Development of methodology for determination of pesticides residue in water by SPE/HPLC/DAD

Environmental Technology (United Kingdom)

Volumn 33, Issue 20, 2012, Pages 2299-2304

  Cappelini, Luciana Teresa Dias ^a   Cordeiro, Daniela ^a   Brondi, Silvia Helena Govoni ^b   Prieto, Kátia Roberta ^a   Vieira, Eny Maria ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

^b EMBRAPA CERRADOS   (Brazil)

Author keywords

liquid chromatography; pesticides; solid phase extraction; water

Indexed keywords

AGRICULTURE; AQUIFERS; GROUNDWATER POLLUTION; HERBICIDES; HYDROGEOLOGY; LIQUID CHROMATOGRAPHY; PESTICIDES; RIVERS; SURFACE WATER RESOURCES; UREA; WATER;

AMETRYN; ANALYTICAL METHOD; CORRELATION COEFFICIENT; CROP YIELD; DETECTION AND QUANTIFICATION LIMIT; DETECTION LIMITS; DIODE ARRAY DETECTION; FIPRONIL; MUNICIPAL WATER; SOLID-PHASE EXTRACTION; WATER SAMPLES;

EXTRACTION;

AMETRYN; ATRAZINE; DIURON; DRINKING WATER; FIPRONIL; PESTICIDE; RIVER WATER;

CROP YIELD; DETECTION METHOD; ENVIRONMENTAL RISK; EXTRACTION METHOD; HEADWATER; LIQUID CHROMATOGRAPHY; PESTICIDE RESIDUE; PRECISION; RIVER POLLUTION; SAMPLING; SUGAR CANE;

ACCURACY; ANALYTIC METHOD; ARTICLE; BRAZIL; DIODE ARRAY DETECTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; RIVER; SIGNAL NOISE RATIO; SOLID PHASE EXTRACTION; SUGARCANE; WASTE WATER MANAGEMENT; WATER ANALYSIS; WATER SAMPLING;

BRAZIL; FEIJAO RIVER; SAO PAULO [BRAZIL];

HEXAPODA;

EID: 84870054813     PISSN: 09593330     EISSN: 1479487X     Source Type: Journal    
DOI: 10.1080/09593330.2012.665494     Document Type: Article

References (31)

1. A.E. Jacomini, P.B. de Camargo, W.E.P. Avelar, and P.S.B. Bonato, Assessment of ametryn contamination in river water, river sediment, and mollusk bivalves in São Paulo State, Brasil, Arch. Environ. Contam. Toxicol. 60 (2011), pp. 452-461.
2. D.A. SOUZA, Development of analytical methods for multiresidue determination of pesticides in drinking water of São Carlos - SP (Desenvolvimento de metodologia analítica para determinação de multiresíduos de pesticidas em água de abastecimento de São Carlos - SP), Doctoral thesis, São Paulo University, 2000.
3. F.M. Lanças and S.H.G. Brondi, HPLC determination of pesticide residues widely employed in sugar cane cultures in river water samples, J. Liq. Chromatogr. Related Technol. 27 (2004), pp. 171-179.
4. M.A.L. Milhone, D.O.B. Sousa, F.A.A. Lima, and R.F.N. Nascimento, Avaliação do potencial de contaminação de águas superficiais e subterrâneas por pesticidas aplicados na agricultura do Baixo Jaguaribe, CE. Eng. Sanit. Ambient. 14 (2009), pp. 363-372.
5. P.T. Hasset and F.G. Lee, Modeling of pesticide in aqueous environment, in Environmental Dynamic of Pesticides, R. Haque and W.H. Freed, eds., New York, Plenum, 1975, pp. 173-184.
6. Ministério da Saúde. Portaria n 518 de 25 de março de 2004. Estabelece os procedimentos e responsabilidades relativas ao controle e vigilância da água para consumo humano e seu padrão de potabilidade e da procedência, 2004. Available at http://dtr2001.saude. gov.br/sas/PORTARIAS/Port2004/ GM/GM-518.htm
7. Council Directive 98/83/EC, Concerning the quality of water intended for human consumption, Off. J. Eur. Union 5th December 1998 L330, 32-43. Available at http://www.iss.it/ binary/publ/publi/0016.1109850012.pdf.
8. Organização Mundial da Saúde (OMS) [World Health Organization, WHO]. Guidelines for Drinking-water Quality, 3rd ed., ch. 8 draft 11, 2006. Available at http://www.who.int/ water-sanitation-health/dwq/gdwq3rd- add1.pdf.
9. P. Parrilla and J.L. Martinez Vidal, Determination of pesticide residue in water using LLE or SPE and HPLC/DAD detection, Anal. Letters 30 (1997), pp. 1719-1738.
10. S.H.G. Brondi and F.M. Lanças, Optimization of a methodology for determination of organochlorine pesticides in surface water by SPME-GC/MS, J. Environ. Sci. Health Part B 40 (2005), pp. 513-523.
11. S.H.G. Brondi, J.C. Rodrigues, and F.M. Lanças, Development and validation of a methodology for the determination of pesticides in water by SPME-LC/DAD, J. Liq. Chromatogr. Related and Technol., 28 (2005), pp. 2909-2919.
12. H. Sabik, R. Jeannot, and B. Rondeau, Multiresidue methods using solid-hase extraction techniques for monitoring priority pesticides, including triazines and degradation products, in ground water and surface waters, J. Chromatogr. A 885 (2000), pp. 217-236.
13. F.M. Lanças, Solid Phase Extraction (SPE) (Extração Em Fase Sólida - SPE), Editora RiMa Ltda, São Carlos, Brazil, 2004, p. 93.
14. G. Doran, S. Helliwell, and P. Eberbach, Extraction of fipronil and thiobecarb from anaerobic water samples using solid-hase extraction, J. AOAC Int. 88 (2005), pp. 854-859.
15. S.H.G. Brondi, A.N. Macedo, G.H.L. Vicente, and A.R.A. Nogueira, Evaluation of the QuEChERS method and gas chromatography-mass spectrometry for the analysis pesticide residues in water and sediment. Bull. Environ. Contam. Toxicol. (86) (2011), pp. 18-22.
16. T. Cserháti, E. Forgács, Z. Deyl, I. Miksik, and A. Eckhardt, Chromatographic determination of herbicide residues in various matrices, Biomed. Chromatogr. 18 (2004), pp. 350-359.
17. A.E. Jacomini, P.B. de Camargo, W.E.P. Avelar, and P.S.B. Bonato, Determination of ametryn in river water, river sediment and bivalve mussels by liquid chromatographytandem mass spectrometry, J. Braz. Chem. Soc. 20 (2009), pp. 107-116.
18. M. Ribani, C.B.G. Bottoli, C.H. Collins, I.C.S.F. Jardim, and L.F.C.V. Melo, Validação em métodos cromatográficos e eletroforéticos, Quim. Nova. 27 (2004), pp. 771-780.
19. Agência Nacional de Vigilância Sanitária (ANVISA), Resolução RE no899,de 29/05/2003. Available at http://www. anvisa.gov.br.
20. World Health Organization, WHO Expert Committee on Specifications for Pharmaceutical Preparations, Thirtysecond report, WHO Technical Report Series 823, 1992, Geneva. Available at http://whqlibdoc.who.int/trs/WHO- TRS-823.pdf.
21. E. Vieira and J. Lichtig, Validação de métodos cromatográficos em análise de resíduos de pesticidas, Arq. Inst. Biol. São Paulo 71 (2004), pp. 1-749.
22. NIST Livro de Química naWeb, Base de dados de Referência padrão do NIST número 69. Available at http://webbook. nist.gov/chemistry
23. F.M. Lanças,Validation of cromatographic analysis methods (Métodos Cromatográficos de Análise), Editora RiMa Ltda, São Carlos, Brazil, 2004, p. 46.
24. California Department of Food and Agriculture, Center for Analytical Chemistry, Environmental Monitoring Section, Determination of atrazine, simazine, diuron, prometon, bromacil, prometryn, hexazinone, cyanazine, metribuzin in river water, 1998.Available at http://www.cdpr.ca.gov/docs/ specproj/tribal/method151.pdf.
25. M.E. Baez and J. Zincker, Parametros de calidad analitica de un metodo de determinacion multiresíduos de plaguicidas por HPLC-DAD, Bol. Soc. Chil. Quim. 44 (1999), pp. 1-13.
26. A. Kotrikla, G. Gatidou, and T.D. Lekkas., Monitoring of triazine and phenylurea herbicides in surface waters of Greece, J. Environ. Sci. Health. Part B 41 (2006), pp. 135-144.
27. A. Polettini, M.M. Montagna, E.A. Hogendoorn, E. Dijkman, P. Van Zoonen, and L.A. Van Ginkel, Applicability of coupled-column liquid chromatography to the analysis of β- agonists in urine by direct sample injection I. Development of a single-residue reversed-hase liquid chromatography-UV method for clenbuterol and selection of chromatographic conditions suitable for multi-residue analysis, J. Chromatogr. A 696 (1995), pp. 19-31.
28. T. Tuzimski and J.J. Sobczyski, Application HPLC-DAD and TLC-DAD after SPE to the quantitative analysis of pesticides in water samples, J. Liq. Chromatogr. Related Technol. 1 (2009), pp. 1241-1258.
29. Environmental Protection Agency, National Primary DrinkingWater Standards, 2001.Available at http://www.epa.gov/ safewater
30. G. Gatidoua, A. Kotriklaa, N.S. Thomaidisb, and T.D. Lekkasa, Determination of the antifouling booster biocides irgarol 1051 and diuron and their metabolites in seawater by high performance liquid chromatography-diode array detector, Anal. Chim. Acta. 528 (2005), pp. 89-99.
31. BRASIL, Conselho Nacional do Meio Ambiente, CONAMA, Resoluçã o no 357/05 de março de 2005. Dispõe sobre a classificaç ão dos corpos de água e diretrizes ambientais para o seu enquadramento, bem como estabelece as condições e padrões de lançamento de efluentes, e dá outras providências. Available at http://www.mma.gov.br/port/ conama/res/res05/res35705.pdf