Development of a fully automated open-column chemicalseparation system-COLUMNSPIDER-and its application to Sr-Nd-Pb isotope analyses of igneous rock samples

Journal of Mineralogical and Petrological Sciences

Volumn 107, Issue 2, 2012, Pages 74-86

  Miyazaki, Takashi ^a   Vaglarov, Bogdan Stefanov ^a   Takei, Masakazu ^b   Suzuki, Masahiro ^b   Suzuki, Hiroaki ^b   Ohsawa, Kouzou ^b   Chang, Qing ^a   Takahashi, Toshiro ^a   Hirahara, Yuka ^a   Hanyu, Takeshi ^a   Kimura, Jun Ichi ^a   Tatsumi, Yoshiyuki ^a  

^a JAPAN AGENCY FOR MARINE EARTH SCIENCE AND TECHNOLOGY   (Japan)

^b HOYUTEC Co Ltd   (Japan)

Author keywords

Chemical separation; Fully automated; Open column; Pipetting robot; Sr Nd Pb isotope

Indexed keywords

EID: 84865815673     PISSN: 13456296     EISSN: 13493825     Source Type: Journal    
DOI: 10.2465/jmps.110520     Document Type: Article

References (57)

1. Aldrich, L.T., Doak, J.B. and Davis, G.L. (1953) The use of ion exchange columns in mineral analysis for age determination. American Journal of Science, 251, 377-387.
2. 144Nd isotopic ratios of Nd separated from geological standards by chromatographic methods. International Journal of Mass Spectrometry, 299, 27-34.
3. 144Nd ratios of twelve GSJ rock reference samples and reproducibility of the data. Geochemical Journal, 26, 105-109.
4. 204Pb double spike and thallium to correct for mass bias with adouble-focusing MC-ICP-MS. Chemical Geology, 211, 275-303.
5. 86Sr isotope ratio in USGS silicate reference materials by multi-collector ICP-mass spectrometry. International Journal of Mass Spectrometry, 242, 251-255.
6. Birck, J.L. (1986) Precision K-Rb-Sr isotopic analysis: Application to Rb-Sr chronology. Chemical Geology, 56, 73-83.
7. Blichert-Toft, J., Weis, D., Maerschalk, C., Agranier, A. and Albarède, F. (2003) Hawaiian hot spot dynamics as inferred from the Hf and Pb isotope evolution of Mauna Kea volcanoGeochemistry, Geophysics, Geosystems, 4(2), 8704, doi: 10.1029/2002GC000340.
8. Chu, Z.-Y., Chen F.-K., Yang Y.-H. and Guo J.-H. (2009) Precise determination of Sm, Nd concentrations and Nd isotopic compositions at the nanogram level in geological samples bythermal ionization mass spectrometry. Journal of Analytical Atomic Spectrometry, 24, 1534-1544.
9. Dickin, A.P. (1995) Radiogenic Isotope Geology. pp. 452, Cambridge University Press, New York.
10. Gale, N.H. (1996) A new method for extracting and purifying lead from difficult matrices for isotopic analysis. Analytica Chimica Acta, 332, 15-21.
11. + isotope analysis. Chemical Geology, 172, 347-359.
12. Hamamoto, T., Yuhara, M., Miyazaki, T., Fukase, M., Kondo, H., Ikawa, T., Ishioka, J., Kagami, H. and Shuto, K. (2000) Rb, Sr, Sm and Nd separation from rocks, minerals and natural water using ion-exchange resin. Science Reports of Niigata University, Series E (Geology), 15, 49-58.
13. Hirahara, Y., Takahashi, T., Miyazaki, T., Vaglarov, B.S., Chang, Q., Kimura, J.-I. and Tatsumi, Y. (2009) Precise Nd isotope analysis of igneous rocks using cation exchange chromatography and thermal ionization mass spectrometry (TIMS). JAMSTEC Report of Research and Devalopment, IFREE Technical Report, Special Issue, 65-71.
14. Horwitz, E.P., Chiarizia, R. and Dietz, M.L. (1992) A Novel Strontium-Selective Extraction Chromatographic Resin. Solvent Extraction and Ion Exchange, 10, 313-336.
15. Horwitz, E.P., Dietz, M.L., Rhoads, S., Felinto, C., Gale, N.H. and Houghton, J. (1994) A lead-selective extraction chromatographic resin and its application to the isolation of lead from geological samples. Analytica Chimica Acta, 292, 263-273.
16. Iizumi, S., Maehara, K., Morris, P.A. and Sawada, Y. (1994) Sr isotope data of some GSJ rock reference samples. Memoirs of the Faculty of Science, Shimane University, 28, 83-86.
17. Iizumi, S., Morris, P.A. and Sawada, Y. (1995) Nd isotope data for GSJ reference samples JB-1a, JB-3 and JG-1a and the La Jolla standard. Memoirs of the Faculty of Science, Shimane University, 29, 73-76.
18. Ishizuka, O., Taylor, R.N., Milton, J.A. and Nesbitt, R.W. (2003) Fluid-mantle interaction in an intra-oceanic arc: constraints from high-precision Pb isotopes, Earth and Planetary Science Letters, 211, 221-236.
19. Kagami, H., Iwata, M., Sano, S. and Honma, H. (1987) Sr and Nd isotopic compositions and Rb, Sr, Sm and Nd concentrations of standard samples. Technical Report of ISEI, Okayama University, Series B, No.4, 1-16.
20. Kimura, J.-I. and Nakano, N. (2004) Precise lead isotope analysis using Multiple Colector-Inductively Coupled Plasma-Mass Spectrometry (MC-ICP-MS): Analytical technique and evaluation of mass fractionation during Pb separation. Geoscience Report of Shimane University, 23, 9-15.
21. Koide, Y. and Nakamura, E. (1990) Lead isotope analyses of standard rock samples. Mass Spectroscopy, 38, 241-252. Kuritani, T and Nakamura, E. (2002) Precise isotope analysis of nanogram-level Pb for natural rock samples without use of double spikes. Chemical Geology, 186, 31-43
22. Le Fèvre, B. and Pin, C. (2005) A straightforward separation scheme for concomitant Lu-Hf and Sm-Nd isotope ratio and isotope dilution analysis. Analytica Chimica Acta, 543, 209-221.
23. Li, C.-F., Chen, F. and Li, X.-H. (2007) Precise isotopic measurements of sub-nanogram Nd of standard reference material by thermal ionization mass spectrometry using the NdO+ technique. International Journal of Mass Spectrometry, 266, 34-41.
24. Li, C.-F., Li, X.-H, Li, Q.-L., Guo, J.-H. and Li, X.-H. (2011) Directly determining 143Nd/144Nd isotope ratios using thermal ionization mass spectrometry for geological samples without separation of Sm-Nd. Journal of Analytical Atomic Spectrometry, doi: 10.1039/C0JA00081G.
25. Makishima, A. and Nakamura, E. (1991) Precise measurement of cerium isotope composition in rock samples. Chemical Geology, 94, 1-11.
26. Makishima, A., Nath, B.N. and Nakamura, E. (2007) Precise determination of Pb isotope ratios by simple double spike MCICP-MS technique without Tl addition. Journal of Analytical Atomic Spectrometry, 22, 407-410.
27. Makishima, A., Nath, B.N. and Nakamura, E. (2008) New sequential separation procedure for Sr, Nd and Pb isotope ratio measurement in geological material using MC-ICP-MS and TIMS. Geochemical Journal, 42, 237-246.
28. Manhes, G., Minster, J.F. and Allègre, C.J. (1978) Comparative uranium-thorium-lead and rubidium-strontium study of the Saint Severin amphoterite: consequences for early solar system chronology. Earth and Planetary Science Letters, 39, 14-24.
29. Meynadier, L., Gorge, C., Birck, J.-L. and Allègre, C.J. (2006) Automated separation of Sr from natural water samples or carbonate rocks by high performance ion chromatography. Chemical Geology, 227, 26-36.
30. Míková, J. and Denková, P. (2007) Modified chromatographic separation scheme for Sr and Nd isotope analysis in geological silicate samples. Journal of Geosciences, 52, 221-226.
31. Misawa, K., Yamazaki, F., Ihira, N. and Nakamura, N. (2000) Separaiton of rare earth elements and strontium from chondritic meteorites by miniaturized extraction chromatography for elemental and isotopic analyses. Geochemical Journal, 34, 11-21.
32. Miyazaki, T. and Shuto, K. (1998) Sr and Nd isotope ratios of twelve GSJ rock reference samples. Geochemical Journal, 32, 345-350.
33. Miyazaki, T., Kanazawa, N., Takahashi, T., Hirahara, Y., Vaglarov, B.S., Chang, Q., Kimura, J.-I. and Tatsumi, Y. (2009) Precise Pb isotope analysis of igneous rocks using fully-automated double spike thermal ionization mass spectrometry (FA-DSTIMS). JAMSTEC Report of Research and Devalopment, IFREE Technical Report, Special Issue, 73-80.
34. Na, C.-K., Nakano, T., Tazawa, K., Sakagawa, M. and Ito, T. (1995). A systematic and practical method of liquid chromatography for the determination of Sr and Nd isotopic ratios and REE concentrations in geological samples. Chemical Geology, 123, 225-237.
35. Ohno, T. and Hirata, T. (2007) Simultaneous determination of mass-dependent isotopic fractionation and radiogenic isotope variation of Strontium in geochemical samples by Multiple Collector-ICP-Mass Spectrometry. Analytical Sciences, 23, 1275-1280.
36. Orihashi, Y., Maeda, J., Tanaka, R., Zeniya, R. and Niida, K. (1998) Sr and Nd isotopic data for the seven GSJ rock reference samples; JA-1, JB-1a, JB-2, JB-3, JG-1a, JGb-1 and JR-1. Geochemical Journal, 32, 205-211.
37. Pin, C. and Bassin, C. (1992) Evaluation of a strontium-specific extraction chromatographic method for isotopic analysis in geological materials. Analytica Chimica Acta, 269, 249-255.
38. Pin, C., Briot, D., Bassin, C. and Poitrasson, F. (1994) Concomitant separation of strontium and samarium-neodymium for isotopic analysis in silicate samples, based on specific extraction chromatography. Analytica Chimica Acta, 298, 209-217.
39. Pin, C. and Zalduegui, J.-F.S. (1997) Sequential separation of light rare-earth elements, thorium and uranium by miniaturized extraction chromatography: Application to isotopic analyses of silicate rocks. Analytica Chimica Acta, 339, 79-89.
40. Raczek, I., Peter Jochum, K. and Hofmann, A.W. (2003) Neodymium and Strontium Isotope Data for USGS Reference Materials BCR-1, BCR-2, BHVO-1, BHVO-2, AGV-1, AGV-2, GSP-1, GSP-2 and Eight MPI-DING Reference Glasses. Geostandards Newsletter: The Journal of Geostandards and Geoanalysis, 27, 173-179.
41. 146Nd, a natural tracer: an application to oceanic basalts. Earth and Planetary Science Letters, 31, 269-278.
42. Scher, H.D. and Delaney, M.L. (2010) Breaking the glass ceiling for high resolution Nd isotope records in early Cenozoic paleoceanography. Chemical Geology, 269, 329-338.
43. Shibata, T., Yoshikawa, M. and Tatsumi, Y. (2003) An analytical method for determining precise Sr and Nd isotopic compositions and result for thirteen rock standard materials. Frontier Research on Earth Evolution, 1, 363-367.
44. Shibata, T. and Yoshikawa, M. (2004) Precise isotope determination of trace amounts of Nd in Magnesium-rich samples. Journal of the Mass Spectrometry Society of Japan, 52, 317-324.
45. Shibata, T., Yoshikawa, M. and Sugimono, T. (2007) Semi-automatic chemical separation system for Sr and Nd isotope analyses. Journal of Minaralogical and Petrological Sciences, 102, 298-301.
46. Stray, H. (1992) Improved HPLC method for the separation of Rb and Sr in connection with Rb-Sr dating. Chemical Geology, 102, 129-135.
47. Takahashi, T., Hirahara, Y., Miyazaki, T., Vaglarov, B.S., Chang, Q., Kimura, J.-I. and Tatsumi, Y. (2009) Precise determination of Sr isotope ratios in igneous rock samples and application to micro-analysis of plagioclase phenocrysts. JAMSTEC Report of Research and Devalopment, IFREE Technical Report, Special Issue, 59-64.
48. Tanaka, T., Togashi, S., Kamioka, H., Amakawa, H., Kagami, H., Hamamoto, T., Yuhara, M., Orihashi, Y., Yoneda, S., Shimizu, H., Kunimaru, T., Takahashi, K., Yanagi, T., Nakano, T., Fujimaki, H., Shinjo, R., Asahara, Y., Tanimizu, M. and Dragusanu, C. (2000) JNdi-1: a neodymium isotopic reference in consistency with La Jolla neodymium. Chemical Ge Geology, 168, 279-281.
49. Tanimizu, M. and Ishikawa, T. (2006) Development of rapid and precise Pb isotope analytical techniques using MC-ICP-MS and new results for GSJ rock reference samples. Geochemcal Journal, 40, 121-133.
50. Walker, R.J., Carlson, R.W., Shirey, S.B. and Boyd, F.R. (1989) Os, Sr, Nd, and Pb isotope systematics of southern African peridotite xenoliths: Implications for the chemical evolution of subcontinental mantle. Geochimica et Cosmochimica Acta, 53, 1583-1595.
51. Weiss, D.J., Kober, B., Dolgopolova, A., Gallagher, K., Spiro, B., Le Roux, G., Mason, T.F.D., Kylander, M. and Coles, B.J. (2004) Accurate and precise Pb isotope ratio measurements in environmental samples by MC-ICP-MS. International Journal of Mass Spectrometry, 232, 205-215.
52. Weis, D., Kieffer, B., Maerschalk, C., Barling, J., de Jong, J., Williams, G.A., Hanano, D., Pretorius, W., Mattielli, N., Scoates, J.S., Goolaerts, A., Friedman, R.M. and Mahoney, J.B. (2006) High-precision isotopic characterization of USGS reference materials by TIMS and MC-ICP-MS. Geochemistry Geophysics Geosystems, 7, Q08006, doi:10.1029/2006GC001283.
53. Woodhead, J.D. and Hergt, J.M. (2000) Pb-Isotope analyses of USGS reference materials. Geostandards Newsletter: The Journal of Geostandards and Geoanalysis, 24, 33-38.
54. Yang, Y.-H., Zhang, H.-F., Chu, Z.-Y., Xie, L.-W. and Wu, F.-Y. (2010a) Combined chemical separation of Lu, Hf, Rb, Sr, Sm and Nd from a single rock digest and precise and accurate isotope determinations of Lu-Hf, Rb-Sr and Sm-Nd isotope systems using Multi-Collector ICP-MS and TIMS. International Journal of Mass Spectrometry, 290, 120-126.
55. Yang, Y.-H., Wu, F.-Y., Xie, L.-W. and Zhang, Y.-B. (2010b) High-Precision Measurements of the 143Nd/144Nd Isotope Ratio in Certified Reference Materials without Nd and Sm Separation by Multiple Collector Inductively Coupled Plasma Mass Spectrometry. Analytical Letters, 43, 142-150.
56. Yang, Y.-H., Chu, Z.-Y., Wu, F.-Y., Xie, L.-W. and Yang, J.-H. (2011) Precise and accurate determination of Sm, Nd concentrations and Nd isotopic compositions in geological samples by MC-ICP-MS. Journal of Analytical Atomic Spectrometry, 26, 1237-1244.
57. Yoshikawa, M. and Nakamura, E. (1993) Precise isotope determination of trace amounts of Sr in Magnesium-rich samples. Journal of Mineralogy, Petrology and Economic Geology, 88, 548-561.