siewing, M. Z. Naturforsch. 1982, 37b, 631-645.
13. Miles, W. J.; Garrett, B. B.; Clark, R. J. Inorg. Chem. 1969, 8, 2817-2818.
14. Kidd, R. G.; Goodfellow, R. J. In NMR and the Periodic Table; Harris, R. K., Mann, B. E., Eds.; Academic Press: London, 1979; pp 218-222.
15. Rehder, D. In Multinuclear NMR; Mason, J., Ed.; Plenum: New York, 1989; pp 507-511.
16. Granger, P. In Encyclopedia of NMR; Grant, D. M., Harris, R. K., Eds.; John Wiley and Sons: Chichester, 2002; Vol. 6, pp 3889-3900.
17. Pregosin, P. S. Transition Metal Nuclear Magnetic Resonance; Elsevier: Amsterdam, 1991.
18. Segel, S. L. J. Chem. Phys. 1969, 51, 848-850.
19. Mooberry, E. S.; Sheline, R. K. J. Chem. Phys. 1972, 56, 1852-1855.
20. Mooberry, E. S.; Spiess, H. W.; Sheline, R. K. J. Chem. Phys. 1972, 57, 813-821.
21. Burton, D. J.; Harris, R. K. Chem. Commun. 1982, 256-257.
22. Tarasov, V. P.; Kirkakosyan, G. A.; Meladze, M. A.; German, K. É. Koordinats. Khim. 1993, 19, 269-283.
23. Spiess, H. W.; Sheline, R. K. J. Chem. Phys. 1971, 54, 1099-1103.
24. Slater, J. L.; Pupp, M.; Sheline, R. K. J. Chem. Phys. 1972, 57, 2105-2108.
25. Sweigart, D. A.; Reingold, J. A. In Encyclopedia of Inorganic Chemistry; King, R. B., Ed.; Wiley: Chichester, 2005; Vol. 5, p 2907.
26. Toxicological Profile for Manganese; U.S. Department of Health and Human Services: Washington, DC, 2000; p 329.
27. Gorsich, R. D. J. Am. Chem. Soc. 1962, 84, 2486-2491.
28. 3 and allowed to react for 2 h. The solvent was reduced to half volume, poured into cold water, and filtered, and then the precipitate was extracted with hot hexane (yields 70-80%).
29. Bodart, P. R.; Amoureux, J.-P.; Dumazy, Y.; Lefort, R. Mol. Phys. 2000, 98, 1545-1551.
30. Larsen, F. H.; Jakobsen, H. J.; Ellis, P. D.; Nielsen, N. C. J. Magn. Reson. 1998, 131, 144-147.
31. Larsen, F. H.; Jakobsen, H. J.; Ellis, P. D.; Nielsen, N. C. J. Phys. Chem. A 1997, 101, 8597-8606.
32. Lipton, A. S.; Wright, T. A.; Bowman, M. K.; Reger, D. L.; Ellis, P. D. J. Am. Chem. Soc. 2002, 124, 5850-5860.
33. Amoureux, J.-P.; Fernandez, C.; Steuernagel, S. J. Magn. Reson. A 1996, 123, 116-118.
34. van Lenthe E.; Jan Baerends, E. J. Chem. Phys. 2000, 112, 8279-8291.
35. Schreckenbach, G.; Ziegler, T. J. Phys. Chem. 1995, 99, 606-611.
36. Schreckenbach, G.; Ziegler, T. Int. J. Quantum Chem. 1996, 60, 753-766.
37. Schreckenbach, G.; Ziegler, T. Int. J. Quantum Chem. 1997, 61, 899-918.
38. Wolff, S. K.; Ziegler, T. J. Chem. Phys. 1998, 109, 895-905.
39. Wolff, S. K.; Ziegler, T.; van Lenthe, E.; Baerends, E. J. J. Chem. Phys. 1999, 110 7689-7698.
40. Guerra, C. F.; Snijders, J. G.; te Velde, G.; Baerends, E. J. Theor. Chem. Acc. 1998, 99, 391-403.
41. ADF 2004.01, SCM [online], Theoretical Chemistry; Vrije Universiteit: Amsterdam, Availaible from http://www.scm.com.
42. Vosko, S. H.; Wilk, L.; Nusair, M.; Can. J. Phys. 1980, 58, 1200-1211.
43. Becke, A. D. Phys. Rev. A 1988, 38, 3098-3100.
44. Perdew, J. P. Phys. Rev. B 1986, 33, 8822-8824.
45. Perdew, J. P. Phys. Rev. B 1986, 34, 7406.
46. Bühl M. J. Phys. Chem. A 2002, 106, 10505-10509.
47. Fitzpatrick, P. J.; Le Page, Y.; Sedman, J.; Butler, I. S. Inorg Chem. 1981, 20, 2852-2861.
48. Full, J.; González, L.; Daniel, C. J. Phys. Chem. A 2001, 105, 184-189.
49. Lichtenberger, D. L.; Fenske, R. F. J. Am. Chem. Soc. 1976, 98, 50-63.
50. Albright, T. A. Acc. Chem. Res. 1982, 15, 149-55.
51. Ramsey, N. F. Phys. Rev. 1950, 78, 699-703.
52. Jameson, C. J.; Gutowsky, H. A. J. Chem. Phys. 1964, 40, 1714-1724.
53. Daniel, C.; Full, J.; González, L.; Kaposta, C.; Krenz, M.; Lupulescu, C.; Manz, J.; Minemoto, S.; Oppel, M.; Rosendo-Francisco, P.; Vajda, S.; Wöste, L. Chem. Phys. 2001, 267, 247-260.
54. Akitt, J. W.; McDonald, W. S. J. Magn. Reson. 1984, 58, 401-412.
55. Oorns, K. J.; Feindel, K. W.; Willans, M. J.; Wasylishen, R. E.; Hanna, J. V.; Pike, K. J.; Smith, M. E. Solid State Nucl. Magn. Reson. 2005, 28, 125-134.
56. Churchill, M. R.; Amoh, K. N.; Wasserman, H. J. Inorg. Chem. 1981, 20, 1609-1611.
57. Q is small, this is not likely to significantly affect the simulated line shapes.
58. Wi, S.; Frydman, L. J. Chem. Phys. 2000, 112, 3248-3261.
59. Siegel, R.; Nakashima, T. T.; Wasylishen, R. E. Chem. Phys. Lett. 2006, 421, 529-533.
60. Weber, H. P.; Bryan, R. F. Acta Crystallogr. 1967, 22, 822-836.
61. Christendat, D.; Butler, I. S.; Gilson, F. R.; Morin, D. F. G. Can. J. Chem. 1999, 77, 1892-1898.
62. Medek, A.; Harwood: J. S.; Frydman, L. J. Am. Chem. Soc. 1995, 117, 12779-12787.
63. Han, O. H.; Oldfield, E. Inorg. Chem. 1990, 29, 3666-3669.
64. Alred, A. L.; Rochow, E. G. J. Inorg. Nucl. Chem. 1958, 5, 264-268.
65. Ooms, K. J.; Wasylishen, R. E. Can. J. Chem. 2006, 84, 300-308.
66. Mason, J. Solid State Nucl. Magn. Reson. 1993, 2, 285-288.
67. Willans, M. J.; Feindel, K. W.; Ooms, K. J.; Wasylishen, R. E. Chem. Eur. J., 2006, 12, 159-168.