Micromixing efficiency of a spinning disk reactor

Industrial and Engineering Chemistry Research

Volumn 51, Issue 36, 2012, Pages 11643-11652

  Jacobsen, Nikolas C ^a   Hinrichsen, Olaf ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

BARIUM SULFATE; DISK SPEED; EXPERIMENTAL INVESTIGATIONS; FEED LOCATIONS; INDUCTION TIME; IODIDE IODATES; MEAN SIZE; MICRO REACTOR; MICRO-MIXING; MIXING QUALITY; MIXING TIME; OPERATING PARAMETERS; PARALLEL REACTIONS; PRECIPITATION REACTION; ROTATIONAL SPEED; SPINNING DISK REACTOR; SPINNING DISKS;

BARIUM; CHEMICAL REACTORS; MIXING; REACTION KINETICS;

SYNTHESIS (CHEMICAL);

EID: 84866334462     PISSN: 08885885     EISSN: 15205045     Source Type: Journal    
DOI: 10.1021/ie300411b     Document Type: Article

References (30)

1. Aoune, A.; Ramshaw, C. Process intensification: heat and mass transfer characteristics of liquid films on rotating discs Int. J. Heat Mass Transfer 1999, 42, 2543-2556
2. 3 Catalyst J. Appl. Polym. Sci. 2006, 101, 8-19
3. Oxley, P.; Brechtelsbauer, C.; Ricard, F.; Lewis, N.; Ramshaw, C. Evaluation of Spinning Disk Reactor Technology for the Manufacture of Pharmaceuticals Ind. Eng. Chem. Res. 2000, 39, 2175-2182
4. 2 photocatalytic reactor Chemosphere 2001, 42, 397-403
5. Tai, C. Y.; Tai, C.-T.; Chang, M.-H.; Liu, H.-S. Synthesis of Magnesium Hydroxide and Oxide Nanoparticles Using a Spinning Disk Reactor Ind. Eng. Chem. Res. 2007, 46, 5536-5541
6. Meeuwse, M.; Lempers, S.; van der Schaaf, J.; Schouten, J. C. Liquid-Solid Mass Transfer and Reaction in a Rotor-Stator Spinning Disc Reactor Ind. Eng. Chem. Res. 2010, 49, 10751-10757
7. Meeuwse, M.; van der Schaaf, J.; Kuster, B. F. M.; Schouten, J. C. Gas-liquid mass transfer in a rotor-stator spinning disc reactor Chem. Eng. Sci. 2010, 65, 466-471
8. Meeuwse, M.; van der Schaaf, J.; Schouten, J. C. Mass Transfer in a Rotor-Stator Spinning Disk Reactor with Cofeeding of Gas and Liquid Ind. Eng. Chem. Res. 2010, 49, 1605-1610
9. Fournier, M.-C.; Falk, L.; Villermaux, J. A new parallel competing reaction system for assessing micromixing efficiency-Determination of micromixing time by a simple mixing model Chem. Eng. Sci. 1996, 51, 5187-5192
10. Schwarzer, H. C.; Peukert, W. Experimental Investigation into the Influence of Mixing on Nanoparticle Precipitation Chem. Eng. Technol. 2002, 25, 657-661
11. Guichardon, P.; Falk, L. Characterisation of micromixing efficiency by the iodide-iodate reaction system. Part I: experimental procedure Chem. Eng. Sci. 2000, 55, 4233-4243
12. Guichardon, P.; Falk, L.; Villermaux, J. Characterisation of micromixing effciency by the iodide-iodate reaction system. Part II: kinetic study Chem. Eng. Sci. 2000, 55, 4245-4253
13. Koälbl, A.; Kraut, M.; Schubert, K. The iodide iodate method to characterize microstructured mixing devices AIChE J. 2008, 54, 639-645
14. Schaer, E.; Guichardon, P.; Falk, L.; Plasari, E. Determination of local energy dissipation rates in impinging jets by a chemical reaction method Chem. Eng. J. 1999, 72, 125-138
15. Chen, Y.-S.; Tai, C. Y.-D.; Chang, M.-H.; Liu, H.-S. Characteristics of Micromixing in a Rotating Packed Bed J. Chin. Inst. Chem. Eng. 2006, 37, 63-69
16. Falk, L.; Commenge, J.-M. Performance comparison of micromixers Chem. Eng. Sci. 2010, 65, 405-411
17. Moore, S. R. Mass Transfer to thin liquid films on rotating surfaces, with and without chemical reaction. Dissertation, University of Newcastle upon Tyne, Newcastle upon Tyne, England, 1986.
18. Cafiero, L. M.; Baffi, G.; Chianese, A.; Jachuck, R. J. J. Process Intensification: Precipitation of Barium Sulfate Using a Spinning Disk Reactor Ind. Eng. Chem. Res. 2002, 41, 5240-5246
19. Dehkordi, A. M.; Vafaeimanesh, A. Synthesis of Barium Sulfate Nanoparticles Using a Spinning Disk Reactor: Effects of Supersaturation, Disk Rotation Speed, Free Ion Ratio, and Disk Diameter Ind. Eng. Chem. Res. 2009, 48, 7574-7580
20. Schneider, M.-A.; Maeder, T.; Ryser, P.; Stoessel, F. A microreactor-based system for the study of fast exothermic reactions in liquid phase: characterization of the system Chem. Eng. J. 2004, 101, 241-250
21. Baldyga, J.; Podgórska, W.; Pohorecki, R. Mixing-precipitation model with application to double feed semibatch precipitation Chem. Eng. Sci. 1995, 50, 1281-1300
22. McCarthy, E. D.; Dunk, W. A. E.; Boodhoo, K. V. K. Application of an intensified narrow channel reactor to the aqueous phase precipitation of barium sulphate J. Colloid Interface Sci. 2007, 305, 72-87
23. Nusselt, W. Die Oberflaechenkondensation des Wasserdampfes Z. Ver. Dtsch. Ing. 1916, 60, 569-575
24. Jachuck, R. J. J.; Ramshaw, C. Process intensification: Heat transfer characteristics of tailored rotating surfaces Heat Recovery Syst. CHP 1994, 14, 475-491
25. Kockmann, N.; Kiefer, T.; Engler, M.; Woias, P. Convective mixing and chemical reactions in microchannels with high flow rates Sens. Actuators, B 2006, 117, 495-508
26. Cai, Z. Herstellung von Polymeren und Partikeln in einem Spinning Disk Reactor. Dissertation, Technische Universitaät Muänchen, Muänchen, Germany, 2008.
27. Koälbl, A.; Schmidt-Lehr, S. The iodide iodate reaction method: The choice of the acid Chem. Eng. Sci. 2010, 65, 1897-1901
28. Carosso, P. A.; Pelizzetti, E. A stopped-flow technique in fast precipitation kinetics-The case of barium sulphate J. Cryst. Growth 1984, 68, 532-536
29. Monnin, C. A thermodynamic model for the solubility of Barite and celestite in electrolyte solutions and seawater to 200°C and to 1 kbar Chem. Geol. 1999, 153, 187-209
30. Bromley, L. A. Thermodynamic properties of strong electrolytes in aqueous solutions AlChE J. 1973, 19, 313-320