Robust calibrations on reduced sample sets for API content prediction in tablets: Definition of a cost-effective NIR model development strategy

Analytica Chimica Acta

Volumn 761, Issue , 2013, Pages 62-70

  Pieters, Sigrid ^a   Saeys, Wouter ^b   Van den Kerkhof, Tom ^c   Goodarzi, Mohammad ^b   Hellings, Mario ^c   De Beer, Thomas ^d   Heyden, Yvan Vander ^a  

^a VRIJE UNIVERSITEIT BRUSSEL   (Belgium)

^b UNIVERSITY OF LEUVEN   (Belgium)

^c JOHNSON AND JOHNSON   (United States)

^d GHENT UNIVERSITY   (Belgium)

Author keywords

Augmentation methods; Near infrared spectroscopy; Orthogonal projection methods; Prior spectral information; Tablets

Indexed keywords

ABSORPTION SIGNALS; ACTIVE PHARMACEUTICAL INGREDIENTS; ANALYTES; ARTIFICIAL DATA; AUGMENTATION METHODS; CONTENT VARIATION; FREQUENCY SHIFT; LATENT VARIABLE; MODEL DEVELOPMENT; MODEL PERFORMANCE; ORTHOGONAL PROJECTION; ORTHOGONAL PROJECTION METHOD; PLS REGRESSION; PRE-PROCESSING; PREDICTION PERFORMANCE; PURE COMPONENTS; ROBUST CALIBRATION; SAMPLE SETS; SPECTRAL INFORMATION; SPECTRAL SHAPES; SPECTRAL VARIATION; TABLETS;

CLUTTER (INFORMATION THEORY); COST EFFECTIVENESS; FORECASTING; INFRARED DEVICES; NEAR INFRARED SPECTROSCOPY;

CALIBRATION;

ARTICLE; CALIBRATION; COST; EXTERNAL PARAMETER ORTHOGONALIZATION; MATHEMATICAL ANALYSIS; NEAR INFRARED SPECTROSCOPY; NOISE REDUCTION; PARTIAL LEAST SQUARES REGRESSION; PREDICTION; PRIORITY JOURNAL; TABLET; WATER CONTENT;

CALIBRATION; MODELS, CHEMICAL; PHARMACEUTICAL PREPARATIONS; SPECTROSCOPY, NEAR-INFRARED; TABLETS; WATER;

EID: 84872162159     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2012.11.034     Document Type: Article

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