Development and validation of a methodology for the determination of pesticides in water by SPME-LC/DAD

Journal of Liquid Chromatography and Related Technologies

Volumn 28, Issue 18, 2005, Pages 2909-2919

  Brondi, Silvia H G ^a   Rodrigues Da Silva, José C ^b   Lanças, Fernando M ^b  

^a Physiology and Pharmacology Laboratory School of Veterinary Medicine University Center of Octavio Bastos Education Foundation   (Brazil)

^b UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Liquid chromatography; Pesticides; Solid phase microextraction; Water

Indexed keywords

DESORPTION; DETECTORS; EXTRACTION; PESTICIDES; PHASE COMPOSITION; SAMPLING; TEMPERATURE DISTRIBUTION; WATER;

ANALYTE; DIURON; POLYACRILATE FIBER; SOLID-PHASE MICROEXTRACTION;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

ACRYLIC ACID DERIVATIVE; DIURON; PESTICIDE; TEBUTHIURON; WATER;

ARTICLE; CHEMICAL ANALYSIS; DESORPTION; DIODE; DIODE ARRAY DETECTION; FIBER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIC STRENGTH; LIQUID CHROMATOGRAPHY; PH; SAMPLING; SOLID PHASE MICROEXTRACTION; SUGARCANE; TEMPERATURE; TEMPERATURE DEPENDENCE;

SACCHARUM; SACCHARUM HYBRID CULTIVAR;

EID: 27744573048     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070500271931     Document Type: Article

References (28)

1. Hatrík, S.; Tekel, J. Extraction methodology and chromatography for the determination of residual pesticides in water. J. Chromatogr. A 1996, 733, 217-233.
2. Albanis, T.A.; Hela, D.G. Multi-residue pesticide analysis in environmental water samples using solid-phase extraction discs and gas chromatography with flame thermionic and mass-selective detection. J. Chromatogr. A 1995, 707, 283-292.
3. Arthur, C.L.; Pratt, K.; Motlagh, S.; Pawliszyn, J. Environmental analysis of organic compounds in water using solid phase micro extraction. J. High Resol. Chromatogr. 1992, 15, 741-744.
4. Potter, D.; Pawliszyn, J. Detection of substituted benzenes in water at the pg/mL level using solid-phase microextraction and gas chromatography-ion trap mass spectrometry. J. Chromatogr. 1992, 625, 247-255.
5. Louch, D.; Motlagh, S.; Pawliszyn, J. Dynamics of organic compound extraction from water using liquid-coated fused silica fibers. Anal. Chem. 1992, 64, 1187-1199.
6. Chai, M.; Arthur, C.L.; Pawliszyn, J.; Belardi, R.P.; Pratt, K.F. Determination of volatile chlorinated hydrocarbons in air and water with solid-phase microextraction. Analyst 1993, 118, 1501-1505.
7. Eisert, R.; Levsen, K.; Fresenius, J. Determination of organophosphorus, Triazine and 2,6-dinitroaniline pesticides in aqueous samples via solid-phase microextraction (SPME) and gas-chromatography with nitrogen-phosphorus detection. J. Anal. Chem. 1995, 351, 555-562.
8. Popp, P.; Kalbitz, K.; Oppermann, G. Application of solid-phase microextraction and gas chromatography with electron-capture and mass spectrometric detection for the determination of hexachlorocyclohexanes in soil solutions. J. Chromatogr. A 1994, 687, 133-140.
9. Magdic, S.; Pawliszyn, J. Analysis of organochlorine pesticides using solid-phase microextraction. J. Chromatogr A 1996, 723, 11-22.
10. Page, B.D.; Lacroix, G. Application of solid-phase microextraction to the headspace gas chromatographic analysis of semi-volatile organochlorine contaminants in aqueous matrices. J. Chromatogr. A 1997, 757, 173-182.
11. Chen, J.; Pawliszyn, J. Solid Phase Microextraction Coupled to High-Performance Liquid Chromatography. Anal. Chem. 1995, 67, 2530-2533.
12. Lord, H.; Pawliszyn, J. Evolution of solid-phase microextraction technology. J. Chromatogr. A 2000, 885, 153-195.
13. Pawliszyn, J. Aplications of Solid Phase Microextraction; Cambridge. RSC Chromatograph Monographs: Ontario, Canada, 1997.
14. Jinno, K.; Muramatsu, T.; Saito, Y.; Magdic, S.; Pawliszyn, J. Analysis of pesticides in environmental water samples by solid-phase microextraction high performance liquid chromatography. J. Chromatogr. A 1996, 754, 137-144.
15. Silva, J.C.R. Project. Construction and Evaluation of a System for Solvating Gás Chromatography (Projeto, Construção e Avaliação de um Sistema para Cromatografia a Gás Solvatante); Tese de Doutorado: USP, São Carlos, Brazil. 2002: 258.
16. Alpendura, M.F. Solid-phase microextraction: a promising technique for sample preparation in environmental analysis. J. Chromatogr. A 2000, 889, 3-14.
17. Arthur, C.L.; Pawliszyn, J. Solid phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 1990, 62, 2145-2148.
18. Zhang, Z.Y.; Yang, M.J.; Pawliszyn, J. Solid-phase microextraction. Anal. Chem. 1994, 60, 844-853.
19. Magdic, S.; Boyd-Boland, A.; Jinno, K.; Pawliszyn, J. Analysis of organophosphorus inseticides from environmental samples using solid-phase microextraction. J. Chromatogr. A 1996, 736, 219-228.
20. Barrionuevo, W.R.; Lanças, F.M. Solid-phase microextraction of pyrethroid pesticides from water at low and sub-ppt levels at different temperatures. J. High Resol. Chromatogr. 2000, 23, 485-488.
21. Ferrari, R. Inter-laboratory validation of solid-phase microextraction for the determination of triazine herbicides and their degradation products at ng/L level in water samples. J. Chromatogr. A 1998, 795, 371-376.
22. Young, R.; Lopez-Avila, V. On line determination of organochlorine pesticides in water by solid-phase microextraction and gas chromatography with electron capture detection. J. High Resol. Chromatogr. 1996, 19, 247-256.
23. Natangelo, M.; Tavazzi, S.; Fanelli, R.; Benfenati, E. Analysis of some pesticides in water samples using solid-phase microextraction-gas chromatography with different mass spectrometric techniques. J. Chromatogr. A 1999, 859, 193-201.
24. Guandalini, S. Determination of Organophosphorus Pesticides Residues in Surface Waters through SPE-GC and SPME-GC Coupling (Determinação de Resíduos de Pesticidas Organofosforados em Águas Superficiais através dos Acoplamentos SPE-GC c SPME-GC): Dissertação de Mestrado: USP, São Carlos. Brazil, 1999; 79.
25. Leite, F. Validation Procedures in Chemical Analysis (Validaç ão em Análise Química); Editora Átomo Ltda: Campinas, Brazil, 1996; 64.
26. Chasin, A.A.M.; Nascimento, E.S.; Ribeiro-Neto, L.M.; Siqueira, M.E.P.B.; Andraus, M.H.; Salvadori, M.C.; Fernícola, N.A.G.; Gorni, R.; Salcedo, S. Validation of analytical methodologies for toxicological analysis (Validação de Métodos em Análises Toxicológicas: uma Abordagem Geral). Rev. Bras. Toxicol. 1998, 11, 1-6.
27. Laboratório Vegetal do Ministério da Agricultra. Validation of Analytical Methodologies for Determination of Pesticides Residues (Roteiro para Validação de Metodologia Analítica Visando a Determinação de Resíduos de Pesticidas). GARP, ANDEF: São Paulo, SP, 1997.
28. Gou, J.; Tragas, C.; Lord, H.; Pawliszyn, J. On-line coupling of in-tube solid phase microextraction (SPME) to HPLC for analysis of carbamates in water samples: comparison of two commercially available autosamplers. J. Microcol. Sep. 2000, 12, 125-134.