Identification and quantification of dimethylamylamine in geranium by liquid chromatography tandem mass spectrometry

Analytical Chemistry Insights

Volumn 7, Issue 1, 2012, Pages 47-58

  Li, J S ^a   Chen, M ^a   Li, Z C ^a  

^a Intertek AAC Labs   (United States)

Author keywords

1,3 dimethylamylamine; 1,4 dimethylamylamine; Geranium (Pelargonium graveolens); liquid chromatography tandem mass spectrometry (LC MS MS)

Indexed keywords

EID: 84865092972     PISSN: None     EISSN: 11773901     Source Type: Journal    
DOI: 10.4137/ACI.S9969     Document Type: Article

References (20)

1. Ping Z, Jun Q. A study on the chemical constituents of geranium Oil. J Guizhou Inst Technol. 1996;25:82-5.
2. Babu KGD, Kaul VK. Variation in essential oil composition of rose-scented geranium (Pelargonium sp.) distilled by different distillation techniques. Flavour Fragr J. 2005;20:222-31.
3. Fayed SA. Antioxidant and Anticancer Activities of Citrus reticulate (Petitgrain mandarin) and Pelargonium graveolens (Geranium) Essential Oils. Res J Agric Bio Sci. 2009;5:740-7.
4. Gomes PB, Mata VG, Rodrigues AE. Characterization of Portuguese-grown geranium oil (Pelargonium sp.). J Essent Oil Res. 2004;16:490-5.
5. Jain N, Aggarwal KK, Syamasundar KV, Srivastava SK, Kumar S. Essential oil composition of geranium (Pelargonium sp.) from the plains of northern India. Flavour Fragr J. 2001;16:44-6.
6. Jalali-Heravi M, Zekavat B, Sereshti H. Characterization of essential oil components of Iranian geranium oil using gas chromatography-mass spectrometry combined with chemometric resolution techniques. J Chromatogr A. 2006;1114:154-63.
7. Kulkarni RN, Mallavarapu GR, Baskaran K, Ramesh S, Kumar S. Composition of the essential oils of two isomenthone-rich variants of geranium (Pelargonium sp.). Flavour Fragr J. 1998;13:389-92.
8. Lalli JYY, Viljoen AM, Baser KHC, Demirci B, Ozek T. The essential oil composition and chemotaxonomical appraisal of South African Pelargoniums (Geraniaceae). J Essent Oil Res. 2006;18:89-105.
9. Peterson A, Machmudah S, Roy BC, Goto M, Sasaki M, Hirose T. Extraction of essential oil from geranium (Pelargonium graveolens) with supercritical carbon dioxide. J Chem Technol Biotechnol. 2006;81:167-72.
10. Prakasa EVS, Rao RS, Rao G, Ramesh S. Seasonal variation in oil content and its composition in two chemotypes of scented geranium (Pelargonium sp.). J Essent Oil Res. 1995;7:159-63.
11. Shellie RA, Marriott PJ. Comprehensive two-dimensional gas chromatography-mass spectrometry analysis of Pelargonium graveolens essential oil using rapid scanning quadrupole mass spectrometry. Analyst. 2003;128:879-83.
12. Vermia RS, Verma RK, Yadav AK, Chauhan A. Changes in the essencial oil composition of rose-scented geranium (Pelargonium graveolens L' Herit. Ex. Ait) due to date of transplanting under hill conditions of Uttarakhand. Indian J Nat Prod Resour. 2010;1:367-70.
13. Vorce SP, Holler JM, Cawrse BM, Magluilo Jr J. Dimethylamylamine: a drug causing positive immunoassay results for amphetamines. J Anal Toxicol. 2011;35:183-7.
14. Perrenoud L, Saugy M, Saudan C. Detection in urine of 4-methyl-2-hexaneamine, a doping agent. J Chromatogr B. 2009;877:3767-70.
15. Dorsey JD, Dill KA. The molecular mechanism of retention in reversed-phase liquid chromatography. Chem Rev. 1989;89:331-4.
16. Mallet CR, Lu Z, Mazzeo JR. A study of ion suppression effects in electrospray ionization from mobile phase additives and solid-phase extracts. Rapid Commun Mass Spectrom. 2004;18:49-58.
17. Annesley TM. Ion Suppression in Mass Spectrometry. Clin Chem. 2003;49:1041-3.
18. Batista Jr JM, Lopez SN, Mota JS, et al. Resolution and absolute configuration assignment of a natural racemic chromane from Peperomia obtusifolia (Piperaceae). Chirality. 2009;21:799-801.
19. Jung DJ, Porzel A, Huneck S. Gigasol and other coumarins from Angelica gigas, Phytochem. 1991;30:710-2.
20. Wust M, Reindl J, Fuchs S, Beck T, Mosandl A. Structure elucidation, enantioselective analysis, and biogenesis of nerol oxide in Pelargonium species. J Agric Food Chem. 1999;47:3145-50.