Feasibility and application of an HPLC/UVD to determine dinotefuran and its shorter wavelength metabolites residues in melon with tandem mass confirmation

Food Chemistry

Volumn 136, Issue 2, 2013, Pages 1038-1046

  Rahman, Md Musfiqur ^a   Park, Jong Hyouk ^a   Abd El Aty, A M ^b   Choi, Jeong Heui ^a   Yang, Angel ^a   Park, Ki Hun ^a   Nashir Uddin Al Mahmud, Md ^c   Im, Geon Jae ^d   Shim, Jae Han ^a  

^a Chonnam National University   (South Korea)

^b Cairo University   (Egypt)

^c UNIVERSITY OF DHAKA   (Bangladesh)

^d National Institute of Animal Science   (South Korea)

Author keywords

Dinotefuran; HPLC UVD; Matrix interaction; Metabolites; SPE clean up

Indexed keywords

AMMONIUM BICARBONATES; ANALYTES; ANALYTICAL METHOD; BEST CHOICE; CALIBRATION CURVES; DINOTEFURAN; HIGH WATER; HPLC-UVD; ION PAIRING; LC-MS/MS; LIMITS OF DETECTION; LIMITS OF QUANTITATIONS; MATRIX INTERFERENCE; MOBILE PHASIS; RAPID METHOD; REAL SAMPLES; RELATIVE STANDARD DEVIATIONS; REVERSE-PHASE COLUMN; SECONDARY AMINES; SHORTER WAVELENGTH; SOLID PHASE EXTRACTION CARTRIDGES; SPE CLEAN-UP; TANDEM MASS; TARGET ANALYTES; UV DETECTION;

ACETONITRILE; AMMONIUM COMPOUNDS; BIOMOLECULES; CALIBRATION; DETECTORS; ELECTROSPRAY IONIZATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MOBILE AGENTS; PURIFICATION;

METABOLITES;

1 METHYL 2 NITRO GUANIDINE; 1 METHYL 3 (TETRAHYDRO 3 FURYLMETHYL) GUANIDINE; 1 METHYL 3 (TETRAHYDRO 3 FURYLMETHYL) UREA; DINOTEFURAN; FURAN DERIVATIVE; INSECTICIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOLATION AND PURIFICATION; MELON; METABOLITE; NONHUMAN; SHORTER WAVELENGTH; SPECTRAL SENSITIVITY; TANDEM MASS SPECTROMETRY; ULTRAVIOLET SPECTROSCOPY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CUCURBITACEAE; FOOD CONTAMINATION; GUANIDINES; INSECTICIDES; NITRO COMPOUNDS; PESTICIDE RESIDUES; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

CUCUMIS;

EID: 84869077661     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.08.064     Document Type: Article

References (21)

1. M. Anastassiades, S. Lehotay, D. Stajnbaher, and F. Schenk Fast and easy multiresidue method employing acetonitrile extraction/portioning and dispersive solid-phase extraction for the determination of pesticide residues in produce Journal of AOAC International 86 2 2003 412 431
2. M. Careri, A. Mangia, and M. Musci Applications of liquid chromatography-mass spectrometry interfacing systems in food analysis: Pesticide, drug and toxic Journal of Chromatography A 727 1996 153 184
3. Codex Alimentarius Commision. (2009). Directrices para el diseño y La implementación de programas nacionales de aseguramiento de inocuidad alimentaria relacionados con el uso de medicamentos veterinarios en los animales destinados a producción de alimentos. CAC/GL 71.
4. European Commission. (2007). Method validation and quality control procedures for pesticide residues analysis in food and feed, Document No. SANCO/2007/3131. Available at: < www.ec.europa.eu/food/plant/protection/ resources/qualcontrol-en.pdf >.
5. K. Ford, and J. Casida Comparative metabolism and pharmacokinetics of seven neonicotinoid insecticides in spinach Journal of Agricultural and Food Chemistry 56 2008 10168 10175
6. FAO/WHO Recommended method of sampling for the determination of pesticide residues. Codex alimentarius commission of the joint FAOIWHO food standards programme 2nd ed. 1986 Food and Agricultural Organization/World Health Organization Rome [Part VI, Vol. XIII]
7. Global Agriculture Information Network (GAIN). (2007). Report no. JA7044. Available at: < http://www.fas.usda.gov/gainfiles/200708/146292145.pdf >, < http://www.eiken.pref.kanagawa.jp/004chousa/04reserch/files/38HTML/11- hayashi/11-hayashi.htm > (accessed 26 09 2010).
8. P. Jeschke, and R. Nauen Review Neonicotinoids - from zero to hero in insecticide chemistry Pest Management Science 64 2008 1084 1098
9. A. Kamel Refined methodology for the determination of neonicotinoid pesticides and their metabolites in honey bees and bee products by liquid chromatography-tandem mass spectrometry (LC-MS/MS)† Journal of Agricultural and Food Chemistry 58 2010 5926 5931
10. B. Kmellar, P. Fodor, L. Pareja, C. Ferrer, M.A. Martinez-Uroz, and A. Valverde Validation and uncertainty study of a comprehensive list of 160 pesticide residues in multi-class vegetables by liquid chromatography-tandem mass spectrometry Journal of Chromatography A 1215 2008 37 50
11. KFDA MRLs for Pesticides in Food 2011 Korea Food and Drug Administration Republic of Korea p. 104
12. S. Liu, Z. Zhen, F. Wei, Y. Ren, W. Gui, and H. Wu Simultaneous determination of seven neonicotinoid pesticide residues in food by ultraperformance liquid chromatography tandem mass spectrometry Journal of Agricultural and Food Chemistry 58 2010 3271 3278
13. S.J. Lehotay, K. Mastovska, and A.R. Lightfield Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables Journal of AOAC International 88 2005 615 629
14. S. Lehotay Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study Journal of AOAC International 90 2 2007 485 520
15. R. Nauen, U. Ebbinghaus-Kintscher, V.L. Salgado, and M. Kaussmann Thiamethoxam is a neonicotinoid precursor converted to clothianidin in insects and plants Pesticide Biochemistry and Physiology 76 2 2003 55 69
16. M. Ribani, C.H. Collins, and C.B.G. Bottoli Validation of chromatographic methods: Evaluation of detection and quantification limits in the determination of impurities in omeprazole Journal of Chromatography A 1156 2007 201 205
17. SANCO. (2009). Document No. 10684. Method validation and quality control procedures for pesticide residues analysis in food and feed.
18. C.D.S. Tomlin The pesticide manual: A world compendium 2003 British Crop Protection Council Hampshire, UK [13th ed.; p. 336]
19. G. Tanner, and C. Czerwenka LC-MS/MS analysis of neonicotinoid insecticides in honey: Methodology and residue findings in Austrian honeys Journal of Agricultural and Food Chemistry 59 2011 2271 12277
20. E. Watanabe, K. Baba, and S. Miyake Analytical evaluation of enzyme-linked immunosorbent assay for neonicotinoid dinotefuran for potential application to quick and simple screening method in rice samples Talanta 84 2011 1107 1111
21. E. Watanabe, K. Baba, and H. Eun Simultaneous determination of neonicotinoid insecticides in agricultural samples by solid-phase extraction cleanup and liquid chromatography equipped with diode-array detection Journal of Agricultural and Food Chemistry 55 2007 3798 3804