Aqueous route synthesis of mesoporous ZrO 2 by agarose templation

Journal of the American Ceramic Society

Volumn 95, Issue 11, 2012, Pages 3455-3462

  Ma, Xing ^a   Klosterman, Luke ^a   Hu, Yan Yan ^b   Liu, Xunpei ^a   Schmidt Rohr, Klaus ^b   Mallapragada, Surya ^a   Akinc, Mufit ^a  

^a Iowa State University   (United States)

^b IOWA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AFTER-HEAT TREATMENT; AGAROSE; AGAROSE GEL; BARRETT-JOYNER-HALENDA METHODS; HIERARCHICAL STRUCTURES; HIGH SURFACE AREA; MESOPOROUS; MESOPOROUS ZIRCONIA; MONOCLINIC PHASE; MORPHOLOGICAL FEATURES; NITROGEN ADSORPTION; NMR STUDIES; OH GROUP; POROUS ZIRCONIA; ROUTE SYNTHESIS; SELF-ASSEMBLING; TEMPLATION; ZIRCONYL NITRATES;

FOURIER TRANSFORM INFRARED SPECTROSCOPY; GAS ADSORPTION; NANOCOMPOSITES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SCANNING ELECTRON MICROSCOPY; SPECIFIC SURFACE AREA; TRANSMISSION ELECTRON MICROSCOPY; X RAY POWDER DIFFRACTION; ZIRCONIUM;

ZIRCONIA;

EID: 84868460763     PISSN: 00027820     EISSN: 15512916     Source Type: Journal    
DOI: 10.1111/j.1551-2916.2012.05417.x     Document Type: Article

References (41)

1. G. L. Drisko, V. Luca, E. Sizgek, N. Scales, and, R. A. Caruso, " Template Synthesis and Adsorption Properties of Hierarchically Porous Zirconium Titanium Oxides," Langmuir, 25 [ 9 ] 5286-93 (2009).
2. J. Zhou, M. Zhou, and, R. A. Caruso, " Agarose Template for the Fabrication of Macroporous Metal Oxide Structures," Langmuir, 22 [ 7 ] 3332-6 (2006).
3. J. H. Schattka, E. H.-M. Wong, M. Antonietti, and, R. A. Caruso, " Sol-Gel Templating of Membranes to Form Thick, Porous Titania, Titania/Zirconia and Titania/Silica Films," J. Mater. Chem., 16 [ 15 ] 1414-20 (2006).
4. K. Kordesch, and, G. Simader, Fuel Cells and Their Applications. Wiley-VCH Publishers, New York, 1996.
5. 2 and its Mixed Oxides," Catal. Today, 20 [ 2 ] 185-98 (1994).
6. T. V. Thamaraiselvi, and, S. Rajeswari, " Biological Evaluation of Bioceramic Materials-A Review," Trends Biomater. Artif. Organs., 18 [ 1 ] 9-17 (2004).
7. M. Huckel, et al,., " Porous Zirconia: A New Support Material for Enzyme Immobilization," J. Biochem. Biophys. Methods, 31 [ 3-4 ] 165-79 (1996).
8. 2 Bone Scaffold Coated with Hydroxyapatite with Fluorapatite Intermediate Layer," Biomaterials, 24, 3277-84 (2003).
9. C. Perego, and, P. L. Villa, eds. " The Catalytic Process from Laboratory to the Industrial Plant "; p. 293 in Proceedings of the 3rd Seminar on Catalysis, Edited by, D. Sanfiljppo,. Italian Chemical Society, Rimini, Italy, 1994.
10. M. L. Occellia, S. Biza, A. Aurouxb, and, G. J. Rayc, " Effects of the Nature of the Aluminum Source on the Acidic Properties of Some Mesostructured Materials," Microporous Mesoporous Mater., 26 [ 1-3 ] 193-213 (1998).
11. W. R. Moser, Advanced Catalysts and Nanostructured Materials: Modern Synthetic Methods. Academic Press, San Diego, CA, 1996, xxvi, p. 592
12. A. Vantomme, A. Leonard, Z. Y. Yan, and, B. L. Su, " Hierarchically Nanostructured Porous Functional Ceramics "; pp. 1933-8 in High-Performance Ceramics IV, Pts 1-3, Edited by, W. Pan, and, J. H. Gong,. Trans Tech Publications Ltd, Stafa-Zurich, 2007.
13. H. Zhang, G. C. Hardy, Y. Z. Khimyak, M. J. Rosseinsky, and, A. I. Cooper, " Synthesis of Hierarchically Porous Silica and Metal Oxide Beads Using Emulsion-Templated Polymer Scaffozds." Chem. Mater., 16 [ 22 ] 4245-56 (2004).
14. R. N. Das, S. Nad, and, P. Pramanik, " Nanocrystalline Yttria-Stabilized Zirconia Fibers from Plant Fibers and Their Polymer Composites," J. Am. Ceram. Soc., 91 [ 3 ] 1034-6 (2008).
15. G. K. Chuah, " An Investigation into the Preparation of High Surface Area Zirconia," Catal. Today, 49 [ 1-3 ] 131-9 (1999).
16. R. Srinivasana, M. B. Harrisa, S. F. Simpsona, R. J. De Angelisa, and, B. H. Davis, " Zirconium Oxide Crystal Phase: The Role of the pH and Time to Attain the Final pH for Precipitation of the Hydrous Oxide," J. Mater. Res., 3 [ 4 ] 787-97 (1988).
17. M. Rezaei, S. M. Alavi, S. Sahebdelfar, and, Z.-F. Yan, " Effect of Process Parameters on the Synthesis of Mesoporous Nanocrystalline Zirconia with Triblock Copolymer as Template," J. Porous Mater., 15 [ 2 ] 171-9 (2008).
18. S. Arnott, A. Fulmer, and, W. E. Scott, " Agarose Double Helix and its Function in Agarose Gel Structure," J. Mol. Biol., 90 [ 2 ] 269-84 (1974).
19. D. A. Rees, and, E. J. Welsh, " Secondary and Tertiary Structure of Polysaccharides in Solutions and Gels," Angew. Chem. Int. Ed., 16 [ 4 ] 214-23 (1977).
20. H. Itagaki, H. Fukiishi, T. Imai, and, M. Watase, " Molecular Structure of Agarose Chains in Thermoreversible Hydrogels Revealed by Means of a Fluorescent Probe Technique," J. Polym. Sci. Part B Polym. Phys., 43 [ 6 ] 680-8 (2005).
21. E. Fernándeza, C. Mijangosa, J. M. Guenetb, M. Teresa Cuberesc, and, D. Lõpeza, " New Hydrogels Based on the Interpenetration of Physical Gels of Agarose and Chemical Gels of Polyacrylamide," Eur. Polym. J., 45 [ 3 ] 932-9 (2009).
22. M. A. Blesa, A. J. G. Maroto, S. I. Passaggio, N. E. Figliolia, and, G. Rigotti, " Hydrous Zirconium Dioxide: Interfacial Properties, the Formation of Monodisperse Spherical Particles, and its Crystallization at High Temperatures," J. Mater. Sci., 20 [ 12 ] 4601-9 (1985).
23. P. Patnaik, Handbook of Inorganic Chemicals. McGraw-Hill, New York, 2002.
24. M. N. Rahaman, Ceramic Processing and Sintering. Materials Engineering. M. Dekker. Inc., New York, 2003, p. 875.
25. I. A. Sheka, and, T. V. Pevzner, " Solubility of Zirconium and Hafnium Hydroxides in Sodium Hydroxide Solution," Zh. Neorg. Khim., 5 [ 10 ] 2311-4 (1960).
26. S. Roy, " Nanocrystalline Undoped Tetragonal and Cubic Zirconia Synthesized Using Poly-Acrylamide as Gel and Matrix," J. Sol-Gel. Sci. Technol., 44, 227-33 (2007).
27. H. T. Rijnten, " Formation, preparation and properties of hydrous zirconia "; pp. 315-72 in Physical Chemistry and Aspects of Adsorbent and Catalysts, Edited by, B. G. Linsen,. Academic, New York, 1970.
28. V. Sánchez Escribano, C. del Hoyo Martínez, E. Fernández Lõpez, J. M. Gallardo Amores, and, G. Busca, " Characterization of a Ceria-Zirconia-Supported Cu Oxides Catalyst: An FT-IR Study on the Catalytic Oxidation of Propylene," Catal. Commun., 10 [ 6 ] 861-4 (2009).
29. A. A. M. Ali, and, M. I. Zaki, " Thermal and Spectroscopic Studies of Polymorphic Transitions of Zirconia During Calcination of Sulfated and Phosphated Zr(OH)(4) Precursors of Solid Acid Catalysts," Thermochim. Acta, 336 [ 1-2 ] 17-25 (1999).
30. D. J. Brasch, C. T. Chuah, and, L. D. Melton, " A C-13 Nmr-Study of Some Agar-Related Polysaccharides from New-Zealand Seaweeds," Aust. J. Chem., 34 [ 5 ] 1095-105 (1981).
31. V. Salinier, G. P. Niccolai, V. Dufaud, and, J. M. Basset, " Silica-Supported Zirconium Complexes and Their Polyoligosilsesquioxane Analogues in the Transesterification of Acrylates: Part 2. Activity, Recycling and Regeneration," Adv. Synth. Catal., 351 [ 13 ] 2168-77 (2009).
32. Y. Yusufoglua, Y. Hu, M. Kanapathipillaia, M. Kramera, Y. E. Kalaya, P. Thiyagarajana, M. Akinc, K. Schmidt-Rohra, and, S. Mallapragada, " Bioinspired Synthesis of Self-Assembled Calcium Phosphate Nanocomposites Using Block Copolymer-Peptide Conjugates," J. Mater. Res., 23 [ 12 ] 3196-212 (2008).
33. The International Centre for Diffraction Data. 2008, ICDD DDView + 4.8.0.0 PDF-4 RDB 4.0804, Newtown Square, PA.
34. D. L. Porter, and, A. H. Heuer, " Microstructural Development in Mgo-Partially Stabilized Zirconia (MG-PSZ)," J. Am. Ceram. Soc., 62 [ 5-6 ] 298-305 (1979).
35. B. D. Cullity, and, S. R. Stock, Elements of X-Ray Diffraction, 3rd Edition. Prentice Hall, 2001.
36. P. Kountouros, and, G. Petzow, " Defect chemistry, phase stability and properties of zirconia polycrystals "; pp. 30-48 in Science and Technology of Zirconia V, Edited by, S.P.S. Badwal, M.J. Bannister, and, R.H.J. Hannink,. Technomic Publishing Company Inc, Lancaster, Pennsylvania, PA, 1993.
37. A.e.a. Pluen, " Diffusion of Macromolecules in Agarose Gels: Comparison of Linear and Globular Configurations," Biophys. J., 77, 542-52 (1999).
38. M. Djabourov, A. H. Clark, D. W. Rowlands, and, S. B. Ross-Murphy, " Small-Angle X-ray Scattering Characterization of Agarose Sols and Gels," Macromolecules, 22, 180-8 (1989).
39. T. C. Laurent, " Determination of the Structure of Agarosegels by Gel Chromatography," Biochim. Biophys. Acta, 136 [ 2 ] 199-205 (1966).
40. S. Gregg, and, K. Sing, Adsorption, Surface Area and Porosity, 2nd edition. Academic Press, London, New York, 1982.
41. P. Trens, M. J. Hudson, and, R. Denoyel, " Formation of Mesoporous, Zirconium(IV) Oxides of Controlled Surface Areas," J. Mater. Chem., 8 [ 9 ] 2147-52 (1998).