Liquid-liquid test reactions to characterize two-phase mixing in microchannels

Heat Transfer Engineering

Volumn 34, Issue 2-3, 2013, Pages 169-177

  Kockmann, Norbert ^a   Karlen, Sven ^b   Girard, Christoph ^b   Roberge, Dominique M ^b  

^a TU DORTMUND UNIVERSITY   (Germany)

^b LONZA AG   (Switzerland)

Author keywords

[No Author keywords available]

Indexed keywords

ALKYL ACETATE; ALKYL GROUPS; AQUEOUS PHASE; CHANNEL GEOMETRY; CHARACTERISTIC TIME; DESIGN CONSIDERATIONS; DROPLET GENERATION; DROPLET SIZES; FLOW CHARACTERISTIC; FLOW REGIMES; FLUID PROPERTY; INTERFACIAL AREAS; LIQUID-LIQUIDS; ORGANIC PHASE; REDISPERSIONS; SODIUM HYDROXIDES; SPECIFIC AREAS; TEST REACTIONS; TWO PHASE MIXING; WATER SOLUBILITIES;

ANALYTIC EQUIPMENT; COALESCENCE; DROPS; MASS TRANSFER; MULTIPHASE FLOW; RATE CONSTANTS; SODIUM;

FOOD PROCESSING;

EID: 84867453409     PISSN: 01457632     EISSN: 15210537     Source Type: Journal    
DOI: 10.1080/01457632.2013.703508     Document Type: Conference Paper

References (18)

1. Stitt, E. H. 2002. Alternative Multiphase Reactors for Fine ChemicalsA World Beyond Stirred Tanks?. Chemical Engineering Journal, 90: 47-60.
2. Schneider, M.-A., Maeder, T., Ryser, P., and, Stoessel, F. 2004. A Microreactor-Based System for the Study of Fast Exothermic Reactions in Liquid Phase: Characterization of the System. Chemical Engineering Journal, 101: 241-250.
3. Stefanidis, G. D., Vlachos, D. G., Kaisare, N. S., and, Maestri, M. 2009. Methane Steam Reforming at Microscales: Operation Strategies for Variable Power Output at Millisecond Contact Times. AIChE Journal, 55: 180-191.
4. Crespo-Quesada, M., Grasemann, M., Semagina, N., Renken, A., and, Kiwi-Minsker, L. 2009. Kinetics of the Solvent-Free Hydrogenation of 2-Methyl-3-butyn-2-ol over a Structured Pd-Based Catalyst. Catalysis Today, 147: 247-254.
5. Grasemann, M., Renken, A., Kashid, M. N., and, Kiwi-Minsker, L. 2009. A Novel Compact Reactor for Three-Phase Hydrogenations. Chemical Engineering Science, 65: 364-371.
6. Kockmann, N., and, Roberge, D. M. 2009. Harsh Reaction Conditions in Continuous-Flow Microreactors for Pharmaceutical Production. Chemical Engineering & Technology, 32: 1682-1694.
7. Hessel, V, Renken, A., Schouten, J. C., and, Yoshida, J.-I. 2009. Micro Process Engineering, Weinheim, Germany: Wiley-VCH.
8. Gnther, A., and, Jensen, K. F. 2006. Multiphase Microfluidics: From Flow Characteristics to Chemical and Materials Synthesis. Lab on Chip, 6: 1487-1503.
9. Doku, G. N., Verboom, W., Reinhoudt, D. N., and, van den Berg, A. 2005. On-Microchip Multiphase ChemistryA Review of Microreactor Design Principles and Reagent Contacting Modes. Tetrahedron, 61: 2733-2742.
10. Hessel, V., Angeli, P., Gavriilidis, A., and, Lwe, H. 2005. Gas-Liquid and Gas-Liquid-Solid Microstructured Reactors: Contacting Principles and Applications. Industrial & Engineering Chemistry Research, 44: 9750-9769.
11. Kashid, M. N., and, Kiwi-Minsker, L. 2009. Microstructured Reactors for Multiphase Reactions: State of the Art. Industrial & Engineering Chemistry Research, 48: 6465-6485.
12. Kobayashi, I., and, Nakajima, M. 2006. Generation and Multiphase Flow of Emulsions in Microchannels. In Micro Process Engineering, Edited by: Kockmann, N. Vol. 5, Weinheim, Germany: Wiley-VCH.
13. Lb, P., Hessel, V., Men, Y., and, Pennemann, H. 2004. Impact of Fluid Path Geometry and Operating Parameters on l/l-Dispersion in Interdigital Micromixers. Chemical Engineering Science, 61: 2959-2967.
14. Jensen, F. W., Watson, G. M., and, Beckham, J. B. 1951. Study of Saponification Reaction Rate of Ethyl Acetate by High Frequency Titrimetry. Analytical Chemistry, 23: 1171-1773.
15. Bkenkamp, D., Desai, A., Yang, X., Tai, Y., Marzluff, E., and, Mayo, S. 1998. Microfabricated Silicon Mixers for Submillisecond Quench-Flow Analysis. Analytical Chemistry, 70: 232-236.
16. Asai, H., Nakamura, H., and, Yamada, M. 1997. Micellar-Catalyzed Alkaline Hydrolysis of n-Butyl Acetate by Cetyltrimethylamonium Bromide. Chemical Engineering Journal, 67: 19-25.
17. Bourne, J. R. 2004. Mixing and Selectivity of Chemical Reactions. Organic Process Research & Development, 7: 471-508.
18. Kockmann, N., and, Gottsponer, M. 2010. Heat Transfer Limitations of Gas-Liquid Exothermic Reactions in Microchannels. In FEDSM-ICNMM2010-30389 1-5. Montreal, Canada. August