Method development and validation for ultra-high-pressure LC/MS/MS determination of hop prenylflavonoids in human serum

Journal of AOAC International

Volumn 95, Issue 6, 2012, Pages 1744-1749

  Yuan, Yang ^a   Qiu, Xi ^a   Nikolic, Dejan ^a   Dahl, Jeffrey H ^b   Van Breemen, Richard B ^a  

^a UNIVERSITY OF ILLINOIS AT CHICAGO   (United States)

^b Shimadzu Scientific Instruments   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ACCURACY AND PRECISION; ANALYTICAL METHOD; CANCER CHEMOPREVENTION; CLINICAL STUDY; COLLISION-INDUCED DISSOCIATION; DIETARY SUPPLEMENTS; GRADIENT ELUTION; HUMAN SERUM; ION ELECTROSPRAY; LIQUID-LIQUID EXTRACTION; METHOD DEVELOPMENT; PACKING MATERIALS; SELECTED REACTION MONITORING; SIMULTANEOUS DETERMINATIONS; TANDEM MS; ULTRA-HIGH-PRESSURE LC; XANTHOHUMOL;

MASS SPECTROMETRY;

BODY FLUIDS;

DYES, REAGENTS, INDICATORS, MARKERS AND BUFFERS; FLAVONOID;

ARTICLE; BLOOD; CALIBRATION; CHEMISTRY; ELECTROSPRAY MASS SPECTROMETRY; FEMALE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMULUS; HYDROLYSIS; MASS SPECTROMETRY; MIDDLE AGED; PRENYLATION; REPRODUCIBILITY; STANDARD; VALIDATION STUDY;

CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FEMALE; FLAVONOIDS; HUMANS; HUMULUS; HYDROLYSIS; INDICATORS AND REAGENTS; MASS SPECTROMETRY; MIDDLE AGED; PRENYLATION; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

HUMULUS; HUMULUS LUPULUS;

EID: 84871302996     PISSN: 10603271     EISSN: None     Source Type: Journal    
DOI: 10.5740/jaoacint.11-542     Document Type: Article

References (17)

1. Stevens, J.F., & Page, J.E. (2004) Phytochemistry 65, 1317-1330. http://dx.doi.org/10.1016/j.phytochem.2004.04.025
2. Gerhäuser, C. (2005) Eur. J. Cancer 41, 1941-1954. http://dx.doi.org/10.1016/j.ejca.2005.04.012
3. Miranda, C., Stevens, J., Helmrich, A., Henderson, M., Rodriguez, R., Yang, Y.H., Deinzer, M., Barnes, D., & Buhler, D. (1999) Food Chem. Toxicol. 37, 271-285. http://dx.doi.org/10.1016/S0278-6915(99)00019-8
4. Miranda, C., Aponso, G., Stevens, J., Deinzer, M., & Buhler, D. (2000) Cancer Lett. 149, 21-29. http://dx.doi.org/10.1016/S0304-3835(99)00328-6
5. Gerhauser, C., Alt, A., Heiss, E., Gamal-Eldeen, A., Klimo, K., Knauft, J., Neumann, I., Scherf, H.R., Frank, N., & Bartsch, H. (2002) Mol. Cancer Ther. 1, 959-969
6. Milligan, S., Kalita, J., Heyerick, A., Rong, H., De Cooman, L., & De Keukeleire, D. (1999) J. Clin. Endocrinol. Metab. 84, 2249-2252. http://dx.doi.org/10.1210/jc.84.6.2249
7. Milligan, S., Kalita, J., Pocock, V., van De Kauter, V., Stevens, J., Deinzer, M., Rong, H., & De Keukeleire, D. (2000) J. Clin. Endocrinol. Metab. 85, 4912-4915. http://dx.doi.org/10.1210/jc.85.12.4912
8. Liu, J., Burdette, J.E., Xu, H., Gu, C., van Breemen, R.B., Bhat, K.P.L., Booth, N., Constantinou, A.I., Pezzuto, J.M., & Fong, H.H.S. (2001) J. Agric. Food Chem. 49, 2472-2479. http://dx.doi.org/10.1021/jf0014157
9. Chadwick, L.R., Nikolic, D., Burdette, J.E., Overk, C.R., Bolton, J.L., van Breemen, R.B., Fröhlich, R., Fong, H.H.S., Farnsworth, N.R., & Pauli, G.F. (2004) J. Nat. Prod. 67, 2024-2032. http://dx.doi.org/10.1021/ np049783i
10. Milligan, S., Kalita, J., Pocock, V., Heyerick, A., De Cooman, L., Rong, H., & De Keukeleire, D. (2002) Reproduction 123, 235-242. http://dx.doi.org/10.1530/rep.0.1230235
11. Nikolic, D., Li, Y., Chadwick, L.R., Pauli, G.F., & van Breemen, R.B. (2005) J. Mass Spectrom. 40, 289-299. http://dx.doi.org/10.1002/jms.753
12. Wyns, C., Derycke, L., Soenen, B., Bolca, S., Deforce, D., Bracke, M., & Heyerick, A. (2011) Talanta 85, 197-205. http://dx.doi.org/10.1016/j. talanta.2011.03.047
13. Schaefer, O., Bohlmann, R., Schleuning, W.D., Schulze-Forster, K., & Hümpel, M. (2005) J. Agric. Food Chem. 53, 2881-2889. http://dx.doi.org/10. 1021/jf047897u
14. Avula, B., Ganzera, M., Warnick, J.E., Feltenstein, M.W., Sufka, K.J., & Khan, I.A. (2004) J. Chromatogr. Sci. 42, 378-382
15. Wyns, C., Bolca, S., De Keukeleire, D., & Heyerick, A. (2010) J. Chromatogr. B 878, 949-956. http://dx.doi.org/10.1016/j.jchromb.2010.02.022
16. Bolca, S., Li, J., Nikolic, D., Roche, N., Blondeel, P., Possemiers, S., De Keukeleire, D., Bracke, M., Heyerick, A., van Breemen, R.B., & Depypere H. (2010) Mol. Nutr. Food Res. 54, S284-S294. http://dx.doi.org/10.1002/mnfr. 200900519
17. Bonfiglio, R., King, R.C., Olah, T.V., & Merkle, K. (1999) Rapid Commun. Mass Spectrom. 13, 1175-1185. http://dx.doi.org/10.1002/(SICI)1097- 0231(19990630)13:12<1175::AIDRCM639> 3.0.CO;2-0