Preparation, structure, and reactivity of dipalladium(I) complexes containing the carbanion 2-C 6F 4PPh 2: Coexistence of distinct, noninterconverting head-to-head [dipalladium(0/II)] and head-to-tail [dipalladium(I)] species

Organometallics

Volumn 31, Issue 15, 2012, Pages 5561-5572

  Bhargava, Suresh K ^a   Privér, Steven H ^a   Willis, Anthony C ^b   Bennett, Martin A ^b  

^a RMIT UNIVERSITY   (Australia)

^b AUSTRALIAN NATIONAL UNIVERSITY   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

BINDING MODES; BRIDGING LIGANDS; DINUCLEAR; IN-SITU; IODOBENZENE; METAL ATOMS; METAL-METAL DISTANCES; METAL-METAL INTERACTIONS; METHYL COMPLEXES; METHYL IODIDE; MIXED-VALENT; OXIDATIVE ADDITIONS; PALLADIUM COMPLEXES; REDUCTIVE ELIMINATION; TERT-BUTYL ISOCYANIDE; TRIPHENYLARSINE;

BINDING ENERGY; CHLORINE COMPOUNDS; CYANIDES; FLUORINE; IODINE; ISOMERS; LIGANDS; METALS; PALLADIUM; PLATINUM; PLATINUM COMPOUNDS; SEPARATION;

PALLADIUM COMPOUNDS;

EID: 84864984643     PISSN: 02767333     EISSN: 15206041     Source Type: Journal    
DOI: 10.1021/om300525p     Document Type: Article

References (75)

1. Mohr, F.; Privér, S. H.; Bhargava, S. K.; Bennett, M. A. Coord. Chem. Rev. 2006, 250, 1851
2. Chakravarty, A. R.; Cotton, F. A.; Tocher, D. A.; Tocher, J. H. Organometallics 1985, 4, 8
3. Bennett, M. A.; Dirnberger, T.; Hockless, D. C. R.; Wenger, E.; Willis, A. C. J. Chem. Soc., Dalton Trans. 1998, 2367
4. Bender, R.; Bouaoud, S. E.; Braunstein, P.; Dusausoy, Y.; Merabet, J.; Raya, J.; Rouag, D. J. Chem. Soc., Dalton Trans. 1999, 735
5. Bennett, M. A.; Berry, D. E.; Bhargava, S. K.; Ditzel, E. J.; Robertson, G. B.; Willis, A. C. J. Chem. Soc., Chem. Commun. 1987, 1613
6. Bennett, M. A.; Bhargava, S. K.; Messelhäuser, J.; Privér, S. H.; Welling, L. L.; Willis, A. C. Dalton Trans. 2007, 3158
7. Aarif, A. M.; Estevan, F.; García-Barnabé, A.; Lahuerta, P.; Sanaú, M.; Ubeda, M. A. Inorg. Chem. 1997, 36, 6472
8. Estevan, F.; García-Bernabé, A.; Lahuerta, P.; Sanaú, M.; Ubeda, M. A.; Ramírez de Arellano, M. C. Inorg. Chem. 2000, 39, 5964
9. Bennett, M. A.; Bhargava, S. K.; Keniry, M. A.; Privér, S. H.; Simmonds, P. A.; Wagler, J. A.; Willis, A. C. Organometallics 2008, 27, 5361
10. Usón, R.; Forniés, J. Adv. Organomet. Chem. 1988, 28, 219
11. Alves, O. L.; Vitorge, M.; Sourisseau, C. Nouv. J. Chim. 1983, 7, 231
12. Otsuka, S.; Nakamura, A.; Tatsuno, Y. J. Am. Chem. Soc. 1969, 91, 6994
13. Brown, M. P.; Puddephatt, R. J.; Rashidi, M.; Seddon, K. R. J. Chem. Soc., Dalton Trans. 1977, 951
14. Brown, M. P.; Puddephatt, R. J.; Rashidi, M.; Seddon, K. R. J. Chem. Soc., Dalton Trans. 1978, 1540
15. Xu, Q.; Heaton, B. T.; Jacob, C.; Mogi, K.; Ichihashi, Y.; Souma, Y.; Kanamori, K.; Eguchi, T. J. Am. Chem. Soc. 2000, 122, 6862
16. Bennett, M. A.; Bhargava, S. K.; Privér, S. H.; Willis, A. C. Eur. J. Inorg. Chem. 2008, 3467
17. Deacon, G. B.; Nelson-Reed, K. T. J. Organomet. Chem. 1987, 322, 257
18. Deacon, G. B.; Elliott, P. W.; Erven, A. P.; Meyer, G. Z. Anorg. Allg. Chem. 2005, 631, 843
19. Wisner, J. M.; Bartczak, T. J.; Ibers, J. A.; Low, J. L.; Goddard, W. A., III. J. Am. Chem. Soc. 1986, 108, 347
20. Wisner, J. M.; Bartczak, T. J.; Ibers, J. A. Organometallics 1986, 5, 2044
21. Albano, V.; Bellon, P. L.; Scatturin, V. J. Chem. Soc., Chem. Commun. 1966, 507
22. Chaloner, P. A.; Hitchcock, P. B.; Broadwood-Strong, G. T. L. Acta Crystallogr., Sect. C 1989, 45, 1309
23. 3 plane: Stromnova, T. A.; Sergienko, V. S.; Kisin, A. V.; Porai-Koshits, M. A.; Moiseev, I. I. Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.) 1987, 36, 821
24. Fong, S.-W. A.; Evans, K.; Henderson, W.; Nicholson, B. K.; Hor, T. S. A. Inorg. Chim. Acta 2010, 363, 301
25. Barnes, N. A.; Brisdon, A. K.; Fay, J. G.; Pritchard, R. G.; Warren, J. E. Inorg. Chim. Acta 2005, 358, 2543
26. Arnold, D. P.; Bennett, M. A.; McLaughlin, G. M.; Robertson, G. B.; Whittaker., M. J. J. Chem. Soc., Chem. Commun. 1983, 32
27. Allen, E. A.; Wilkinson, W. Spectrochim. Acta 1974, 30A, 1219
28. Goggin, P. L. J. Chem. Soc., Dalton Trans. 1974, 1483
29. de Graaf, W.; Boersma, J.; Smits, W. J. J.; Spek, A. L.; van Koten, G. Organometallics 1989, 8, 2907
30. Kim, Y. J.; Osakada, K.; Takenaka, A.; Yamamoto, A. J. Am. Chem. Soc. 1990, 110, 1096
31. Crutchley, R. J.; Powell, J.; Faggiani, R.; Lock, C. J. L. Inorg. Chim. Acta 1977, 24, L15
32. Osakada, K.; Ozawa, Y.; Yamamoto, A. J. Chem. Soc., Dalton Trans. 1991, 759
33. 2O as a result of 50% disorder between terminal iodide and methyl ligands: Olmstead, M. M.; Farr, J. P.; Balch, A. L. Inorg. Chim. Acta 1981, 52, 47
34. Bennett, M. A.; Bhargava, S. K.; Ke, M.; Willis, A. C. J. Chem. Soc., Dalton Trans. 2000, 3537
35. Werner, H. Adv. Organomet. Chem. 1981, 19, 155, and references therein.
36. Murahashi, T.; Kurosawa, H. Coord. Chem. Rev. 2002, 231, 207, and references therein.
37. Maitlis, P. M.; Espinet, P.; Russell, M. J. H. In Comprehensive Organometallic Chemistry; Wilkinson, G.; Stone, F. G. A.; Abel, E. W., Eds.; Pergamon: Oxford, 1982; Vol. 6, p 265.
38. Dixon, K. R.; Dixon, A. C. In Comprehensive Organometallic Chemistry II; Abel, E. W.; Stone, F. G. A.; Wilkinson, G., Eds.; Pergamon: Oxford, 1995; Vol. 9, p 193.
39. Canty, A. J. In Comprehensive Organometallic Chemistry II; Abel, E. W.; Stone, F. G. A.; Wilkinson, G., Eds.; Pergamon: Oxford, 1995; Vol. 9, p 226.
40. Barder, T. J. Am. Chem. Soc. 2006, 128, 898
41. Han, X.; Weng, Z.; Hor, T. S. A. J. Organomet. Chem. 2007, 692, 5690
42. Proutiere, F.; Aufiero, M.; Schoenebeck, F. J. Am. Chem. Soc. 2012, 134, 606
43. Aufiero, M.; Proutiere, F.; Schoenebeck, F. Angew. Chem., Int. Ed. 2012, 51, 7226
44. Young, S. J.; Kellenberger, B.; Reibenspies, J. H.; Himmel, S. E.; Manning, M.; Anderson, O. P.; Stille, J. K. J. Am. Chem. Soc. 1988, 110, 5744
45. Rashidi, M.; Vittal, J. J.; Puddephatt, R. J. J. Chem. Soc., Dalton Trans. 1994, 1283
46. Benner, L. S.; Balch, A. L. J. Am. Chem. Soc. 1978, 100, 6099
47. Guimerans, R. R.; Balch, A. L. Inorg. Chim. Acta 1983, 22, L177
48. Farr, J. P.; Wood, F. E.; Balch, A. L. Inorg. Chem. 1983, 22, 3387
49. Párkányi, L.; Szalontai, G.; Besenyei, G. Inorg. Chim. Acta 2006, 359, 2933
50. Anderson, G. K.; Kumar, R. Inorg. Chim. Acta 1985, 97, L21
51. Balch, A. L.; Hunt, C. T.; Lee, C. L.; Olmstead, M. M.; Farr, J. P. J. Am. Chem. Soc. 1981, 103, 3764
52. Puddephatt, R. J. Chem. Soc. Rev. 1983, 12, 99
53. Bennett, M. A.; Bhargava, S. K.; Mirzadeh, N.; Privér, S. H.; Wagler, J.; Willis, A. C. Dalton Trans. 2009, 7537
54. Sakamoto, M.; Shimizu, I.; Yamamoto, A. Chem. Lett. 1995, 12, 1101
55. Kwong, F. Y.; Lai, C. M.; Lu, M.; Chan, K. S. Tetrahedron 2004, 60, 5635
56. Penno, D.; Lillo, V.; Koshevoy, I. O.; Sanaú, M.; Ubeda, M. A.; Lahuerta, P.; Fernández, E. Chem.-Eur. J. 2008, 14, 10648
57. Ugo, R.; Cariati, F.; La Monica, G. Inorg. Synth. 1968, 11, 195
58. Coulson, D. R. Inorg. Synth. 1990, 28, 107
59. Kemmitt, R. D. W.; McKenna, P.; Russell, D. R.; Sherry, L. J. S. J. Chem. Soc., Dalton Trans. 1985, 259
60. Tatsuno, Y.; Yoshida, T.; Otsuka, S. Inorg. Synth. 1990, 28, 342
61. Green, M.; Howard, J. A. K.; Murray, M.; Spencer, J. L.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1977, 1509
62. Ogoshi, S.; Morita, M.; Inoue, K.; Kurosawa, H. J. Organomet. Chem. 2004, 689, 662
63. Dell'Amico, D. B.; Labella, L.; Marchetti, F.; Samaritani, S. J. Organomet. Chem. 2011, 696, 1349
64. gNMR (version 5.1) for Windows; Cherwell Scientific Publishing.
65. SMART software (version 5.625) for the CCD Detector System; Bruker AXS Inc.: Madison, WI, 2001.
66. SAINTPLUS software (version 6.22) for the CCD Detector System; Bruker AXS Inc.: Madison, WI, 2001.
67. Blessing, R. H. Acta Crystallogr., Sect. A 1995, 51, 33
68. Sheldrick, G. M. SHELXTL (version 6.10); University of Göttingen, Germany, 1994.
69. COLLECT Software; Nonius-BV: Delft, The Netherlands, 1997-2001.
70. Otwinowski, Z.; Minor, W. In Methods in Enzymology; Carter, C. W., Jr.; Sweet, R. M., Eds.; Academic Press, 1997; Vol. 276, pp 307-326.
71. SIR92: Altomare, A.; Cascarano, G.; Giacovazzo, C.; Guagliardi, A.; Burla, M. C.; Polidori, G.; Camalli, M. J. Appl. Crystallogr. 1994, 27, 435
72. Betteridge, P. W.; Carruthers, J. R.; Cooper, R. J.; Prout, K.; Watkin, D. J. J. Appl. Crystallogr. 2003, 36, 1487
73. International Tables for X-ray Crystallography; The Kynoch Press: Birmingham, England, 1974; Vol. IV.
74. International Tables for X-ray Crystallography; Kluwer Academic: Boston, MA, 1992; Vol C.
75. Krannich, L. K.; Kanjolia, R. K.; Watkins, C. L. Magn. Reson. Chem. 1987, 25, 320