Simulation of the chromatographic separation process in HPLC employing suspended-state NMR spectroscopy - Comparison of interaction behavior for monomeric and hydride-modified C18 stationary phases

Journal of Separation Science

Volumn 36, Issue 1, 2013, Pages 173-181

  Yeman, Helen ^a   Nicholson, Tim ^a   Matyska, Maria T ^b   Pesek, Joseph J ^b   Albert, Klaus ^a  

^a UNIVERSITY OF TÜBINGEN   (Germany)

^b SAN JOSE STATE UNIVERSITY   (United States)

Author keywords

1H suspended state NMR spectroscopy; Chemical environments; Signal half widths; Signal splitting; Spin lattice relaxation time

Indexed keywords

ALKYL CHAIN; ANALYTE MOLECULES; ANALYTES; CHEMICAL ENVIRONMENT; CHROMATOGRAPHIC SEPARATIONS; HIGH RESOLUTION; INTERACTION BEHAVIOR; LIGAND DENSITY; MOBILE PHASE; MODIFIED SILICA; MODIFIED SURFACES; NMR SIGNALS; SEPARATION BEHAVIORS; SHIFT-AND; SIGNAL HALF-WIDTHS; SIGNAL SPLITTING; SOLID STATE NMR; SPECTROSCOPIC BEHAVIOR; STATIONARY PHASIS; SURFACE COVERAGES;

CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDRIDES; MOLECULES; SILICA; SPIN-LATTICE RELAXATION;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

MONOMER; SILICON DIOXIDE;

ARTICLE; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHYSICAL CHEMISTRY; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SIMULATION; SOLID STATE; SYNTHESIS;

ANILINE COMPOUNDS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; NAPHTHALENES; PHENOLS;

EID: 84872101372     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201200729     Document Type: Article

References (30)

1. Horváth, C., Melander, W., Molnár, I., J. Chromatogr. A 1976, 125, 129-156.
2. Horváth, C., Melander, W., J. Chromatogr. Sci. 1977, 15, 393-404.
3. Colin, H., Guiochon, G., J. Chromatogr. A 1977, 141, 289-312.
4. Dorsey, J. G., Dill, K. A., Chem. Rev. 1989, 89, 331-346.
5. Kazakevich, Y. V., J. Chromatogr. A 2006, 1126, 232-243.
6. Kaliszan, R., J. Chromatogr. A 1993, 656, 417-435.
7. Kaliszan, R., van Straten, M. A., Markuszewski, M., Cramers, C. A., Claessens, H. A., J. Chromatogr. A 1999, 855, 455-486.
8. Rogers, S. D., Dorsey, J. G., J. Chromatogr. A 2000, 892, 57-65.
9. Neue, U. D., Van Tran, K., Iraneta, P. C., Alden, B. A., J. Sep. Sci. 2003, 26, 174-186.
10. Claessens, H. A., van Straten, M. A., Cramers, C. A., Jezierska, M., Buszewski, B., J. Chromatogr. A 1998, 826, 135-156.
11. Sander, L. C., Wise, S. A., J. Sep. Sci. 2003, 26, 283-294.
12. Gritti, F., Guiochon, G., Anal. Chem. 2005, 77, 4257-4272.
13. Gritti, F., Guiochon, G., J. Chromatogr. A 2006, 1115, 142-163.
14. Sander, L. C., Lippa, K. A., Wise, S. A., Anal. Bioanal. Chem. 2005, 382, 646-668.
15. Albert, K., Lacker, T., Raitza, M., Pursch, M., Egelhaaf, H. J., Oelkrug, D., Angew. Chem. Int. Ed. 1998, 37, 777-780.
16. Caldarelli, S., in:, Graham, A. W., (Ed.), Annual Reports on NMR Spectroscopy, Academic Press 2011, pp. 159-173.
17. Friebolin, V., Marten, S., Albert, K., Magn. Reson. Chem. 2010, 48, 111-116.
18. Coen, M., Lindon, J. C., Gavaghan, C., Holmes, E., Humpfer, E., Wilson, I. D., Stanley, P. D., Nicholson, J. K., Analyst 2001, 126, 548-550.
19. Coen, M., Wilson, I. D., Nicholson, J. K., Tang, H., Lindon, J. C., Anal. Chem. 2004, 76, 3023-3028.
20. Galushko, S., Chromatographia 1993, 36, 39-42.
21. Kühnle, M., Friebolin, V., Albert, K., Rimmer, C. A., Lippa, K. A., Sander, L. C., Anal. Chem. 2009, 81, 10136-10142.
22. Chu, C. H., Jonsson, E., Auvinen, M., Pesek, J. J., Sandoval, J. E., Anal. Chem. 1993, 65, 808-816.
23. Albert, K., Bayer, E., J. Chromatogr. A 1991, 544, 345-370.
24. Albert, K., J. Sep. Sci. 2003, 26, 215-224.
25. Pursch, M., Sander, L. C., Albert, K., Anal. Chem. 1996, 68, 4107-4113.
26. Ellwanger, A., Matyska, M., Albert, K., Pesek, J., Chromatogr. 1999, 49, 424-430.
27. Sandoval, J. E., Pesek, J. J., Anal. Chem. 1991, 63, 2634-2641.
28. Pesek, J. J., Matyska, M. T., Larrabee, S., J. Sep. Sci. 2007, 30, 637-647.
29. Pfleiderer, B., Albert, K., Lork, K. D., Unger, K. K., Brückner, H., Bayer, E., Angew. Chem. 1989, 101, 336-340.
30. Voelkel, R., Angew. Chem. Int. Ed. 1988, 27, 1468-1483.